ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 Summary Report Surface Area Single point surface area at P/Po = 0.291245783: 4.5679 m²/g BET Surface Area: 4.7358 m²/g t-Plot External Surface Area: 5.3333 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å width: 3.525 m²/g BJH Desorption cumulative surface area of pores between 17.000 Å and 3000.000 Å width: 5.1148 m²/g Pore Volume Single point desorption total pore volume of pores less than 983.417 Å width at P/Po = 0.979908857: 0.011105 cm³/g t-Plot micropore volume: -0.000291 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å width: 0.011002 cm³/g BJH Desorption cumulative volume of pores between 17.000 Å and 3000.000 Å width: 0.011809 cm³/g Pore Size Desorption average pore width (4V/A by BET): 93.7986 Å BJH Adsorption average pore width (4V/A): 124.860 Å BJH Desorption average pore width (4V/A): 92.350 Å Horvath-Kawazoe Maximum pore volume at P/Po = 0.010616744: 0.001117 cm³/g Median pore width: 7.487 Å ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 Isotherm Tabular Report Quantity Relative Absolute Adsorbed Elapsed Saturation Pressure Pressure (cm³/g Time Pressure (P/Po) (mmHg) STP) (h:min) (mmHg) ----- 1.#QNAN0000 1.#QNAN0 1.#QNB 01:01 745.283386 0.000005550 0.004135 0.0177 01:53 1.#QNAN0 0.000003040 0.002265 0.0383 02:33 1.#QNAN0 0.000003400 0.002533 0.0580 03:13 1.#QNAN0 0.000005923 0.004411 0.0756 03:54 1.#QNAN0 0.000010446 0.007779 0.0900 04:35 1.#QNAN0 0.000020477 0.015248 0.1093 04:45 1.#QNAN0 0.000034621 0.025780 0.1279 04:56 1.#QNAN0 0.000062088 0.046231 0.1530 05:07 1.#QNAN0 0.000094570 0.070415 0.1749 05:17 1.#QNAN0 0.000134080 0.099829 0.1960 05:28 1.#QNAN0 0.000180728 0.134556 0.2165 05:38 1.#QNAN0 0.000217960 0.162271 0.2306 05:47 1.#QNAN0 0.000258139 0.192177 0.2441 05:56 1.#QNAN0 0.000301171 0.224206 0.2570 06:05 1.#QNAN0 0.000346820 0.258181 0.2695 06:14 1.#QNAN0 0.000395225 0.294205 0.2814 06:23 1.#QNAN0 0.000445538 0.331647 0.2930 06:32 1.#QNAN0 0.000498294 0.370906 0.3041 06:40 1.#QNAN0 0.000553132 0.411712 0.3148 06:48 1.#QNAN0 0.000634363 0.472163 0.3295 06:55 1.#QNAN0 0.000715871 0.532816 0.3429 07:02 1.#QNAN0 0.000794827 0.591566 0.3550 07:10 1.#QNAN0 0.000871012 0.648251 0.3659 07:17 1.#QNAN0 0.000943202 0.701960 0.3755 07:24 1.#QNAN0 0.001011955 0.753108 0.3843 07:31 1.#QNAN0 0.001076923 0.801438 0.3922 07:38 1.#QNAN0 0.001138415 0.847178 0.3993 07:45 1.#QNAN0 0.001196086 0.890072 0.4057 07:52 1.#QNAN0 0.001249156 0.929541 0.4116 07:59 1.#QNAN0 0.001297980 0.965847 0.4168 08:06 1.#QNAN0 0.001343826 0.999936 0.4215 08:13 1.#QNAN0 0.001387241 1.032214 0.4259 08:20 1.#QNAN0 0.001427016 1.061782 0.4298 08:27 1.#QNAN0 0.001463273 1.088732 0.4332 08:34 1.#QNAN0 0.001497694 1.114313 0.4365 08:41 1.#QNAN0 0.001529246 1.137763 0.4393 08:47 1.#QNAN0 0.001557662 1.158875 0.4419 08:54 1.#QNAN0 0.001585002 1.179185 0.4443 09:01 1.#QNAN0 0.001610228 1.197921 0.4464 09:08 1.#QNAN0 0.001632930 1.214779 0.4484 09:15 1.#QNAN0 0.001654942 1.231122 0.4502 09:22 1.#QNAN0 0.001731062 1.287716 0.4567 09:29 1.#QNAN0 0.001807790 1.344752 0.4629 09:37 1.#QNAN0 0.001885256 1.402341 0.4691 09:44 1.#QNAN0 0.001963521 1.460520 0.4751 09:51 1.#QNAN0 0.002042484 1.519210 0.4809 09:59 1.#QNAN0 0.002121935 1.578265 0.4866 10:06 1.#QNAN0 0.002202283 1.637985 0.4921 10:13 1.#QNAN0 0.002283140 1.698079 0.4975 10:20 1.#QNAN0 0.002364622 1.758635 0.5029 10:27 1.#QNAN0 0.002446999 1.819854 0.5081 10:34 1.#QNAN0 0.002562750 1.905890 0.5151 10:41 1.#QNAN0 0.002646545 1.968150 0.5201 10:49 1.#QNAN0 0.002730860 2.030792 0.5249 10:57 1.#QNAN0 0.002815826 2.093915 0.5296 11:05 1.#QNAN0 0.002901016 2.157208 0.5341 11:12 1.#QNAN0 0.002986679 2.220850 0.5386 11:19 1.#QNAN0 0.003073144 2.285076 0.5430 11:27 1.#QNAN0 0.003159629 2.349323 0.5473 11:34 1.#QNAN0 0.003246811 2.414075 0.5516 11:42 1.#QNAN0 0.003334508 2.479216 0.5557 11:49 1.#QNAN0 0.003423044 2.544976 0.5597 11:56 1.#QNAN0 0.003511451 2.610629 0.5636 12:04 1.#QNAN0 0.003599507 2.676016 0.5675 12:12 1.#QNAN0 0.003689078 2.742535 0.5713 12:19 1.#QNAN0 0.003779082 2.809363 0.5750 12:27 1.#QNAN0 0.003869069 2.876174 0.5786 12:35 1.#QNAN0 0.003960075 2.943750 0.5821 12:42 1.#QNAN0 0.004051125 3.011354 0.5855 12:49 1.#QNAN0 0.004142272 3.079016 0.5889 12:57 1.#QNAN0 0.004234028 3.147138 0.5922 13:04 1.#QNAN0 0.004325941 3.215362 0.5954 13:12 1.#QNAN0 0.004418854 3.284337 0.5986 13:19 1.#QNAN0 0.004535908 3.371263 0.6026 13:25 1.#QNAN0 0.004628380 3.439877 0.6056 13:34 1.#QNAN0 0.004721856 3.509246 0.6086 13:42 1.#QNAN0 0.004814618 3.578094 0.6114 13:49 1.#QNAN0 0.004908192 3.647527 0.6143 13:57 1.#QNAN0 0.005002018 3.717144 0.6171 14:05 1.#QNAN0 0.005096199 3.787021 0.6198 14:13 1.#QNAN0 0.005190689 3.857123 0.6225 14:21 1.#QNAN0 0.005284572 3.926770 0.6251 14:29 1.#QNAN0 0.005379037 3.996845 0.6277 14:37 1.#QNAN0 0.005473919 4.067226 0.6302 14:45 1.#QNAN0 0.005569501 4.138138 0.6326 14:52 1.#QNAN0 0.005664380 4.208493 0.6350 15:01 1.#QNAN0 0.005760164 4.279548 0.6374 15:08 1.#QNAN0 0.005856516 4.351004 0.6397 15:16 1.#QNAN0 0.005951773 4.421643 0.6419 15:24 1.#QNAN0 0.006048565 4.493434 0.6441 15:31 1.#QNAN0 0.006144891 4.564859 0.6463 15:39 1.#QNAN0 0.006241620 4.636596 0.6484 15:46 1.#QNAN0 0.006338182 4.708188 0.6505 15:54 1.#QNAN0 0.006436145 4.780816 0.6525 16:02 1.#QNAN0 0.006533658 4.853124 0.6545 16:09 1.#QNAN0 0.006631641 4.925759 0.6564 16:17 1.#QNAN0 0.006728744 4.997754 0.6583 16:24 1.#QNAN0 0.006826933 5.070552 0.6602 16:31 1.#QNAN0 1.#QNAN0000 1.#QNAN0 1.#QNB 16:34 742.719482 0.007567747 5.620555 0.6765 16:41 1.#QNAN0 0.008319805 6.178933 0.6899 16:48 1.#QNAN0 0.009082474 6.745187 0.7010 16:54 1.#QNAN0 0.009843030 7.309845 0.7122 17:00 1.#QNAN0 0.010616744 7.884374 0.7222 17:02 1.#QNAN0 0.029661027 22.027250 0.8465 17:03 1.#QNAN0 0.050181802 37.266350 0.9285 17:05 1.#QNAN0 0.070433874 52.305870 0.9942 17:06 1.#QNAN0 0.090382843 67.120178 1.0508 17:07 1.#QNAN0 0.110528240 82.080238 1.1008 17:08 1.#QNAN0 0.130568260 96.961533 1.1472 17:10 1.#QNAN0 0.150672720 111.890892 1.1933 17:11 1.#QNAN0 0.170701070 126.763611 1.2375 17:12 1.#QNAN0 0.190718422 141.627472 1.2789 17:14 1.#QNAN0 0.210832191 156.563324 1.3217 17:15 1.#QNAN0 0.230964473 171.512802 1.3596 17:16 1.#QNAN0 0.251721008 186.924973 1.4027 17:18 1.#QNAN0 0.271273457 201.443573 1.4400 17:19 1.#QNAN0 0.291245783 216.273849 1.4805 17:20 1.#QNAN0 0.311273606 231.144287 1.5228 17:22 1.#QNAN0 0.331518027 246.176315 1.5612 17:23 1.#QNAN0 0.352203051 261.535400 1.6050 17:24 1.#QNAN0 0.372806088 276.832367 1.6463 17:26 1.#QNAN0 0.392473247 291.434143 1.6861 17:28 1.#QNAN0 0.412911296 306.609344 1.7298 17:29 1.#QNAN0 0.432717312 321.313812 1.7699 17:31 1.#QNAN0 0.452646682 336.110992 1.8102 17:32 1.#QNAN0 0.472013129 350.488647 1.8519 17:34 1.#QNAN0 0.492973498 366.051086 1.8952 17:35 1.#QNAN0 0.512944707 380.877380 1.9351 17:37 1.#QNAN0 0.533372679 396.044189 1.9772 17:38 1.#QNAN0 0.553581930 411.046814 2.0208 17:40 1.#QNAN0 0.573535451 425.859314 2.0644 17:42 1.#QNAN0 0.593847601 440.939636 2.1078 17:43 1.#QNAN0 0.613524586 455.546387 2.1544 17:45 1.#QNAN0 0.633957363 470.715973 2.2027 17:46 1.#QNAN0 0.653802232 485.446960 2.2549 17:48 1.#QNAN0 0.673998633 500.440735 2.3081 17:49 1.#QNAN0 0.693975056 515.268982 2.3670 17:51 1.#QNAN0 0.714354766 530.396423 2.4305 17:53 1.#QNAN0 0.734326823 545.223145 2.4977 17:54 1.#QNAN0 0.754356831 560.092773 2.5733 17:55 1.#QNAN0 0.774598597 575.119507 2.6570 17:56 1.#QNAN0 0.794686303 590.029358 2.7526 17:58 1.#QNAN0 0.814909568 605.042053 2.8598 17:59 1.#QNAN0 0.834849541 619.841797 2.9854 18:01 1.#QNAN0 0.854972508 634.779724 3.1322 18:02 1.#QNAN0 0.874818270 649.511719 3.3117 18:03 1.#QNAN0 0.895039212 664.519470 3.5279 18:05 1.#QNAN0 0.915109393 679.417786 3.8109 18:06 1.#QNAN0 0.935294088 694.401001 4.2014 18:07 1.#QNAN0 0.955264364 709.222046 4.7648 18:09 1.#QNAN0 0.974701090 723.646729 5.6949 18:11 1.#QNAN0 0.993844613 737.850525 7.8861 18:14 1.#QNAN0 0.979908857 727.498474 7.1796 18:16 1.#QNAN0 0.961575008 713.881409 6.0737 18:18 1.#QNAN0 0.940248967 698.043152 5.2547 18:20 1.#QNAN0 0.918746891 682.077209 4.7157 18:21 1.#QNAN0 0.897808873 666.527466 4.3355 18:23 1.#QNAN0 0.877232099 651.248779 4.0548 18:24 1.#QNAN0 0.856878948 636.136230 3.8318 18:25 1.#QNAN0 0.836441937 620.959045 3.6423 18:27 1.#QNAN0 0.816298601 606.002563 3.4806 18:28 1.#QNAN0 0.796103389 591.007690 3.3395 18:29 1.#QNAN0 0.775858192 575.973511 3.2169 18:31 1.#QNAN0 0.755590388 560.922791 3.1087 18:33 1.#QNAN0 0.735439580 545.961365 3.0115 18:34 1.#QNAN0 1.#QNAN0000 1.#QNAN0 1.#QNB 18:36 742.354614 0.715347153 531.041260 2.9160 18:38 1.#QNAN0 0.713898384 529.965759 2.9046 18:39 1.#QNAN0 0.693483161 514.810425 2.8296 18:41 1.#QNAN0 0.655035075 486.268311 2.7020 18:42 1.#QNAN0 0.634589802 471.090668 2.6363 18:44 1.#QNAN0 0.633481047 470.267578 2.6305 18:46 1.#QNAN0 0.613211803 455.220612 2.5734 18:47 1.#QNAN0 0.593759481 440.780090 2.5207 18:49 1.#QNAN0 0.573509106 425.747131 2.4686 18:51 1.#QNAN0 0.553338566 410.773438 2.4197 18:53 1.#QNAN0 0.533099126 395.748596 2.3686 18:54 1.#QNAN0 0.512138056 380.188049 2.3178 18:55 1.#QNAN0 0.492882688 365.893738 2.2475 18:57 1.#QNAN0 0.472379122 350.672821 2.0554 18:59 1.#QNAN0 0.452119580 335.633057 1.8924 19:01 1.#QNAN0 0.432347429 320.955109 1.8033 19:02 1.#QNAN0 0.411945320 305.809509 1.7430 19:04 1.#QNAN0 0.391803309 290.856995 1.6934 19:05 1.#QNAN0 0.371479966 275.769867 1.6467 19:07 1.#QNAN0 0.351517726 260.950806 1.6020 19:08 1.#QNAN0 0.331397462 246.014435 1.5596 19:09 1.#QNAN0 0.311322603 231.111771 1.5182 19:10 1.#QNAN0 0.291132474 216.123535 1.4743 19:12 1.#QNAN0 0.271105034 201.256073 1.4308 19:13 1.#QNAN0 0.251038767 186.359787 1.3896 19:14 1.#QNAN0 0.231005922 171.488312 1.3472 19:16 1.#QNAN0 0.211026251 156.656311 1.3065 19:17 1.#QNAN0 0.190948370 141.751404 1.2636 19:19 1.#QNAN0 0.170907930 126.874290 1.2210 19:20 1.#QNAN0 0.150700134 111.872940 1.1730 19:22 1.#QNAN0 0.130616190 96.963531 1.1259 19:23 1.#QNAN0 0.110578699 82.088608 1.0792 19:25 1.#QNAN0 0.090506841 67.188171 1.0285 19:27 1.#QNAN0 0.070409984 52.269176 0.9711 19:29 1.#QNAN0 0.050418957 37.428745 0.9078 19:31 1.#QNAN0 0.030562503 22.688215 0.8208 19:32 1.#QNAN0 0.010370981 7.698946 0.6786 19:35 1.#QNAN0 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 Isotherm Linear Plot 000-629 rep 628 Cook 3FB-3-1 - Adsorption Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 5.54983e-006 0.0176961 3.04028e-006 0.0382787 3.40009e-006 0.0579932 5.92287e-006 0.0756076 1.04459e-005 0.0899906 2.04765e-005 0.109323 3.46209e-005 0.127854 6.20882e-005 0.152957 9.45702e-005 0.174883 0.00013408 0.196027 0.000180728 0.216518 0.00021796 0.230591 0.000258139 0.244093 0.000301171 0.257048 0.00034682 0.269499 0.000395225 0.281429 0.000445538 0.292991 0.000498294 0.304093 0.000553132 0.314823 0.000634363 0.329476 0.000715871 0.342936 0.000794827 0.355028 0.000871012 0.365886 0.000943202 0.375539 0.00101195 0.384291 0.00107692 0.392169 0.00113841 0.399255 0.00119609 0.405701 0.00124916 0.411609 0.00129798 0.416769 0.00134383 0.421532 0.00138724 0.42588 0.00142702 0.429786 0.00146327 0.433246 0.00149769 0.436455 0.00152925 0.439332 0.00155766 0.441886 0.001585 0.444252 0.00161023 0.446402 0.00163293 0.448357 0.00165494 0.45021 0.00173106 0.456668 0.00180779 0.462934 0.00188526 0.46908 0.00196352 0.475058 0.00204248 0.480897 0.00212194 0.486551 0.00220228 0.492144 0.00228314 0.497536 0.00236462 0.502853 0.002447 0.508059 0.00256275 0.515143 0.00264655 0.520062 0.00273086 0.524872 0.00281583 0.529603 0.00290102 0.53415 0.00298668 0.538636 0.00307314 0.543029 0.00315963 0.547344 0.00324681 0.551565 0.00333451 0.555652 0.00342304 0.559678 0.00351145 0.563585 0.00359951 0.567463 0.00368908 0.571265 0.00377908 0.574959 0.00386907 0.578561 0.00396008 0.582103 0.00405113 0.585536 0.00414227 0.588904 0.00423403 0.592224 0.00432594 0.595441 0.00441885 0.598612 0.00453591 0.602561 0.00462838 0.605563 0.00472186 0.608583 0.00481462 0.611439 0.00490819 0.614258 0.00500202 0.617077 0.0050962 0.619804 0.00519069 0.622507 0.00528457 0.625081 0.00537904 0.627655 0.00547392 0.63016 0.0055695 0.632638 0.00566438 0.635007 0.00576016 0.637354 0.00585652 0.63965 0.00595177 0.641904 0.00604857 0.644077 0.00614489 0.64625 0.00624162 0.648382 0.00633818 0.650455 0.00643614 0.652489 0.00653366 0.654485 0.00663164 0.656442 0.00672874 0.658322 0.00682693 0.660209 0.00756775 0.676516 0.0083198 0.689865 0.00908247 0.700951 0.00984303 0.71222 0.0106167 0.722203 0.029661 0.846505 0.0501818 0.928525 0.0704339 0.994245 0.0903828 1.05081 0.110528 1.10077 0.130568 1.1472 0.150673 1.19335 0.170701 1.2375 0.190718 1.27891 0.210832 1.32172 0.230964 1.35959 0.251721 1.40268 0.271273 1.44003 0.291246 1.48053 0.311274 1.52279 0.331518 1.5612 0.352203 1.60497 0.372806 1.64626 0.392473 1.68611 0.412911 1.72978 0.432717 1.76985 0.452647 1.81021 0.472013 1.85193 0.492973 1.89521 0.512945 1.93506 0.533373 1.97715 0.553582 2.02084 0.573535 2.06437 0.593848 2.10776 0.613525 2.15436 0.633957 2.20266 0.653802 2.25486 0.673999 2.30813 0.693975 2.36696 0.714355 2.43051 0.734327 2.49766 0.754357 2.57328 0.774599 2.65705 0.794686 2.75258 0.81491 2.85976 0.83485 2.98545 0.854973 3.13223 0.874818 3.31168 0.895039 3.52788 0.915109 3.81089 0.935294 4.20145 0.955264 4.76479 0.974701 5.69488 0.993845 7.88613 000-629 rep 628 Cook 3FB-3-1 - Desorption Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 0.993845 7.88613 0.979909 7.1796 0.961575 6.07369 0.940249 5.25471 0.918747 4.71568 0.897809 4.33548 0.877232 4.05483 0.856879 3.83177 0.836442 3.64233 0.816299 3.48062 0.796103 3.33949 0.775858 3.21692 0.75559 3.10871 0.73544 3.01154 0.715347 2.91601 0.713898 2.90458 0.693483 2.8296 0.655035 2.70199 0.63459 2.63634 0.633481 2.63048 0.613212 2.57344 0.593759 2.5207 0.573509 2.46857 0.553339 2.41967 0.533099 2.36858 0.512138 2.31778 0.492883 2.24747 0.472379 2.05541 0.45212 1.89242 0.432347 1.8033 0.411945 1.74299 0.391803 1.69341 0.37148 1.64671 0.351518 1.60202 0.331397 1.55963 0.311323 1.51819 0.291132 1.47426 0.271105 1.43078 0.251039 1.38963 0.231006 1.34717 0.211026 1.30652 0.190948 1.26356 0.170908 1.22099 0.1507 1.17299 0.130616 1.1259 0.110579 1.07917 0.0905068 1.02854 0.07041 0.971085 0.050419 0.907798 0.0305625 0.820817 0.010371 0.678582 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 Isotherm Log Plot 000-629 rep 628 Cook 3FB-3-1 - Adsorption Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 5.54983e-006 0.0176961 3.04028e-006 0.0382787 3.40009e-006 0.0579932 5.92287e-006 0.0756076 1.04459e-005 0.0899906 2.04765e-005 0.109323 3.46209e-005 0.127854 6.20882e-005 0.152957 9.45702e-005 0.174883 0.00013408 0.196027 0.000180728 0.216518 0.00021796 0.230591 0.000258139 0.244093 0.000301171 0.257048 0.00034682 0.269499 0.000395225 0.281429 0.000445538 0.292991 0.000498294 0.304093 0.000553132 0.314823 0.000634363 0.329476 0.000715871 0.342936 0.000794827 0.355028 0.000871012 0.365886 0.000943202 0.375539 0.00101195 0.384291 0.00107692 0.392169 0.00113841 0.399255 0.00119609 0.405701 0.00124916 0.411609 0.00129798 0.416769 0.00134383 0.421532 0.00138724 0.42588 0.00142702 0.429786 0.00146327 0.433246 0.00149769 0.436455 0.00152925 0.439332 0.00155766 0.441886 0.001585 0.444252 0.00161023 0.446402 0.00163293 0.448357 0.00165494 0.45021 0.00173106 0.456668 0.00180779 0.462934 0.00188526 0.46908 0.00196352 0.475058 0.00204248 0.480897 0.00212194 0.486551 0.00220228 0.492144 0.00228314 0.497536 0.00236462 0.502853 0.002447 0.508059 0.00256275 0.515143 0.00264655 0.520062 0.00273086 0.524872 0.00281583 0.529603 0.00290102 0.53415 0.00298668 0.538636 0.00307314 0.543029 0.00315963 0.547344 0.00324681 0.551565 0.00333451 0.555652 0.00342304 0.559678 0.00351145 0.563585 0.00359951 0.567463 0.00368908 0.571265 0.00377908 0.574959 0.00386907 0.578561 0.00396008 0.582103 0.00405113 0.585536 0.00414227 0.588904 0.00423403 0.592224 0.00432594 0.595441 0.00441885 0.598612 0.00453591 0.602561 0.00462838 0.605563 0.00472186 0.608583 0.00481462 0.611439 0.00490819 0.614258 0.00500202 0.617077 0.0050962 0.619804 0.00519069 0.622507 0.00528457 0.625081 0.00537904 0.627655 0.00547392 0.63016 0.0055695 0.632638 0.00566438 0.635007 0.00576016 0.637354 0.00585652 0.63965 0.00595177 0.641904 0.00604857 0.644077 0.00614489 0.64625 0.00624162 0.648382 0.00633818 0.650455 0.00643614 0.652489 0.00653366 0.654485 0.00663164 0.656442 0.00672874 0.658322 0.00682693 0.660209 0.00756775 0.676516 0.0083198 0.689865 0.00908247 0.700951 0.00984303 0.71222 0.0106167 0.722203 0.029661 0.846505 0.0501818 0.928525 0.0704339 0.994245 0.0903828 1.05081 0.110528 1.10077 0.130568 1.1472 0.150673 1.19335 0.170701 1.2375 0.190718 1.27891 0.210832 1.32172 0.230964 1.35959 0.251721 1.40268 0.271273 1.44003 0.291246 1.48053 0.311274 1.52279 0.331518 1.5612 0.352203 1.60497 0.372806 1.64626 0.392473 1.68611 0.412911 1.72978 0.432717 1.76985 0.452647 1.81021 0.472013 1.85193 0.492973 1.89521 0.512945 1.93506 0.533373 1.97715 0.553582 2.02084 0.573535 2.06437 0.593848 2.10776 0.613525 2.15436 0.633957 2.20266 0.653802 2.25486 0.673999 2.30813 0.693975 2.36696 0.714355 2.43051 0.734327 2.49766 0.754357 2.57328 0.774599 2.65705 0.794686 2.75258 0.81491 2.85976 0.83485 2.98545 0.854973 3.13223 0.874818 3.31168 0.895039 3.52788 0.915109 3.81089 0.935294 4.20145 0.955264 4.76479 0.974701 5.69488 0.993845 7.88613 000-629 rep 628 Cook 3FB-3-1 - Desorption Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 0.993845 7.88613 0.979909 7.1796 0.961575 6.07369 0.940249 5.25471 0.918747 4.71568 0.897809 4.33548 0.877232 4.05483 0.856879 3.83177 0.836442 3.64233 0.816299 3.48062 0.796103 3.33949 0.775858 3.21692 0.75559 3.10871 0.73544 3.01154 0.715347 2.91601 0.713898 2.90458 0.693483 2.8296 0.655035 2.70199 0.63459 2.63634 0.633481 2.63048 0.613212 2.57344 0.593759 2.5207 0.573509 2.46857 0.553339 2.41967 0.533099 2.36858 0.512138 2.31778 0.492883 2.24747 0.472379 2.05541 0.45212 1.89242 0.432347 1.8033 0.411945 1.74299 0.391803 1.69341 0.37148 1.64671 0.351518 1.60202 0.331397 1.55963 0.311323 1.51819 0.291132 1.47426 0.271105 1.43078 0.251039 1.38963 0.231006 1.34717 0.211026 1.30652 0.190948 1.26356 0.170908 1.22099 0.1507 1.17299 0.130616 1.1259 0.110579 1.07917 0.0905068 1.02854 0.07041 0.971085 0.050419 0.907798 0.0305625 0.820817 0.010371 0.678582 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 BET Surface Area Report BET Surface Area: 4.7358 ± 0.0144 m²/g Slope: 0.907253 ± 0.002756 g/cm³ STP Y-Intercept: 0.011949 ± 0.000514 g/cm³ STP C: 76.929684 Qm: 1.0879 cm³/g STP Correlation Coefficient: 0.9999492 Molecular Cross-Sectional Area: 0.1620 nm² Quantity Relative Adsorbed Pressure (cm³/g 1/[Q(Po/P (P/Po) STP) - 1)] --- 0.050181802 0.9285 0.056900 0.070433874 0.9942 0.076209 0.090382843 1.0508 0.094559 0.110528240 1.1008 0.112887 0.130568260 1.1472 0.130907 0.150672720 1.1933 0.148660 0.170701070 1.2375 0.166333 0.190718422 1.2789 0.184270 0.210832191 1.3217 0.202128 0.230964473 1.3596 0.220897 0.251721008 1.4027 0.239827 0.271273457 1.4400 0.258507 0.291245783 1.4805 0.277554 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 BET Surface Area Plot 000-629 rep 628 Cook 3FB-3-1 Relative Pressure (P/Po) 1/[Q(Po/P - 1)] 0.0501818 0.0569 0.0704339 0.0762093 0.0903828 0.0945592 0.110528 0.112887 0.130568 0.130907 0.150673 0.14866 0.170701 0.166333 0.190718 0.18427 0.210832 0.202128 0.230964 0.220897 0.251721 0.239827 0.271273 0.258507 0.291246 0.277554 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 t-Plot Report Micropore Volume: -0.000291 cm³/g Micropore Area: * External Surface Area: 5.3333 m²/g Slope: 0.344798 ± 0.003166 cm³/g·Å STP Y-Intercept: -0.188406 ± 0.009506 cm³/g STP Correlation Coefficient: 0.999874 Surface Area Correction Factor: 1.000 Density Conversion Factor: 0.0015468 Total Surface Area (BET): 4.7358 m²/g Thickness Range: 2.6000 Å to 3.5000 Å Thickness Equation: Harkins and Jura t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 Quantity Relative Statistical Adsorbed Pressure Thickness (cm³/g (P/Po) (Å) STP) --- 0.000005550 1.6263 0.0177 0.000003040 1.5875 0.0383 0.000003400 1.5945 0.0580 0.000005923 1.6306 0.0756 0.000010446 1.6702 0.0900 0.000020477 1.7211 0.1093 0.000034621 1.7643 0.1279 0.000062088 1.8162 0.1530 0.000094570 1.8567 0.1749 0.000134080 1.8924 0.1960 0.000180728 1.9246 0.2165 0.000217960 1.9457 0.2306 0.000258139 1.9653 0.2441 0.000301171 1.9837 0.2570 0.000346820 2.0010 0.2695 0.000395225 2.0175 0.2814 0.000445538 2.0329 0.2930 0.000498294 2.0477 0.3041 0.000553132 2.0617 0.3148 0.000634363 2.0806 0.3295 0.000715871 2.0977 0.3429 0.000794827 2.1129 0.3550 0.000871012 2.1264 0.3659 0.000943202 2.1384 0.3755 0.001011955 2.1492 0.3843 0.001076923 2.1588 0.3922 0.001138415 2.1675 0.3993 0.001196086 2.1754 0.4057 0.001249156 2.1824 0.4116 0.001297980 2.1886 0.4168 0.001343826 2.1943 0.4215 0.001387241 2.1995 0.4259 0.001427016 2.2042 0.4298 0.001463273 2.2084 0.4332 0.001497694 2.2122 0.4365 0.001529246 2.2158 0.4393 0.001557662 2.2189 0.4419 0.001585002 2.2218 0.4443 0.001610228 2.2245 0.4464 0.001632930 2.2269 0.4484 0.001654942 2.2292 0.4502 0.001731062 2.2370 0.4567 0.001807790 2.2446 0.4629 0.001885256 2.2520 0.4691 0.001963521 2.2592 0.4751 0.002042484 2.2663 0.4809 0.002121935 2.2732 0.4866 0.002202283 2.2800 0.4921 0.002283140 2.2867 0.4975 0.002364622 2.2932 0.5029 0.002446999 2.2997 0.5081 0.002562750 2.3084 0.5151 0.002646545 2.3146 0.5201 0.002730860 2.3207 0.5249 0.002815826 2.3266 0.5296 0.002901016 2.3325 0.5341 0.002986679 2.3382 0.5386 0.003073144 2.3439 0.5430 0.003159629 2.3495 0.5473 0.003246811 2.3550 0.5516 0.003334508 2.3604 0.5557 0.003423044 2.3658 0.5597 0.003511451 2.3710 0.5636 0.003599507 2.3762 0.5675 0.003689078 2.3813 0.5713 0.003779082 2.3864 0.5750 0.003869069 2.3914 0.5786 0.003960075 2.3963 0.5821 0.004051125 2.4012 0.5855 0.004142272 2.4060 0.5889 0.004234028 2.4107 0.5922 0.004325941 2.4154 0.5954 0.004418854 2.4201 0.5986 0.004535908 2.4258 0.6026 0.004628380 2.4303 0.6056 0.004721856 2.4348 0.6086 0.004814618 2.4392 0.6114 0.004908192 2.4435 0.6143 0.005002018 2.4478 0.6171 0.005096199 2.4521 0.6198 0.005190689 2.4563 0.6225 0.005284572 2.4604 0.6251 0.005379037 2.4645 0.6277 0.005473919 2.4686 0.6302 0.005569501 2.4727 0.6326 0.005664380 2.4766 0.6350 0.005760164 2.4806 0.6374 0.005856516 2.4845 0.6397 0.005951773 2.4884 0.6419 0.006048565 2.4922 0.6441 0.006144891 2.4961 0.6463 0.006241620 2.4998 0.6484 0.006338182 2.5036 0.6505 0.006436145 2.5073 0.6525 0.006533658 2.5110 0.6545 0.006631641 2.5147 0.6564 0.006728744 2.5183 0.6583 0.006826933 2.5219 0.6602 0.007567747 2.5479 0.6765 0.008319805 2.5726 0.6899 0.009082474 2.5961 0.7010 0.009843030 2.6182 0.7122 0.010616744 2.6395 0.7222 0.029661027 2.9929 0.8465 0.050181802 3.2391 0.9285 0.070433874 3.4342 0.9942 0.090382843 3.6026 1.0508 0.110528240 3.7582 1.1008 0.130568260 3.9035 1.1472 0.150672720 4.0428 1.1933 0.170701070 4.1772 1.2375 0.190718422 4.3086 1.2789 0.210832191 4.4387 1.3217 0.230964473 4.5680 1.3596 0.251721008 4.7009 1.4027 0.271273457 4.8264 1.4400 0.291245783 4.9553 1.4805 0.311273606 5.0859 1.5228 0.331518027 5.2197 1.5612 0.352203051 5.3586 1.6050 0.372806088 5.4998 1.6463 0.392473247 5.6375 1.6861 0.412911296 5.7842 1.7298 0.432717312 5.9303 1.7699 0.452646682 6.0817 1.8102 0.472013129 6.2335 1.8519 0.492973498 6.4035 1.8952 0.512944707 6.5718 1.9351 0.533372679 6.7509 1.9772 0.553581930 6.9358 2.0208 0.573535451 7.1268 2.0644 0.593847601 7.3308 2.1078 * The micropore area is not reported because either the micropore volume is negative or the calculated external surface area is larger than the total surface area. ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 t-Plot Harkins and Jura 000-629 rep 628 Cook 3FB-3-1 Thickness (Å) Quantity Adsorbed (cm³/g STP) 2.61819 0.71222 2.63953 0.722203 2.99291 0.846505 3.23907 0.928525 3.43421 0.994245 Not Fitted Points Thickness (Å) Quantity Adsorbed (cm³/g STP) 1.62627 0.0176961 1.58752 0.0382787 1.59451 0.0579932 1.63063 0.0756076 1.67021 0.0899906 1.72112 0.109323 1.76425 0.127854 1.81625 0.152957 1.85669 0.174883 1.89238 0.196027 1.92458 0.216518 1.94565 0.230591 1.96529 0.244093 1.98371 0.257048 2.00103 0.269499 2.01748 0.281429 2.03293 0.292991 2.04768 0.304093 2.06174 0.314823 2.08063 0.329476 2.09774 0.342936 2.1129 0.355028 2.12643 0.365886 2.13841 0.375539 2.14917 0.384291 2.15882 0.392169 2.16755 0.399255 2.1754 0.405701 2.18237 0.411609 2.18858 0.416769 2.19425 0.421532 2.19949 0.42588 2.20417 0.429786 2.20835 0.433246 2.21225 0.436455 2.21576 0.439332 2.21888 0.441886 2.22183 0.444252 2.22453 0.446402 2.22692 0.448357 2.22922 0.45021 2.23699 0.456668 2.24457 0.462934 2.25197 0.46908 2.25921 0.475058 2.2663 0.480897 2.27323 0.486551 2.28004 0.492144 2.2867 0.497536 2.29324 0.502853 2.29967 0.508059 2.30845 0.515143 2.31461 0.520062 2.32067 0.524872 2.32664 0.529603 2.33249 0.53415 2.33824 0.538636 2.34393 0.543029 2.34949 0.547344 2.35499 0.551565 2.36041 0.555652 2.36578 0.559678 2.37104 0.563585 2.37618 0.567463 2.38132 0.571265 2.38638 0.574959 2.39136 0.578561 2.39631 0.582103 2.40118 0.585536 2.40598 0.588904 2.41073 0.592224 2.41541 0.595441 2.42008 0.598612 2.42585 0.602561 2.43033 0.605563 2.4348 0.608583 2.43917 0.611439 2.44352 0.614258 2.44782 0.617077 2.45207 0.619804 2.45629 0.622507 2.46042 0.625081 2.46453 0.627655 2.4686 0.63016 2.47265 0.632638 2.47663 0.635007 2.48059 0.637354 2.48453 0.63965 2.48838 0.641904 2.49225 0.644077 2.49605 0.64625 2.49983 0.648382 2.50356 0.650455 2.50731 0.652489 2.51099 0.654485 2.51466 0.656442 2.51825 0.658322 2.52185 0.660209 2.5479 0.676516 2.57257 0.689865 2.59607 0.700951 3.60261 1.05081 3.75816 1.10077 3.90345 1.1472 4.04279 1.19335 4.1772 1.2375 4.3086 1.27891 4.43875 1.32172 4.56798 1.35959 4.70088 1.40268 4.82635 1.44003 4.9553 1.48053 5.08589 1.52279 5.21965 1.5612 5.35861 1.60497 5.49978 1.64626 5.63753 1.68611 5.78424 1.72978 5.93033 1.76985 6.0817 1.81021 6.23347 1.85193 6.40353 1.89521 6.57179 1.93506 6.7509 1.97715 6.93583 2.02084 7.12682 2.06437 7.33079 2.10776 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 BJH Adsorption Pore Distribution Report Faas Correction Halsey t = 3.54 [ -5 / ln(P/Po) ] ^ 0.333 Width Range: 17.000 Å to 3000.000 Å Adsorbate Property Factor: 9.53000 Å Density Conversion Factor: 0.0015468 Fraction of Pores Open at Both Ends: 0.00 Incremental Cumulative Cumulative Average Pore Pore Incremental Pore Width Volume Volume Pore Area Area Pore Width Range (Å) (Å) (cm³/g) (cm³/g) (m²/g) (m²/g) ------ 3147.5 - 779.5 910.3 0.003672 0.003672 0.161 0.161 779.5 - 445.0 525.1 0.001546 0.005218 0.118 0.279 445.0 - 309.4 352.7 0.000944 0.006162 0.107 0.386 309.4 - 236.7 263.1 0.000660 0.006821 0.100 0.486 236.7 - 191.8 209.3 0.000479 0.007301 0.092 0.578 191.8 - 160.9 173.5 0.000366 0.007667 0.084 0.662 160.9 - 138.8 148.1 0.000306 0.007973 0.083 0.745 138.8 - 121.7 129.1 0.000249 0.008222 0.077 0.822 121.7 - 108.3 114.2 0.000214 0.008436 0.075 0.897 108.3 - 97.4 102.2 0.000181 0.008616 0.071 0.968 97.4 - 88.4 92.4 0.000161 0.008778 0.070 1.038 88.4 - 80.8 84.2 0.000140 0.008918 0.067 1.104 80.8 - 74.3 77.3 0.000127 0.009045 0.066 1.170 74.3 - 68.8 71.3 0.000111 0.009156 0.062 1.232 68.8 - 63.8 66.1 0.000105 0.009261 0.064 1.296 63.8 - 59.5 61.5 0.000098 0.009359 0.064 1.359 59.5 - 55.6 57.4 0.000087 0.009445 0.060 1.420 55.6 - 52.2 53.8 0.000087 0.009532 0.065 1.484 52.2 - 49.1 50.6 0.000078 0.009611 0.062 1.546 49.1 - 46.3 47.6 0.000077 0.009688 0.065 1.611 46.3 - 43.7 44.9 0.000070 0.009758 0.062 1.674 43.7 - 41.4 42.5 0.000072 0.009830 0.068 1.742 41.4 - 39.2 40.2 0.000073 0.009903 0.073 1.815 39.2 - 37.1 38.1 0.000070 0.009973 0.073 1.888 37.1 - 35.2 36.1 0.000066 0.010039 0.073 1.961 35.2 - 33.4 34.3 0.000074 0.010113 0.086 2.047 33.4 - 31.8 32.6 0.000073 0.010186 0.090 2.137 31.8 - 30.3 31.0 0.000069 0.010255 0.089 2.226 30.3 - 28.9 29.5 0.000069 0.010324 0.093 2.320 28.9 - 27.5 28.1 0.000078 0.010402 0.111 2.430 27.5 - 26.2 26.8 0.000069 0.010471 0.103 2.533 26.2 - 24.9 25.5 0.000071 0.010541 0.111 2.644 24.9 - 23.7 24.3 0.000077 0.010618 0.127 2.771 23.7 - 22.5 23.1 0.000062 0.010681 0.108 2.879 22.5 - 21.4 22.0 0.000073 0.010754 0.134 3.012 21.4 - 20.4 20.9 0.000067 0.010821 0.129 3.141 20.4 - 19.4 19.9 0.000058 0.010879 0.116 3.256 19.4 - 18.4 18.9 0.000070 0.010948 0.148 3.405 18.4 - 17.4 17.9 0.000053 0.011002 0.120 3.525 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 BJH Adsorption dV/dw Pore Volume Halsey : Faas Correction 000-629 rep 628 Cook 3FB-3-1 Pore Width (Å) Pore Volume (cm³/g·Å) 910.333 1.55059e-006 525.075 4.62061e-006 352.745 6.96498e-006 263.098 9.06636e-006 209.32 1.06766e-005 173.476 1.1847e-005 148.106 1.38677e-005 129.051 1.4579e-005 114.198 1.60105e-005 102.245 1.64809e-005 92.4245 1.79433e-005 84.2109 1.83799e-005 77.2569 1.96429e-005 71.3088 1.99787e-005 66.0799 2.12003e-005 61.4934 2.27933e-005 57.4386 2.24521e-005 53.8295 2.55496e-005 50.5549 2.47688e-005 47.6096 2.79655e-005 44.926 2.67173e-005 42.4564 3.06802e-005 40.1873 3.3368e-005 38.0666 3.40063e-005 36.1137 3.52859e-005 34.2666 4.04211e-005 32.5744 4.64611e-005 31.0194 4.51284e-005 29.5392 4.80001e-005 28.1205 5.54566e-005 26.7843 5.36885e-005 25.5042 5.52753e-005 24.2554 6.30981e-005 23.0733 5.41892e-005 21.9563 6.72045e-005 20.887 6.39406e-005 19.8657 5.77718e-005 18.8504 6.7923e-005 17.8509 5.49056e-005 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 BJH Adsorption dV/dw Pore Volume Halsey : Faas Correction 000-629 rep 628 Cook 3FB-3-1 Pore Width (Å) Pore Volume (cm³/g·Å) 910.333 1.55059e-006 525.075 4.62061e-006 352.745 6.96498e-006 263.098 9.06636e-006 209.32 1.06766e-005 173.476 1.1847e-005 148.106 1.38677e-005 129.051 1.4579e-005 114.198 1.60105e-005 102.245 1.64809e-005 92.4245 1.79433e-005 84.2109 1.83799e-005 77.2569 1.96429e-005 71.3088 1.99787e-005 66.0799 2.12003e-005 61.4934 2.27933e-005 57.4386 2.24521e-005 53.8295 2.55496e-005 50.5549 2.47688e-005 47.6096 2.79655e-005 44.926 2.67173e-005 42.4564 3.06802e-005 40.1873 3.3368e-005 38.0666 3.40063e-005 36.1137 3.52859e-005 34.2666 4.04211e-005 32.5744 4.64611e-005 31.0194 4.51284e-005 29.5392 4.80001e-005 28.1205 5.54566e-005 26.7843 5.36885e-005 25.5042 5.52753e-005 24.2554 6.30981e-005 23.0733 5.41892e-005 21.9563 6.72045e-005 20.887 6.39406e-005 19.8657 5.77718e-005 18.8504 6.7923e-005 17.8509 5.49056e-005 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 BJH Adsorption dV/dlog(w) Pore Volume Halsey : Faas Correction 000-629 rep 628 Cook 3FB-3-1 Pore Width (Å) dV/dlog(w) Pore Volume (cm³/g·Å) 910.333 0.00605764 525.075 0.00634835 352.745 0.00598342 263.098 0.00566615 209.32 0.00524687 173.476 0.0047973 148.106 0.00477545 129.051 0.0043658 114.198 0.00423564 102.245 0.00390007 92.4245 0.00383492 84.2109 0.00357714 77.2569 0.00350532 71.3088 0.00328949 66.0799 0.00323403 61.4934 0.00323457 57.4386 0.00297561 53.8295 0.00317262 50.5549 0.00288846 47.6096 0.00307049 44.926 0.0027681 42.4564 0.00300353 40.1873 0.00309196 38.0666 0.00298471 36.1137 0.00293782 34.2666 0.00319348 32.5744 0.00348862 31.0194 0.00322691 29.5392 0.00326836 28.1205 0.00359492 26.7843 0.00331462 25.5042 0.00324982 24.2554 0.00352815 23.0733 0.00288222 21.9563 0.00340144 20.887 0.00307869 19.8657 0.00264563 18.8504 0.00295213 17.8509 0.00225981 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 BJH Adsorption Cumulative Pore Area Halsey : Faas Correction 000-629 rep 628 Cook 3FB-3-1 Pore Width (Å) Pore Area (m²/g) 779.521 0.161337 444.955 0.279102 309.414 0.386153 236.669 0.486426 191.759 0.578052 160.868 0.662438 138.782 0.745158 121.698 0.822356 108.349 0.897215 97.39 0.967876 88.3937 1.03774 80.7678 1.10432 74.3236 1.16985 68.7614 1.23219 63.8005 1.29585 59.5101 1.35946 55.6484 1.41984 52.2443 1.48447 49.0807 1.54647 46.3134 1.61149 43.7036 1.67357 41.3512 1.74157 39.1543 1.81453 37.0997 1.88795 35.2329 1.96091 33.4064 2.04709 31.826 2.13726 30.2951 2.22635 28.8594 2.31967 27.4577 2.43024 26.1774 2.53289 24.9004 2.6436 23.6773 2.77087 22.5308 2.87857 21.4402 3.0121 20.3905 3.14064 19.3945 3.2565 18.3662 3.40471 17.3922 3.52454 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 BJH Adsorption dA/dw Pore Area Halsey : Faas Correction 000-629 rep 628 Cook 3FB-3-1 Pore Width (Å) Pore Area (m²/g·Å) 910.333 6.8133e-005 525.075 0.000351996 352.745 0.000789804 263.098 0.0013784 209.32 0.00204025 173.476 0.00273168 148.106 0.00374533 129.051 0.00451883 114.198 0.00560797 102.245 0.00644759 92.4245 0.00776562 84.2109 0.00873042 77.2569 0.0101702 71.3088 0.0112069 66.0799 0.0128332 61.4934 0.0148265 57.4386 0.0156355 53.8295 0.0189856 50.5549 0.0195975 47.6096 0.0234957 44.926 0.0237879 42.4564 0.0289051 40.1873 0.0332125 38.0666 0.0357334 36.1137 0.0390831 34.2666 0.0471843 32.5744 0.0570522 31.0194 0.0581937 29.5392 0.0649984 28.1205 0.0788841 26.7843 0.080179 25.5042 0.086692 24.2554 0.104056 23.0733 0.0939429 21.9563 0.122433 20.887 0.122451 19.8657 0.116325 18.8504 0.144131 17.8509 0.123032 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 BJH Adsorption dA/dlog(w) Pore Area Halsey : Faas Correction 000-629 rep 628 Cook 3FB-3-1 Pore Width (Å) dA/dlog(w) Pore Area (m²/g·Å) 910.333 0.266172 525.075 0.483614 352.745 0.678499 263.098 0.861452 209.32 1.00265 173.476 1.10616 148.106 1.28974 129.051 1.3532 114.198 1.48361 102.245 1.52577 92.4245 1.6597 84.2109 1.69913 77.2569 1.81489 71.3088 1.84521 66.0799 1.95765 61.4934 2.10402 57.4386 2.0722 53.8295 2.35753 50.5549 2.2854 47.6096 2.57973 44.926 2.46459 42.4564 2.82975 40.1873 3.07755 38.0666 3.13631 36.1137 3.25396 34.2666 3.72781 32.5744 4.28388 31.0194 4.16115 29.5392 4.42579 28.1205 5.11359 26.7843 4.95009 25.5042 5.09691 24.2554 5.81833 23.0733 4.99665 21.9563 6.19673 20.887 5.89592 19.8657 5.32704 18.8504 6.26434 17.8509 5.06376 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 BJH Desorption Pore Distribution Report Faas Correction Halsey t = 3.54 [ -5 / ln(P/Po) ] ^ 0.333 Width Range: 17.000 Å to 3000.000 Å Adsorbate Property Factor: 9.53000 Å Density Conversion Factor: 0.0015468 Fraction of Pores Open at Both Ends: 0.00 Incremental Cumulative Cumulative Average Pore Pore Incremental Pore Width Volume Volume Pore Area Area Pore Width Range (Å) (Å) (cm³/g) (cm³/g) (m²/g) (m²/g) ------ 3149.1 - 979.8 1164.4 0.001173 0.001173 0.040 0.040 979.8 - 518.4 616.3 0.001884 0.003057 0.122 0.163 518.4 - 336.3 388.9 0.001418 0.004475 0.146 0.308 336.3 - 248.8 279.1 0.000943 0.005418 0.135 0.444 248.8 - 198.6 217.8 0.000671 0.006089 0.123 0.567 198.6 - 165.7 179.0 0.000497 0.006587 0.111 0.678 165.7 - 142.3 152.1 0.000397 0.006984 0.105 0.782 142.3 - 124.6 132.2 0.000340 0.007324 0.103 0.885 124.6 - 110.8 116.8 0.000292 0.007616 0.100 0.985 110.8 - 99.7 104.7 0.000256 0.007871 0.098 1.083 99.7 - 90.6 94.7 0.000222 0.008093 0.094 1.177 90.6 - 82.8 86.3 0.000195 0.008288 0.090 1.267 82.8 - 76.3 79.3 0.000176 0.008464 0.089 1.356 76.3 - 70.7 73.3 0.000177 0.008640 0.096 1.452 70.7 - 70.3 70.5 0.000024 0.008664 0.013 1.466 70.3 - 65.3 67.6 0.000131 0.008795 0.078 1.543 65.3 - 57.5 60.9 0.000224 0.009019 0.147 1.690 57.5 - 54.0 55.6 0.000118 0.009138 0.085 1.775 54.0 - 53.8 53.9 0.000012 0.009150 0.009 1.785 53.8 - 50.7 52.1 0.000099 0.009249 0.076 1.861 50.7 - 48.0 49.2 0.000093 0.009342 0.075 1.936 48.0 - 45.4 46.6 0.000091 0.009433 0.078 2.014 45.4 - 43.0 44.1 0.000085 0.009518 0.077 2.091 43.0 - 40.8 41.8 0.000093 0.009611 0.089 2.180 40.8 - 38.7 39.7 0.000092 0.009703 0.093 2.273 38.7 - 36.9 37.7 0.000153 0.009856 0.163 2.435 36.9 - 35.1 35.9 0.000504 0.010360 0.561 2.997 35.1 - 33.4 34.2 0.000419 0.010780 0.490 3.487 33.4 - 31.9 32.6 0.000200 0.010980 0.245 3.732 31.9 - 30.4 31.1 0.000111 0.011091 0.143 3.875 30.4 - 29.1 29.7 0.000080 0.011170 0.107 3.982 29.1 - 27.7 28.4 0.000071 0.011241 0.100 4.082 27.7 - 26.5 27.1 0.000066 0.011308 0.098 4.180 26.5 - 25.3 25.9 0.000059 0.011366 0.091 4.271 25.3 - 24.2 24.7 0.000056 0.011422 0.091 4.361 24.2 - 23.1 23.6 0.000064 0.011486 0.108 4.469 23.1 - 22.0 22.5 0.000062 0.011549 0.111 4.580 22.0 - 21.0 21.5 0.000053 0.011602 0.099 4.679 21.0 - 20.0 20.5 0.000057 0.011658 0.111 4.790 20.0 - 19.1 19.5 0.000048 0.011707 0.099 4.889 19.1 - 18.1 18.5 0.000054 0.011760 0.116 5.004 18.1 - 17.2 17.6 0.000049 0.011809 0.110 5.115 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 BJH Desorption Cumulative Pore Volume Halsey : Faas Correction BJH Desorption Cumulative Pore Volume Pore Width (Å) Pore Volume (cm³/g) 979.774 0.00117339 518.383 0.00305719 336.328 0.00447502 248.793 0.00541811 198.575 0.00608926 165.681 0.0065867 142.294 0.00698405 124.551 0.00732385 110.839 0.00761576 99.7401 0.00787128 90.5629 0.00809283 82.8486 0.00828812 76.3079 0.0084637 70.6711 0.00864031 70.2938 0.00866404 65.3394 0.00879512 57.5228 0.00901933 53.9983 0.0091375 53.8177 0.00914989 50.6856 0.00924927 47.9525 0.00934183 45.3513 0.00943311 42.9746 0.00951799 40.7766 0.00961071 38.6726 0.00970267 36.8756 0.00985606 35.0881 0.0103602 33.4352 0.0107797 31.9184 0.0109798 30.4422 0.0110908 29.0639 0.0111704 27.7442 0.0112412 26.5099 0.0113076 25.3212 0.0113663 24.1844 0.0114223 23.0851 0.0114861 22.0326 0.0115485 21.0111 0.0116017 20.0191 0.0116583 19.0524 0.0117066 18.0982 0.0117603 17.1573 0.0118088 BJH Desorption dV/dw Pore Volume Pore Width (Å) Pore Volume (cm³/g·Å) 1164.41 5.40889e-007 616.338 4.08287e-006 388.918 7.78795e-006 279.137 1.07739e-005 217.797 1.33645e-005 178.989 1.51228e-005 152.094 1.69899e-005 132.156 1.91514e-005 116.832 2.12876e-005 104.654 2.30232e-005 94.6684 2.41412e-005 86.3294 2.53158e-005 79.2823 2.6844e-005 73.2505 3.13312e-005 70.4813 6.29153e-005 67.6157 2.64557e-005 60.8785 2.86848e-005 55.6357 3.35281e-005 53.9077 6.85883e-005 52.1461 3.17293e-005 49.2336 3.38651e-005 46.5699 3.50909e-005 44.0904 3.57137e-005 41.8101 4.2186e-005 39.6612 4.37052e-005 37.7253 8.53569e-005 35.9311 0.000282032 34.2159 0.000253786 32.6364 0.000131965 31.1401 7.51591e-005 29.7163 5.77992e-005 28.3686 5.36405e-005 27.0945 5.37809e-005 25.8839 4.93989e-005 24.7225 4.92411e-005 23.605 5.80204e-005 22.5303 5.93135e-005 21.4937 5.20298e-005 20.4872 5.71105e-005 19.5079 4.99224e-005 18.5467 5.62434e-005 17.5985 5.16358e-005 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 BJH Desorption dV/dw Pore Volume Halsey : Faas Correction 000-629 rep 628 Cook 3FB-3-1 Pore Width (Å) Pore Volume (cm³/g·Å) 1164.41 5.40889e-007 616.338 4.08287e-006 388.918 7.78795e-006 279.137 1.07739e-005 217.797 1.33645e-005 178.989 1.51228e-005 152.094 1.69899e-005 132.156 1.91514e-005 116.832 2.12876e-005 104.654 2.30232e-005 94.6684 2.41412e-005 86.3294 2.53158e-005 79.2823 2.6844e-005 73.2505 3.13312e-005 70.4813 6.29153e-005 67.6157 2.64557e-005 60.8785 2.86848e-005 55.6357 3.35281e-005 53.9077 6.85883e-005 52.1461 3.17293e-005 49.2336 3.38651e-005 46.5699 3.50909e-005 44.0904 3.57137e-005 41.8101 4.2186e-005 39.6612 4.37052e-005 37.7253 8.53569e-005 35.9311 0.000282032 34.2159 0.000253786 32.6364 0.000131965 31.1401 7.51591e-005 29.7163 5.77992e-005 28.3686 5.36405e-005 27.0945 5.37809e-005 25.8839 4.93989e-005 24.7225 4.92411e-005 23.605 5.80204e-005 22.5303 5.93135e-005 21.4937 5.20298e-005 20.4872 5.71105e-005 19.5079 4.99224e-005 18.5467 5.62434e-005 17.5985 5.16358e-005 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 BJH Desorption dV/dlog(w) Pore Volume Halsey : Faas Correction 000-629 rep 628 Cook 3FB-3-1 Pore Width (Å) dV/dlog(w) Pore Volume (cm³/g·Å) 1164.41 0.00231407 616.338 0.00681364 388.918 0.00754618 279.137 0.00720334 217.797 0.00685441 178.989 0.00632472 152.094 0.00601249 132.156 0.00587496 116.832 0.00576246 104.654 0.00557653 94.6684 0.0052851 86.3294 0.00505089 79.2823 0.004916 73.2505 0.00529913 70.4813 0.0102106 67.6157 0.00412931 60.8785 0.00405199 55.6357 0.00430335 53.9077 0.00851371 52.1461 0.00381633 49.2336 0.00384477 46.5699 0.00376848 44.0904 0.00363081 41.8101 0.00406673 39.6612 0.00399676 37.7253 0.00742278 35.9311 0.0233619 34.2159 0.0200174 32.6364 0.00992741 31.1401 0.00539507 29.7163 0.00395905 28.3686 0.0035076 27.0945 0.0033587 25.8839 0.00294725 24.7225 0.00280602 23.605 0.00315696 22.5303 0.0030804 21.4937 0.0025779 20.4872 0.00269725 19.5079 0.00224518 18.5467 0.00240507 17.5985 0.00209537 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 BJH Desorption Cumulative Pore Area Halsey : Faas Correction 000-629 rep 628 Cook 3FB-3-1 Pore Width (Å) Pore Area (m²/g) 979.774 0.0403084 518.383 0.162566 336.328 0.30839 248.793 0.443533 198.575 0.566794 165.681 0.677962 142.294 0.782462 124.551 0.88531 110.839 0.98525 99.7401 1.08291 90.5629 1.17653 82.8486 1.26701 76.3079 1.3556 70.6711 1.45204 70.2938 1.46551 65.3394 1.54305 57.5228 1.69037 53.9983 1.77533 53.8177 1.78452 50.6856 1.86075 47.9525 1.93595 45.3513 2.01435 42.9746 2.09136 40.7766 2.18007 38.6726 2.27281 36.8756 2.43545 35.0881 2.99666 33.4352 3.48706 31.9184 3.73238 30.4422 3.8749 29.0639 3.98213 27.7442 4.08195 26.5099 4.17995 25.3212 4.2707 24.1844 4.36126 23.0851 4.46935 22.0326 4.58017 21.0111 4.67909 20.0191 4.7897 19.0524 4.88866 18.0982 5.0044 17.1573 5.11483 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 BJH Desorption dA/dw Pore Area Halsey : Faas Correction 000-629 rep 628 Cook 3FB-3-1 Pore Width (Å) Pore Area (m²/g·Å) 1164.41 1.85807e-005 616.338 0.000264976 388.918 0.000800986 279.137 0.00154389 217.797 0.00245449 178.989 0.00337961 152.094 0.00446825 132.156 0.00579662 116.832 0.00728827 104.654 0.00879976 94.6684 0.0102003 86.3294 0.0117298 79.2823 0.0135435 73.2505 0.0171091 70.4813 0.0357061 67.6157 0.0156506 60.8785 0.0188472 55.6357 0.0241054 53.9077 0.0508932 52.1461 0.0243388 49.2336 0.0275138 46.5699 0.0301404 44.0904 0.0324004 41.8101 0.0403597 39.6612 0.0440786 37.7253 0.0905036 35.9311 0.31397 34.2159 0.296687 32.6364 0.16174 31.1401 0.0965431 29.7163 0.0778014 28.3686 0.0756335 27.0945 0.0793974 25.8839 0.0763391 24.7225 0.07967 23.605 0.0983186 22.5303 0.105304 21.4937 0.0968281 20.4872 0.111505 19.5079 0.102364 18.5467 0.121301 17.5985 0.117364 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 BJH Desorption dA/dlog(w) Pore Area Halsey : Faas Correction 000-629 rep 628 Cook 3FB-3-1 Pore Width (Å) dA/dlog(w) Pore Area (m²/g·Å) 1164.41 0.0794934 616.338 0.442201 388.918 0.77612 279.137 1.03223 217.797 1.25886 178.989 1.41343 152.094 1.58125 132.156 1.77819 116.832 1.9729 104.654 2.13142 94.6684 2.2331 86.3294 2.34029 79.2823 2.48025 73.2505 2.8937 70.4813 5.79479 67.6157 2.44281 60.8785 2.66235 55.6357 3.09395 53.9077 6.31725 52.1461 2.92741 49.2336 3.1237 46.5699 3.23684 44.0904 3.29397 41.8101 3.89068 39.6612 4.0309 37.7253 7.87035 35.9311 26.0075 34.2159 23.4012 32.6364 12.1673 31.1401 6.93005 29.7163 5.32914 28.3686 4.94575 27.0945 4.95849 25.8839 4.55456 24.7225 4.54003 23.605 5.34963 22.5303 5.46891 21.4937 4.79751 20.4872 5.26622 19.5079 4.60365 18.5467 5.18705 17.5985 4.76262 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 Horvath-Kawazoe Report Slit Pore Geometry (Original H-K) Maximum Pore Volume: 0.001117 cm³/g at Relative Pressure: 0.010616744 Median Pore Width: 7.487 Å Relative Pressure Range: 5.550e-06 to 1.062e-02 Diameter of Adsorptive Molecule: 3.000 Å Diameter of Adsorptive at Zero Interaction Energy: 2.574 Å Diameter of Sample Atom: 3.040 Å Diameter of Sample Atom at Zero Interaction Energy: 2.609 Å Interaction Parameter: 3.49e-43 erg·cm^4 Density Conversion Factor: 0.0015468 Quantity Cumulative Differential Absolute Relative Adsorbed Pore Pore Pore Pressure Pressure (cm³/g Width Volume Volume (mmHg) (P/Po) STP) (Å) (cm³/g) (cm³/g·Å) ------ 0.00414 0.000005550 0.01770 5.214 0.0000 0.0000 0.00227 0.000003040 0.03828 5.050 0.0001 -0.0002 0.00253 0.000003400 0.05799 5.080 0.0001 0.0010 0.00441 0.000005923 0.07561 5.232 0.0001 0.0002 0.00778 0.000010446 0.08999 5.402 0.0001 0.0001 0.01525 0.000020477 0.10932 5.622 0.0002 0.0001 0.02578 0.000034621 0.12785 5.812 0.0002 0.0002 0.04623 0.000062088 0.15296 6.044 0.0002 0.0002 0.07042 0.000094570 0.17488 6.227 0.0003 0.0002 0.09983 0.000134080 0.19603 6.391 0.0003 0.0002 0.13456 0.000180728 0.21652 6.540 0.0003 0.0002 0.16227 0.000217960 0.23059 6.638 0.0004 0.0002 0.19218 0.000258139 0.24409 6.731 0.0004 0.0002 0.22421 0.000301171 0.25705 6.819 0.0004 0.0002 0.25818 0.000346820 0.26950 6.902 0.0004 0.0002 0.29420 0.000395225 0.28143 6.980 0.0004 0.0002 0.33165 0.000445538 0.29299 7.056 0.0005 0.0002 0.37091 0.000498294 0.30409 7.127 0.0005 0.0002 0.41171 0.000553132 0.31482 7.196 0.0005 0.0002 0.47216 0.000634363 0.32948 7.289 0.0005 0.0002 0.53282 0.000715871 0.34294 7.373 0.0005 0.0002 0.59157 0.000794827 0.35503 7.449 0.0005 0.0002 0.64825 0.000871012 0.36589 7.516 0.0006 0.0003 0.70196 0.000943202 0.37554 7.577 0.0006 0.0002 0.75311 0.001011955 0.38429 7.632 0.0006 0.0002 0.80144 0.001076923 0.39217 7.681 0.0006 0.0002 0.84718 0.001138415 0.39925 7.724 0.0006 0.0003 0.89007 0.001196086 0.40570 7.765 0.0006 0.0002 0.92954 0.001249156 0.41161 7.800 0.0006 0.0003 0.96585 0.001297980 0.41677 7.833 0.0006 0.0002 0.99994 0.001343826 0.42153 7.861 0.0007 0.0003 1.03221 0.001387241 0.42588 7.888 0.0007 0.0002 1.06178 0.001427016 0.42979 7.912 0.0007 0.0003 1.08873 0.001463273 0.43325 7.934 0.0007 0.0002 1.11431 0.001497694 0.43645 7.954 0.0007 0.0003 1.13776 0.001529246 0.43933 7.973 0.0007 0.0002 1.15887 0.001557662 0.44189 7.988 0.0007 0.0003 1.17919 0.001585002 0.44425 8.004 0.0007 0.0002 1.19792 0.001610228 0.44640 8.018 0.0007 0.0002 1.21478 0.001632930 0.44836 8.030 0.0007 0.0002 1.23112 0.001654942 0.45021 8.042 0.0007 0.0002 1.28772 0.001731062 0.45667 8.083 0.0007 0.0002 1.34475 0.001807790 0.46293 8.122 0.0007 0.0002 1.40234 0.001885256 0.46908 8.161 0.0007 0.0002 1.46052 0.001963521 0.47506 8.199 0.0007 0.0002 1.51921 0.002042484 0.48090 8.236 0.0007 0.0002 1.57827 0.002121935 0.48655 8.274 0.0008 0.0002 1.63798 0.002202283 0.49214 8.310 0.0008 0.0002 1.69808 0.002283140 0.49754 8.344 0.0008 0.0002 1.75864 0.002364622 0.50285 8.380 0.0008 0.0002 1.81985 0.002446999 0.50806 8.415 0.0008 0.0002 1.90589 0.002562750 0.51514 8.460 0.0008 0.0002 1.96815 0.002646545 0.52006 8.495 0.0008 0.0002 2.03079 0.002730860 0.52487 8.527 0.0008 0.0002 2.09391 0.002815826 0.52960 8.560 0.0008 0.0002 2.15721 0.002901016 0.53415 8.591 0.0008 0.0002 2.22085 0.002986679 0.53864 8.622 0.0008 0.0002 2.28508 0.003073144 0.54303 8.653 0.0008 0.0002 2.34932 0.003159629 0.54734 8.683 0.0008 0.0002 2.41407 0.003246811 0.55156 8.714 0.0009 0.0002 2.47922 0.003334508 0.55565 8.743 0.0009 0.0002 2.54498 0.003423044 0.55968 8.772 0.0009 0.0002 2.61063 0.003511451 0.56359 8.801 0.0009 0.0002 2.67602 0.003599507 0.56746 8.829 0.0009 0.0002 2.74254 0.003689078 0.57127 8.858 0.0009 0.0002 2.80936 0.003779082 0.57496 8.885 0.0009 0.0002 2.87617 0.003869069 0.57856 8.912 0.0009 0.0002 2.94375 0.003960075 0.58210 8.940 0.0009 0.0002 3.01135 0.004051125 0.58554 8.967 0.0009 0.0002 3.07902 0.004142272 0.58890 8.994 0.0009 0.0002 3.14714 0.004234028 0.59222 9.020 0.0009 0.0002 3.21536 0.004325941 0.59544 9.045 0.0009 0.0002 3.28434 0.004418854 0.59861 9.072 0.0009 0.0002 3.37126 0.004535908 0.60256 9.105 0.0009 0.0002 3.43988 0.004628380 0.60556 9.129 0.0009 0.0002 3.50925 0.004721856 0.60858 9.154 0.0009 0.0002 3.57809 0.004814618 0.61144 9.178 0.0009 0.0002 3.64753 0.004908192 0.61426 9.202 0.0010 0.0002 3.71714 0.005002018 0.61708 9.227 0.0010 0.0002 3.78702 0.005096199 0.61980 9.251 0.0010 0.0002 3.85712 0.005190689 0.62251 9.276 0.0010 0.0002 3.92677 0.005284572 0.62508 9.299 0.0010 0.0002 3.99685 0.005379037 0.62765 9.323 0.0010 0.0002 4.06723 0.005473919 0.63016 9.345 0.0010 0.0002 4.13814 0.005569501 0.63264 9.369 0.0010 0.0002 4.20849 0.005664380 0.63501 9.391 0.0010 0.0002 4.27955 0.005760164 0.63735 9.415 0.0010 0.0002 4.35100 0.005856516 0.63965 9.437 0.0010 0.0002 4.42164 0.005951773 0.64190 9.458 0.0010 0.0002 4.49343 0.006048565 0.64408 9.481 0.0010 0.0001 4.56486 0.006144891 0.64625 9.502 0.0010 0.0002 4.63660 0.006241620 0.64838 9.525 0.0010 0.0001 4.70819 0.006338182 0.65046 9.546 0.0010 0.0002 4.78082 0.006436145 0.65249 9.567 0.0010 0.0001 4.85312 0.006533658 0.65448 9.589 0.0010 0.0001 4.92576 0.006631641 0.65644 9.610 0.0010 0.0001 4.99775 0.006728744 0.65832 9.631 0.0010 0.0001 5.07055 0.006826933 0.66021 9.651 0.0010 0.0001 5.62055 0.007567747 0.67652 9.803 0.0010 0.0002 6.17893 0.008319805 0.68987 9.948 0.0011 0.0001 6.74519 0.009082474 0.70095 10.087 0.0011 0.0001 7.30984 0.009843030 0.71222 10.218 0.0011 0.0001 7.88437 0.010616744 0.72220 10.347 0.0011 0.0001 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 Horvath-Kawazoe Cumulative Pore Volume Plot Slit Pore Geometry (Original H-K) 000-629 rep 628 Cook 3FB-3-1 Pore Width (Å) Pore Volume (cm³/g) 5.21384 2.73723e-005 5.04984 5.92094e-005 5.07977 8.97039e-005 5.23242 0.00011695 5.40201 0.000139197 5.62234 0.000169101 5.81205 0.000197764 6.04397 0.000236595 6.22656 0.000270509 6.39058 0.000303214 6.53958 0.00033491 6.63825 0.000356678 6.73116 0.000377563 6.8191 0.000397602 6.90192 0.000416862 6.98046 0.000435315 7.05561 0.000453198 7.12729 0.000470371 7.19643 0.000486968 7.28856 0.000509634 7.37325 0.000530453 7.44927 0.000549157 7.5164 0.000565952 7.57657 0.000580884 7.63178 0.000594421 7.68087 0.000606607 7.72375 0.000617567 7.76465 0.000627538 7.80031 0.000636677 7.83283 0.000644658 7.8611 0.000652025 7.88835 0.000658752 7.91239 0.000664793 7.9343 0.000670145 7.95405 0.000675108 7.97274 0.000679559 7.98816 0.000683509 8.0036 0.000687168 8.01796 0.000690494 8.03012 0.000693518 8.0423 0.000696385 8.0833 0.000706374 8.12223 0.000716066 8.1613 0.000725573 8.19939 0.00073482 8.23648 0.000743851 8.27369 0.000752597 8.30989 0.000761249 8.34394 0.000769588 8.38037 0.000777812 8.41463 0.000785866 8.46045 0.000796823 8.49495 0.000804432 8.52725 0.000811873 8.55964 0.00081919 8.59096 0.000826223 8.62236 0.000833162 8.65268 0.000839957 8.68308 0.000846632 8.71356 0.00085316 8.74295 0.000859483 8.7724 0.000865709 8.80075 0.000871754 8.82917 0.000877751 8.85766 0.000883633 8.88502 0.000889346 8.91245 0.000894917 8.93994 0.000900397 8.96749 0.000905707 8.99391 0.000910917 9.02039 0.000916052 9.04451 0.000921028 9.0723 0.000925932 9.105 0.000932042 9.12929 0.000936685 9.15363 0.000941356 9.17802 0.000945775 9.20246 0.000950134 9.22694 0.000954495 9.25147 0.000958713 9.27606 0.000962894 9.29946 0.000966875 9.3229 0.000970856 9.34516 0.000974731 9.36869 0.000978564 9.39102 0.000982228 9.41464 0.00098586 9.43706 0.000989411 9.45827 0.000992896 9.48077 0.000996259 9.50205 0.00099962 9.52463 0.00100292 9.54599 0.00100612 9.56739 0.00100927 9.58882 0.00101236 9.61029 0.00101538 9.63053 0.00101829 9.6508 0.00102121 9.80309 0.00104643 9.94822 0.00106708 10.0872 0.00108423 10.2185 0.00110166 10.3471 0.0011171 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:02AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 Horvath-Kawazoe Differential Pore Volume Plot Slit Pore Geometry (Original H-K) 000-629 rep 628 Cook 3FB-3-1 Pore Width (Å) dV/dw (cm³/g·Å) 5.21384 5.24993e-006 5.04984 -0.000194124 5.07977 0.00101878 5.23242 0.000178484 5.40201 0.000131189 5.62234 0.000135715 5.81205 0.000151094 6.04397 0.000167429 6.22656 0.000185745 6.39058 0.000199396 6.53958 0.000212722 6.63825 0.000220619 6.73116 0.000224784 6.8191 0.000227861 6.90192 0.000232562 6.98046 0.000234948 7.05561 0.000237964 7.12729 0.000239575 7.19643 0.000240065 7.28856 0.000246022 7.37325 0.00024582 7.44927 0.00024604 7.5164 0.000250191 7.57657 0.00024816 7.63178 0.000245201 7.68087 0.000248229 7.72375 0.000255594 7.76465 0.00024377 7.80031 0.000256318 7.83283 0.000245406 7.8611 0.000260597 7.88835 0.000246831 7.91239 0.000251251 7.9343 0.000244354 7.95405 0.000251231 7.97274 0.000238135 7.98816 0.000256253 8.0036 0.000236996 8.01796 0.000231624 8.03012 0.000248611 8.0423 0.00023542 8.0833 0.000243625 8.12223 0.000248939 8.1613 0.000243353 8.19939 0.000242804 8.23648 0.000243484 8.27369 0.000235032 8.30989 0.000238968 8.34394 0.000244929 8.38037 0.000225751 8.41463 0.000235072 8.46045 0.000239133 8.49495 0.000220555 8.52725 0.000230371 8.55964 0.000225924 8.59096 0.000224556 8.62236 0.000220975 8.65268 0.000224083 8.68308 0.000219557 8.71356 0.000214182 8.74295 0.00021518 8.7724 0.000211372 8.80075 0.000213203 8.82917 0.000211059 8.85766 0.000206465 8.88502 0.000208797 8.91245 0.000203115 8.93994 0.000199342 8.96749 0.000192688 8.99391 0.000197219 9.02039 0.000193976 9.04451 0.00020629 9.0723 0.00017646 9.105 0.000186817 9.12929 0.000191166 9.15363 0.000191884 9.17802 0.000181204 9.20246 0.000178395 9.22694 0.000178098 9.25147 0.000171926 9.27606 0.000170106 9.29946 0.000170106 9.3229 0.000169813 9.34516 0.00017412 9.36869 0.000162884 9.39102 0.000164055 9.41464 0.000153762 9.43706 0.000158389 9.45827 0.000164336 9.48077 0.00014947 9.50205 0.000157907 9.52463 0.000146065 9.54599 0.000150114 9.56739 0.000147001 9.58882 0.000144054 9.61029 0.000141025 9.63053 0.000143702 9.6508 0.000143972 9.80309 0.000165627 9.94822 0.000142279 10.0872 0.00012339 10.2185 0.000132776 10.3471 0.000120069 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:03AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 Porosity Distribution by Original Density Functional Theory Model: N2 @ 77K on Carbon, Slit Pores Method: Non-negative Regularization; No Smoothing Standard Deviation of Fit: 0.02727, cm³/g STP Volume in Pores < 5.00 Å : 0.00002 cm³/g Total Volume in Pores <= 2006.19 Å : 0.00684 cm³/g Area in Pores > 2006.19 Å : 1.447 m²/g Total Area in Pores >= 5.00 Å : 2.920 m²/g Pore Size Table Cumulative Incremental Cumulative Pore Width Volume Volume Area Incremental (Å) (cm³/g) (cm³/g) (m²/g) Area (m²/g) ----- 5.00 0.00000 0.00000 0.000 0.000 5.36 0.00000 0.00000 0.000 0.000 5.90 0.00000 0.00000 0.000 0.000 6.43 0.00000 0.00000 0.000 0.000 6.79 0.00000 0.00000 0.000 0.000 7.33 0.00000 0.00000 0.000 0.000 8.04 0.00000 0.00000 0.000 0.000 8.58 0.00000 0.00000 0.000 0.000 9.29 0.00000 0.00000 0.000 0.000 10.01 0.00000 0.00000 0.000 0.000 10.90 0.00000 0.00000 0.000 0.000 11.79 0.00000 0.00000 0.000 0.000 12.69 0.00008 0.00008 0.132 0.132 13.58 0.00029 0.00021 0.439 0.307 14.83 0.00037 0.00008 0.541 0.102 15.91 0.00039 0.00002 0.570 0.029 17.16 0.00040 0.00001 0.578 0.008 18.59 0.00040 0.00000 0.578 0.000 20.02 0.00040 0.00000 0.578 0.000 21.62 0.00040 0.00000 0.578 0.000 23.41 0.00040 0.00000 0.578 0.000 25.20 0.00044 0.00004 0.611 0.033 27.34 0.00053 0.00009 0.678 0.067 29.49 0.00061 0.00008 0.735 0.056 31.81 0.00070 0.00009 0.788 0.054 34.31 0.00078 0.00008 0.834 0.046 36.99 0.00083 0.00005 0.863 0.029 40.03 0.00089 0.00006 0.892 0.029 43.25 0.00095 0.00006 0.919 0.027 46.64 0.00102 0.00007 0.949 0.029 50.40 0.00108 0.00006 0.974 0.026 54.33 0.00115 0.00006 0.998 0.024 58.80 0.00121 0.00006 1.018 0.020 63.44 0.00126 0.00006 1.036 0.017 68.45 0.00132 0.00006 1.054 0.018 73.99 0.00139 0.00006 1.071 0.017 79.88 0.00146 0.00007 1.089 0.018 86.32 0.00157 0.00011 1.114 0.025 93.11 0.00168 0.00011 1.138 0.024 100.61 0.00177 0.00009 1.156 0.019 108.66 0.00187 0.00010 1.174 0.018 117.23 0.00197 0.00010 1.191 0.017 126.53 0.00208 0.00011 1.209 0.018 136.71 0.00220 0.00012 1.227 0.018 147.61 0.00233 0.00013 1.244 0.017 159.41 0.00246 0.00013 1.260 0.016 172.10 0.00260 0.00014 1.277 0.017 185.86 0.00274 0.00014 1.292 0.015 200.69 0.00289 0.00015 1.306 0.015 216.60 0.00304 0.00016 1.321 0.014 233.93 0.00319 0.00015 1.334 0.013 252.52 0.00336 0.00017 1.347 0.013 272.71 0.00354 0.00018 1.360 0.013 294.51 0.00368 0.00013 1.369 0.009 317.92 0.00379 0.00011 1.377 0.007 343.30 0.00390 0.00011 1.383 0.006 370.64 0.00396 0.00006 1.386 0.003 400.31 0.00405 0.00009 1.391 0.004 432.30 0.00415 0.00011 1.395 0.005 466.79 0.00431 0.00015 1.402 0.007 503.96 0.00458 0.00027 1.413 0.011 544.17 0.00492 0.00034 1.425 0.012 587.60 0.00517 0.00026 1.434 0.009 634.42 0.00540 0.00023 1.441 0.007 684.99 0.00568 0.00028 1.449 0.008 739.68 0.00586 0.00019 1.454 0.005 798.65 0.00603 0.00017 1.458 0.004 862.45 0.00622 0.00019 1.463 0.004 931.26 0.00638 0.00016 1.466 0.003 1005.60 0.00648 0.00010 1.468 0.002 1085.66 0.00656 0.00008 1.470 0.002 1172.33 0.00666 0.00010 1.471 0.002 1265.80 0.00672 0.00006 1.472 0.001 1366.77 0.00676 0.00004 1.473 0.001 1475.96 0.00680 0.00004 1.473 0.000 1593.55 0.00682 0.00002 1.474 0.000 1720.79 0.00683 0.00000 1.474 0.000 1858.04 0.00683 0.00000 1.474 0.000 2006.19 0.00683 0.00000 1.474 0.000 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:03AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 Porosity Distribution by Original Density Functional Theory Model: N2 @ 77K on Carbon, Slit Pores Method: Non-negative Regularization; No Smoothing Standard Deviation of Fit: 0.02727, cm³/g STP Isotherm Table Fitted Experimental Quantity Absolute Quantity Adsorbed Residual Relative Adsorbed (cm³/g (cm³/g Relative Pressure (cm³/g STP) STP) STP) Residual ----- 0.000008995 0.0866 0.0202 0.0664 0.767146 0.000015520 0.1004 0.0271 0.0733 0.730323 0.000026102 0.1174 0.0387 0.0787 0.670488 0.000042841 0.1361 0.0583 0.0778 0.571473 0.000068697 0.1578 0.0919 0.0659 0.417789 0.000107744 0.1824 0.1473 0.0350 0.192131 0.000165451 0.2102 0.2233 -0.0131 -0.062240 0.000249000 0.2412 0.2985 -0.0574 -0.237861 0.000367617 0.2747 0.3597 -0.0850 -0.309286 0.000532902 0.3110 0.4079 -0.0970 -0.311875 0.000759152 0.3497 0.4468 -0.0971 -0.277760 0.001063641 0.3906 0.4790 -0.0884 -0.226415 0.001466847 0.4336 0.5065 -0.0729 -0.168143 0.001992604 0.4772 0.5304 -0.0532 -0.111478 0.002668156 0.5213 0.5518 -0.0305 -0.058558 0.003524104 0.5641 0.5715 -0.0073 -0.012988 0.004594232 0.6045 0.5902 0.0142 0.023516 0.005915212 0.6410 0.6192 0.0219 0.034112 0.007526182 0.6757 0.6401 0.0356 0.052706 0.009468212 0.7067 0.7084 -0.0017 -0.002421 0.011783670 0.7337 0.7282 0.0055 0.007532 0.014515520 0.7580 0.7462 0.0119 0.015634 0.017706521 0.7824 0.7830 -0.0006 -0.000760 0.021398440 0.8059 0.8004 0.0055 0.006834 0.025631230 0.8283 0.8180 0.0104 0.012507 0.030442240 0.8498 0.8419 0.0079 0.009296 0.035865448 0.8730 0.8610 0.0119 0.013682 0.041930798 0.8980 0.8835 0.0145 0.016144 0.048663601 0.9233 0.9059 0.0174 0.018849 0.056084011 0.9483 0.9308 0.0175 0.018449 0.064206667 0.9750 0.9586 0.0164 0.016801 0.073040441 1.0020 0.9894 0.0126 0.012592 0.082588248 1.0297 1.0224 0.0073 0.007054 0.092847057 1.0572 1.0566 0.0006 0.000539 0.103808001 1.0847 1.0904 -0.0056 -0.005202 0.115456402 1.1122 1.1226 -0.0104 -0.009368 0.127772301 1.1408 1.1530 -0.0122 -0.010703 0.140730694 1.1706 1.1813 -0.0107 -0.009148 0.154301897 1.2016 1.2078 -0.0062 -0.005201 0.168452203 1.2327 1.2329 -0.0002 -0.000166 0.183144197 1.2633 1.2698 -0.0066 -0.005191 0.198337302 1.2951 1.2928 0.0023 0.001754 0.213988706 1.3280 1.3153 0.0127 0.009584 0.230053306 1.3578 1.3675 -0.0098 -0.007188 0.246484801 1.3920 1.3895 0.0026 0.001842 0.263235897 1.4246 1.4116 0.0130 0.009123 0.280259013 1.4581 1.4618 -0.0037 -0.002570 0.297506303 1.4937 1.4848 0.0089 0.005958 0.314930797 1.5300 1.5382 -0.0081 -0.005313 0.332486212 1.5632 1.5627 0.0005 0.000293 0.350127310 1.6007 1.5885 0.0122 0.007644 0.367810607 1.6362 1.6430 -0.0068 -0.004167 0.385494202 1.6719 1.6708 0.0011 0.000648 0.403138310 1.7090 1.6994 0.0096 0.005603 0.420704991 1.7456 1.7473 -0.0017 -0.000996 0.438158900 1.7809 1.7758 0.0051 0.002840 0.455466807 1.8160 1.8248 -0.0088 -0.004843 0.472598106 1.8532 1.8518 0.0014 0.000748 0.489524394 1.8882 1.8778 0.0104 0.005494 0.506219923 1.9216 1.9249 -0.0032 -0.001690 0.522661209 1.9548 1.9492 0.0056 0.002867 0.538827300 1.9889 1.9992 -0.0103 -0.005186 0.554699600 2.0233 2.0224 0.0008 0.000416 0.570261598 2.0572 2.0455 0.0117 0.005679 0.585499227 2.0894 2.0938 -0.0044 -0.002114 0.600400090 2.1232 2.1171 0.0062 0.002899 0.614954293 2.1577 2.1667 -0.0089 -0.004136 0.629153311 2.1910 2.1908 0.0002 0.000109 0.642990828 2.2260 2.2156 0.0104 0.004662 0.656461716 2.2619 2.2653 -0.0035 -0.001540 0.669562697 2.2964 2.2916 0.0048 0.002089 0.682291925 2.3315 2.3414 -0.0099 -0.004245 0.694648683 2.3690 2.3684 0.0006 0.000241 0.706633508 2.4061 2.3955 0.0106 0.004404 0.718248010 2.4431 2.4484 -0.0053 -0.002181 0.729494929 2.4808 2.4744 0.0064 0.002562 0.740377605 2.5196 2.5269 -0.0073 -0.002891 0.750900388 2.5598 2.5516 0.0082 0.003194 0.761068285 2.6000 2.6082 -0.0082 -0.003157 0.770887017 2.6410 2.6320 0.0090 0.003407 0.780362606 2.6831 2.7033 -0.0201 -0.007508 0.789501607 2.7270 2.7266 0.0004 0.000129 0.798311174 2.7708 2.7502 0.0206 0.007441 0.806798697 2.8151 2.8252 -0.0101 -0.003580 0.814971626 2.8601 2.8494 0.0107 0.003735 0.822837889 2.9072 2.9186 -0.0114 -0.003911 0.830405474 2.9560 2.9441 0.0119 0.004028 0.837682605 3.0046 3.0158 -0.0112 -0.003724 0.844677329 3.0539 3.0422 0.0117 0.003817 0.851397991 3.1042 3.1166 -0.0124 -0.003982 0.857852995 3.1558 3.1430 0.0128 0.004050 0.864050388 3.2101 3.2250 -0.0149 -0.004634 0.869998574 3.2656 3.2503 0.0153 0.004672 0.875705481 3.3202 3.3355 -0.0153 -0.004606 0.881179392 3.3753 3.3597 0.0156 0.004630 0.886428118 3.4312 3.4472 -0.0160 -0.004669 0.891459525 3.4871 3.4707 0.0163 0.004679 0.896281302 3.5425 3.5598 -0.0173 -0.004896 0.900900900 3.6011 3.5835 0.0176 0.004890 0.905325770 3.6628 3.6817 -0.0189 -0.005152 0.909563184 3.7256 3.7065 0.0191 0.005130 0.913620114 3.7878 3.8056 -0.0178 -0.004701 0.917503417 3.8497 3.8317 0.0180 0.004681 0.921219707 3.9155 3.9359 -0.0205 -0.005230 0.924775481 3.9835 3.9628 0.0207 0.005190 0.928177178 4.0520 4.0726 -0.0206 -0.005092 0.931430817 4.1197 4.0989 0.0208 0.005050 0.934542298 4.1855 4.2058 -0.0203 -0.004861 0.937517405 4.2514 4.2309 0.0205 0.004821 0.940361619 4.3225 4.3473 -0.0248 -0.005749 0.943080306 4.3966 4.3716 0.0250 0.005684 0.945678592 4.4717 4.4967 -0.0250 -0.005591 0.948161721 4.5462 4.5211 0.0251 0.005527 0.950534225 4.6190 4.6190 0.0001 0.000016 0.952800930 4.6891 4.7090 -0.0199 -0.004253 0.954966187 4.7557 4.7356 0.0200 0.004213 0.957034409 4.8144 4.8245 -0.0101 -0.002096 0.959009588 4.8629 4.8527 0.0102 0.002090 0.960896015 4.9078 4.9169 -0.0091 -0.001855 0.962697208 4.9544 4.9452 0.0092 0.001850 0.964416981 5.0064 5.0230 -0.0166 -0.003315 0.966058910 5.0668 5.0501 0.0167 0.003288 0.967626274 5.1373 5.1373 0.0000 0.000008 0.969122529 5.2192 5.2530 -0.0337 -0.006465 0.970550597 5.3132 5.2794 0.0338 0.006364 0.971913695 5.4193 5.4645 -0.0452 -0.008342 0.973214507 5.5375 5.4922 0.0453 0.008177 0.974455774 5.6672 5.7197 -0.0525 -0.009272 0.975640416 5.8024 5.7498 0.0526 0.009070 0.976770699 5.9318 5.9318 0.0000 0.000003 0.977849126 6.0552 6.0986 -0.0434 -0.007161 0.978878021 6.1730 6.1296 0.0434 0.007033 0.979859591 6.2853 6.3241 -0.0388 -0.006172 0.980795979 6.3925 6.3537 0.0388 0.006075 0.981689274 6.4948 6.4948 0.0000 0.000001 0.982541502 6.5923 6.6240 -0.0316 -0.004801 0.983354270 6.6854 6.6537 0.0317 0.004738 0.984129488 6.7741 6.8002 -0.0261 -0.003855 0.984869003 6.8587 6.8326 0.0261 0.003811 0.985574186 6.9395 6.9605 -0.0210 -0.003026 0.986246824 7.0165 6.9954 0.0210 0.002995 0.986888289 7.0899 7.0899 0.0000 0.000000 0.987500012 7.1599 7.1765 -0.0166 -0.002322 0.988083303 7.2267 7.2100 0.0166 0.002302 0.988639593 7.2903 7.3041 -0.0137 -0.001883 0.989170074 7.3511 7.3373 0.0137 0.001868 0.989675879 7.4090 7.4090 -0.0000 -0.000000 0.990158200 7.4642 7.4713 -0.0072 -0.000961 0.990618110 7.5168 7.5096 0.0072 0.000955 0.991056621 7.5670 7.5709 -0.0039 -0.000514 0.991474688 7.6149 7.6110 0.0039 0.000511 0.991873324 7.6605 7.6605 -0.0000 -0.000000 0.992253423 7.7040 7.7008 0.0032 0.000419 0.992615700 7.7455 7.7395 0.0060 0.000774 0.992961228 7.7850 7.7833 0.0017 0.000221 0.993290603 7.8227 7.8244 -0.0016 -0.000209 0.993604600 7.8587 7.8680 -0.0093 -0.001187 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:03AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 Cumulative Surface Area vs. Pore Width Cumulative Surface Area Pore Width (Angstroms) Cumulative Surface Area (m²/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 0.131744 13.5819 0.439055 14.8329 0.540743 15.9052 0.56989 17.1561 0.577709 18.5858 0.577709 20.0155 0.577709 21.6239 0.577709 23.411 0.577709 25.198 0.610684 27.3426 0.678142 29.4871 0.734524 31.8103 0.788404 34.3122 0.834143 36.9929 0.863109 40.0309 0.89204 43.2477 0.919251 46.6432 0.948684 50.3961 0.974243 54.3277 0.998102 58.7954 1.01821 63.4419 1.0356 68.4458 1.05372 73.9858 1.07061 79.8832 1.08902 86.3167 1.11358 93.1077 1.13757 100.613 1.15642 108.655 1.17409 117.233 1.19098 126.526 1.20909 136.713 1.2269 147.614 1.24405 159.409 1.26014 172.097 1.27676 185.858 1.29189 200.691 1.30648 216.596 1.32082 233.931 1.33367 252.517 1.347 272.711 1.36043 294.513 1.36934 317.924 1.37656 343.301 1.38287 370.644 1.38625 400.309 1.39062 432.298 1.39549 466.789 1.40209 503.961 1.41285 544.171 1.42523 587.597 1.43394 634.419 1.44115 684.994 1.44921 739.679 1.45427 798.653 1.45844 862.452 1.46289 931.255 1.46622 1005.6 1.46821 1085.66 1.46975 1172.33 1.47145 1265.8 1.4724 1366.77 1.47302 1475.96 1.4735 1593.55 1.4738 1720.79 1.47383 1858.04 1.47383 2006.19 1.47383 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:03AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 Incremental Surface Area vs. Pore Width Incremental Surface Area Pore Width (Angstroms) Incremental Surface Area (m²/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 0.131744 13.5819 0.30731 14.8329 0.101688 15.9052 0.0291472 17.1561 0.00781867 18.5858 0 20.0155 0 21.6239 0 23.411 0 25.198 0.0329756 27.3426 0.0674577 29.4871 0.0563821 31.8103 0.0538799 34.3122 0.0457385 36.9929 0.0289664 40.0309 0.0289314 43.2477 0.0272106 46.6432 0.0294333 50.3961 0.025559 54.3277 0.0238583 58.7954 0.0201114 63.4419 0.0173869 68.4458 0.0181194 73.9858 0.0168924 79.8832 0.0184062 86.3167 0.0245666 93.1077 0.0239879 100.613 0.0188433 108.655 0.0176753 117.233 0.0168909 126.526 0.0181057 136.713 0.0178169 147.614 0.0171466 159.409 0.0160884 172.097 0.0166173 185.858 0.0151282 200.691 0.0145936 216.596 0.0143374 233.931 0.0128524 252.517 0.01333 272.711 0.0134347 294.513 0.00890374 317.924 0.00722061 343.301 0.00631333 370.644 0.00338358 400.309 0.00436793 432.298 0.00486344 466.789 0.0066008 503.961 0.0107666 544.171 0.0123728 587.597 0.00871604 634.419 0.00720647 684.994 0.00805733 739.679 0.00506202 798.653 0.00417235 862.452 0.00444796 931.255 0.00333313 1005.6 0.00198948 1085.66 0.00153903 1172.33 0.00169892 1265.8 0.000949017 1366.77 0.000622918 1475.96 0.000475418 1593.55 0.000305942 1720.79 3.20493e-005 1858.04 0 2006.19 0 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:03AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 Differential Surface Area vs. Pore Width Differential Surface Area Pore Width (Angstroms) Differential Surface Area (m²/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 4.30048 13.5819 9.06256 14.8329 2.96568 15.9052 0.922482 17.1561 0.231174 18.5858 0 20.0155 0 21.6239 0 23.411 0 25.198 0.978211 27.3426 1.97635 29.4871 1.7156 31.8103 1.63726 34.3122 1.39552 36.9929 0.865355 40.0309 0.852867 43.2477 0.819689 46.6432 0.886096 50.3961 0.771791 54.3277 0.712755 58.7954 0.597177 63.4419 0.526853 68.4458 0.542724 73.9858 0.503434 79.8832 0.549875 86.3167 0.738511 93.1077 0.720778 100.613 0.561934 108.655 0.532426 117.233 0.51084 126.526 0.542431 136.713 0.532269 147.614 0.514114 159.409 0.4828 172.097 0.498506 185.858 0.453257 200.691 0.439108 216.596 0.430813 233.931 0.38573 252.517 0.400209 272.711 0.402146 294.513 0.267294 317.924 0.216932 343.301 0.189496 370.644 0.101425 400.309 0.130723 432.298 0.145775 466.789 0.198183 503.961 0.323254 544.171 0.371093 587.597 0.261582 634.419 0.216388 684.994 0.241718 739.679 0.15185 798.653 0.125123 862.452 0.133351 931.255 0.0999595 1005.6 0.0597215 1085.66 0.0461984 1172.33 0.0509642 1265.8 0.0284802 1366.77 0.0186753 1475.96 0.0142616 1593.55 0.00918004 1720.79 0.000961152 1858.04 0 2006.19 0 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:03AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 Cumulative Pore Volume vs. Pore Width Cumulative Pore Volume Pore Width (Angstroms) Cumulative Pore Volume (cm³/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 8.35811e-005 13.5819 0.000292275 14.8329 0.000367691 15.9052 0.00039087 17.1561 0.000397577 18.5858 0.000397577 20.0155 0.000397577 21.6239 0.000397577 23.411 0.000397577 25.198 0.000439123 27.3426 0.000531347 29.4871 0.000614474 31.8103 0.000700171 34.3122 0.00077864 36.9929 0.000832218 40.0309 0.000890125 43.2477 0.000948965 46.6432 0.00101761 50.3961 0.00108201 54.3277 0.00114682 58.7954 0.00120594 63.4419 0.0012611 68.4458 0.00132311 73.9858 0.0013856 79.8832 0.00145911 86.3167 0.00156514 93.1077 0.00167681 100.613 0.00177161 108.655 0.00186763 117.233 0.00196664 126.526 0.00208118 136.713 0.00220297 147.614 0.00232953 159.409 0.00245776 172.097 0.00260075 185.858 0.00274133 200.691 0.00288777 216.596 0.00304304 233.931 0.00319337 252.517 0.00336168 272.711 0.00354487 294.513 0.00367598 317.924 0.00379076 343.301 0.00389913 370.644 0.00396183 400.309 0.00404926 432.298 0.00415438 466.789 0.00430844 503.961 0.00457974 544.171 0.00491638 587.597 0.00517246 634.419 0.00540106 684.994 0.00567702 739.679 0.00586423 798.653 0.00603084 862.452 0.00622265 931.255 0.00637785 1005.6 0.00647788 1085.66 0.00656142 1172.33 0.00666101 1265.8 0.00672107 1366.77 0.00676364 1475.96 0.00679873 1593.55 0.0068231 1720.79 0.00682586 1858.04 0.00682586 2006.19 0.00682586 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:03AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 Incremental Pore Volume vs. Pore Width Incremental Pore Volume Pore Width (Angstroms) Incremental Pore Volume (cm³/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 8.35811e-005 13.5819 0.000208693 14.8329 7.54163e-005 15.9052 2.31796e-005 17.1561 6.7069e-006 18.5858 0 20.0155 0 21.6239 0 23.411 0 25.198 4.1546e-005 27.3426 9.22233e-005 29.4871 8.31272e-005 31.8103 8.56968e-005 34.3122 7.84696e-005 36.9929 5.35775e-005 40.0309 5.79075e-005 43.2477 5.88398e-005 46.6432 6.86432e-005 50.3961 6.44038e-005 54.3277 6.48084e-005 58.7954 5.91228e-005 63.4419 5.51529e-005 68.4458 6.20097e-005 73.9858 6.24899e-005 79.8832 7.35172e-005 86.3167 0.000106026 93.1077 0.000111673 100.613 9.47945e-005 108.655 9.60261e-005 117.233 9.90087e-005 126.526 0.000114542 136.713 0.00012179 147.614 0.000126554 159.409 0.000128232 172.097 0.00014299 185.858 0.000140585 200.691 0.00014644 216.596 0.000155271 233.931 0.000150329 252.517 0.000168302 272.711 0.000183189 294.513 0.000131114 317.924 0.00011478 343.301 0.000108369 370.644 6.27052e-005 400.309 8.74261e-005 432.298 0.000105123 466.789 0.000154059 503.961 0.000271298 544.171 0.000336644 587.597 0.000256076 634.419 0.000228596 684.994 0.000275961 739.679 0.000187214 798.653 0.000166613 862.452 0.000191808 931.255 0.0001552 1005.6 0.000100031 1085.66 8.35431e-005 1172.33 9.9585e-005 1265.8 6.00633e-005 1366.77 4.25693e-005 1475.96 3.50849e-005 1593.55 2.43767e-005 1720.79 2.75751e-006 1858.04 0 2006.19 0 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:03AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 Differential Pore Volume vs. Pore Width Differential Pore Volume Pore Width (Angstroms) Differential Pore Volume (cm³/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 0.0027283 13.5819 0.00615435 14.8329 0.00219948 15.9052 0.00073361 17.1561 0.000198302 18.5858 0 20.0155 0 21.6239 0 23.411 0 25.198 0.00123245 27.3426 0.00270193 29.4871 0.00252941 31.8103 0.00260408 34.3122 0.00239418 36.9929 0.0016006 40.0309 0.00170705 43.2477 0.00177248 46.6432 0.00206652 50.3961 0.00194476 54.3277 0.00193612 58.7954 0.00175556 63.4419 0.00167123 68.4458 0.00185736 73.9858 0.00186235 79.8832 0.00219629 86.3167 0.00318729 93.1077 0.0033555 100.613 0.00282691 108.655 0.00289255 117.233 0.00299438 126.526 0.00343159 136.713 0.0036384 147.614 0.00379452 159.409 0.00384813 172.097 0.00428957 185.858 0.00421207 200.691 0.00440625 216.596 0.00466562 233.931 0.00451171 252.517 0.00505298 272.711 0.00548347 294.513 0.00393608 317.924 0.0034484 343.301 0.00325271 370.644 0.00187963 400.309 0.00261649 432.298 0.00315092 466.789 0.00462548 503.961 0.00814537 544.171 0.0100969 587.597 0.00768523 634.419 0.00686402 684.994 0.00827878 739.679 0.005616 798.653 0.0049965 862.452 0.00575044 931.255 0.00465439 1005.6 0.00300279 1085.66 0.00250779 1172.33 0.00298736 1265.8 0.00180251 1366.77 0.00127624 1475.96 0.00105248 1593.55 0.000731444 1720.79 8.26973e-005 1858.04 0 2006.19 0 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:03AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 Standard Deviation of Fit: 0.02727, cm³/g STP Goodness of Fit Input Data Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 5.54983e-006 0.0176961 3.04028e-006 0.0382787 3.40009e-006 0.0579932 5.92287e-006 0.0756076 1.04459e-005 0.0899906 2.04765e-005 0.109323 3.46209e-005 0.127854 6.20882e-005 0.152957 9.45702e-005 0.174883 0.00013408 0.196027 0.000180728 0.216518 0.00021796 0.230591 0.000258139 0.244093 0.000301171 0.257048 0.00034682 0.269499 0.000395225 0.281429 0.000445538 0.292991 0.000498294 0.304093 0.000553132 0.314823 0.000634363 0.329476 0.000715871 0.342936 0.000794827 0.355028 0.000871012 0.365886 0.000943202 0.375539 0.00101195 0.384291 0.00107692 0.392169 0.00113841 0.399255 0.00119609 0.405701 0.00124916 0.411609 0.00129798 0.416769 0.00134383 0.421532 0.00138724 0.42588 0.00142702 0.429786 0.00146327 0.433246 0.00149769 0.436455 0.00152925 0.439332 0.00155766 0.441886 0.001585 0.444252 0.00161023 0.446402 0.00163293 0.448357 0.00165494 0.45021 0.00173106 0.456668 0.00180779 0.462934 0.00188526 0.46908 0.00196352 0.475058 0.00204248 0.480897 0.00212194 0.486551 0.00220228 0.492144 0.00228314 0.497536 0.00236462 0.502853 0.002447 0.508059 0.00256275 0.515143 0.00264655 0.520062 0.00273086 0.524872 0.00281583 0.529603 0.00290102 0.53415 0.00298668 0.538636 0.00307314 0.543029 0.00315963 0.547344 0.00324681 0.551565 0.00333451 0.555652 0.00342304 0.559678 0.00351145 0.563585 0.00359951 0.567463 0.00368908 0.571265 0.00377908 0.574959 0.00386907 0.578561 0.00396008 0.582103 0.00405113 0.585536 0.00414227 0.588904 0.00423403 0.592224 0.00432594 0.595441 0.00441885 0.598612 0.00453591 0.602561 0.00462838 0.605563 0.00472186 0.608583 0.00481462 0.611439 0.00490819 0.614258 0.00500202 0.617077 0.0050962 0.619804 0.00519069 0.622507 0.00528457 0.625081 0.00537904 0.627655 0.00547392 0.63016 0.0055695 0.632638 0.00566438 0.635007 0.00576016 0.637354 0.00585652 0.63965 0.00595177 0.641904 0.00604857 0.644077 0.00614489 0.64625 0.00624162 0.648382 0.00633818 0.650455 0.00643614 0.652489 0.00653366 0.654485 0.00663164 0.656442 0.00672874 0.658322 0.00682693 0.660209 0.00756775 0.676516 0.0083198 0.689865 0.00908247 0.700951 0.00984303 0.71222 0.0106167 0.722203 0.029661 0.846505 0.0501818 0.928525 0.0704339 0.994245 0.0903828 1.05081 0.110528 1.10077 0.130568 1.1472 0.150673 1.19335 0.170701 1.2375 0.190718 1.27891 0.210832 1.32172 0.230964 1.35959 0.251721 1.40268 0.271273 1.44003 0.291246 1.48053 0.311274 1.52279 0.331518 1.5612 0.352203 1.60497 0.372806 1.64626 0.392473 1.68611 0.412911 1.72978 0.432717 1.76985 0.452647 1.81021 0.472013 1.85193 0.492973 1.89521 0.512945 1.93506 0.533373 1.97715 0.553582 2.02084 0.573535 2.06437 0.593848 2.10776 0.613525 2.15436 0.633957 2.20266 0.653802 2.25486 0.673999 2.30813 0.693975 2.36696 0.714355 2.43051 0.734327 2.49766 0.754357 2.57328 0.774599 2.65705 0.794686 2.75258 0.81491 2.85976 0.83485 2.98545 0.854973 3.13223 0.874818 3.31168 0.895039 3.52788 0.915109 3.81089 0.935294 4.20145 0.955264 4.76479 0.974701 5.69488 0.993845 7.88613 Model Fit Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 8.99464e-006 0.020166 1.552e-005 0.0270677 2.61021e-005 0.0386782 4.28409e-005 0.0583297 6.86973e-005 0.0918654 0.000107744 0.147325 0.000165451 0.223283 0.000249 0.298523 0.000367617 0.359713 0.000532902 0.407936 0.000759152 0.446799 0.00106364 0.479034 0.00146685 0.506486 0.0019926 0.530435 0.00266816 0.551831 0.0035241 0.57147 0.00459423 0.590244 0.00591521 0.619183 0.00752618 0.640057 0.00946821 0.708375 0.0117837 0.728178 0.0145155 0.746188 0.0177065 0.782964 0.0213984 0.800429 0.0256312 0.817952 0.0304422 0.841939 0.0358654 0.861013 0.0419308 0.883488 0.0486636 0.905923 0.056084 0.930833 0.0642067 0.958626 0.0730404 0.989353 0.0825882 1.02242 0.0928471 1.05658 0.103808 1.09036 0.115456 1.12265 0.127772 1.15297 0.140731 1.18129 0.154302 1.20783 0.168452 1.23291 0.183144 1.26983 0.198337 1.29284 0.213989 1.31531 0.230053 1.36755 0.246485 1.38947 0.263236 1.41158 0.280259 1.46182 0.297506 1.48476 0.314931 1.53817 0.332486 1.56273 0.350127 1.5885 0.367811 1.64304 0.385494 1.67082 0.403138 1.6994 0.420705 1.74729 0.438159 1.77581 0.455467 1.82484 0.472598 1.85177 0.489524 1.87782 0.50622 1.92485 0.522661 1.94919 0.538827 1.99917 0.5547 2.02243 0.570262 2.04555 0.585499 2.09382 0.6004 2.11706 0.614954 2.16666 0.629153 2.19076 0.642991 2.21561 0.656462 2.26535 0.669563 2.2916 0.682292 2.34142 0.694649 2.36844 0.706634 2.39548 0.718248 2.44839 0.729495 2.47444 0.740378 2.52687 0.7509 2.55159 0.761068 2.60824 0.770887 2.63196 0.780363 2.70327 0.789502 2.72661 0.798311 2.75016 0.806799 2.82516 0.814972 2.84943 0.822838 2.91856 0.830405 2.94406 0.837683 3.01576 0.844677 3.04225 0.851398 3.1166 0.857853 3.143 0.86405 3.22501 0.869999 3.25033 0.875705 3.33554 0.881179 3.35968 0.886428 3.44722 0.89146 3.47074 0.896281 3.5598 0.900901 3.58354 0.905326 3.68172 0.909563 3.70646 0.91362 3.80557 0.917503 3.83168 0.92122 3.93593 0.924775 3.96279 0.928177 4.07265 0.931431 4.09891 0.934542 4.20584 0.937517 4.23088 0.940362 4.3473 0.94308 4.37156 0.945679 4.49668 0.948162 4.52112 0.950534 4.61895 0.952801 4.70901 0.954966 4.73564 0.957034 4.82447 0.95901 4.85272 0.960896 4.91693 0.962697 4.94522 0.964417 5.02303 0.966059 5.05012 0.967626 5.13727 0.969123 5.25298 0.970551 5.27937 0.971914 5.46453 0.973215 5.49219 0.974456 5.71971 0.97564 5.74978 0.976771 5.93176 0.977849 6.09858 0.978878 6.12958 0.97986 6.32414 0.980796 6.35369 0.981689 6.49477 0.982542 6.62398 0.983354 6.65369 0.984129 6.80021 0.984869 6.83261 0.985574 6.96046 0.986247 6.99544 0.986888 7.08988 0.9875 7.17653 0.988083 7.21003 0.98864 7.30407 0.98917 7.33733 0.989676 7.40896 0.990158 7.47135 0.990618 7.50963 0.991057 7.5709 0.991475 7.61097 0.991873 7.66049 0.992253 7.70077 0.992616 7.73947 0.992961 7.78329 0.993291 7.82435 0.993605 7.86799 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-629 rep 628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-629.SMP Started: 1/3/2018 10:08:44AM Analysis Adsorptive: N2 Completed: 1/4/2018 5:57:53AM Analysis Bath Temp.: -195.985 °C Report Time: 10/2/2019 10:03:03AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 15.9033 cm³ Measured Cold Free Space: 46.9078 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 rep of 628 Standard Deviation of Fit: 0.02727, cm³/g STP Goodness of Fit Input Data Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 5.54983e-006 0.0176961 3.04028e-006 0.0382787 3.40009e-006 0.0579932 5.92287e-006 0.0756076 1.04459e-005 0.0899906 2.04765e-005 0.109323 3.46209e-005 0.127854 6.20882e-005 0.152957 9.45702e-005 0.174883 0.00013408 0.196027 0.000180728 0.216518 0.00021796 0.230591 0.000258139 0.244093 0.000301171 0.257048 0.00034682 0.269499 0.000395225 0.281429 0.000445538 0.292991 0.000498294 0.304093 0.000553132 0.314823 0.000634363 0.329476 0.000715871 0.342936 0.000794827 0.355028 0.000871012 0.365886 0.000943202 0.375539 0.00101195 0.384291 0.00107692 0.392169 0.00113841 0.399255 0.00119609 0.405701 0.00124916 0.411609 0.00129798 0.416769 0.00134383 0.421532 0.00138724 0.42588 0.00142702 0.429786 0.00146327 0.433246 0.00149769 0.436455 0.00152925 0.439332 0.00155766 0.441886 0.001585 0.444252 0.00161023 0.446402 0.00163293 0.448357 0.00165494 0.45021 0.00173106 0.456668 0.00180779 0.462934 0.00188526 0.46908 0.00196352 0.475058 0.00204248 0.480897 0.00212194 0.486551 0.00220228 0.492144 0.00228314 0.497536 0.00236462 0.502853 0.002447 0.508059 0.00256275 0.515143 0.00264655 0.520062 0.00273086 0.524872 0.00281583 0.529603 0.00290102 0.53415 0.00298668 0.538636 0.00307314 0.543029 0.00315963 0.547344 0.00324681 0.551565 0.00333451 0.555652 0.00342304 0.559678 0.00351145 0.563585 0.00359951 0.567463 0.00368908 0.571265 0.00377908 0.574959 0.00386907 0.578561 0.00396008 0.582103 0.00405113 0.585536 0.00414227 0.588904 0.00423403 0.592224 0.00432594 0.595441 0.00441885 0.598612 0.00453591 0.602561 0.00462838 0.605563 0.00472186 0.608583 0.00481462 0.611439 0.00490819 0.614258 0.00500202 0.617077 0.0050962 0.619804 0.00519069 0.622507 0.00528457 0.625081 0.00537904 0.627655 0.00547392 0.63016 0.0055695 0.632638 0.00566438 0.635007 0.00576016 0.637354 0.00585652 0.63965 0.00595177 0.641904 0.00604857 0.644077 0.00614489 0.64625 0.00624162 0.648382 0.00633818 0.650455 0.00643614 0.652489 0.00653366 0.654485 0.00663164 0.656442 0.00672874 0.658322 0.00682693 0.660209 0.00756775 0.676516 0.0083198 0.689865 0.00908247 0.700951 0.00984303 0.71222 0.0106167 0.722203 0.029661 0.846505 0.0501818 0.928525 0.0704339 0.994245 0.0903828 1.05081 0.110528 1.10077 0.130568 1.1472 0.150673 1.19335 0.170701 1.2375 0.190718 1.27891 0.210832 1.32172 0.230964 1.35959 0.251721 1.40268 0.271273 1.44003 0.291246 1.48053 0.311274 1.52279 0.331518 1.5612 0.352203 1.60497 0.372806 1.64626 0.392473 1.68611 0.412911 1.72978 0.432717 1.76985 0.452647 1.81021 0.472013 1.85193 0.492973 1.89521 0.512945 1.93506 0.533373 1.97715 0.553582 2.02084 0.573535 2.06437 0.593848 2.10776 0.613525 2.15436 0.633957 2.20266 0.653802 2.25486 0.673999 2.30813 0.693975 2.36696 0.714355 2.43051 0.734327 2.49766 0.754357 2.57328 0.774599 2.65705 0.794686 2.75258 0.81491 2.85976 0.83485 2.98545 0.854973 3.13223 0.874818 3.31168 0.895039 3.52788 0.915109 3.81089 0.935294 4.20145 0.955264 4.76479 0.974701 5.69488 0.993845 7.88613 Model Fit Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 8.99464e-006 0.020166 1.552e-005 0.0270677 2.61021e-005 0.0386782 4.28409e-005 0.0583297 6.86973e-005 0.0918654 0.000107744 0.147325 0.000165451 0.223283 0.000249 0.298523 0.000367617 0.359713 0.000532902 0.407936 0.000759152 0.446799 0.00106364 0.479034 0.00146685 0.506486 0.0019926 0.530435 0.00266816 0.551831 0.0035241 0.57147 0.00459423 0.590244 0.00591521 0.619183 0.00752618 0.640057 0.00946821 0.708375 0.0117837 0.728178 0.0145155 0.746188 0.0177065 0.782964 0.0213984 0.800429 0.0256312 0.817952 0.0304422 0.841939 0.0358654 0.861013 0.0419308 0.883488 0.0486636 0.905923 0.056084 0.930833 0.0642067 0.958626 0.0730404 0.989353 0.0825882 1.02242 0.0928471 1.05658 0.103808 1.09036 0.115456 1.12265 0.127772 1.15297 0.140731 1.18129 0.154302 1.20783 0.168452 1.23291 0.183144 1.26983 0.198337 1.29284 0.213989 1.31531 0.230053 1.36755 0.246485 1.38947 0.263236 1.41158 0.280259 1.46182 0.297506 1.48476 0.314931 1.53817 0.332486 1.56273 0.350127 1.5885 0.367811 1.64304 0.385494 1.67082 0.403138 1.6994 0.420705 1.74729 0.438159 1.77581 0.455467 1.82484 0.472598 1.85177 0.489524 1.87782 0.50622 1.92485 0.522661 1.94919 0.538827 1.99917 0.5547 2.02243 0.570262 2.04555 0.585499 2.09382 0.6004 2.11706 0.614954 2.16666 0.629153 2.19076 0.642991 2.21561 0.656462 2.26535 0.669563 2.2916 0.682292 2.34142 0.694649 2.36844 0.706634 2.39548 0.718248 2.44839 0.729495 2.47444 0.740378 2.52687 0.7509 2.55159 0.761068 2.60824 0.770887 2.63196 0.780363 2.70327 0.789502 2.72661 0.798311 2.75016 0.806799 2.82516 0.814972 2.84943 0.822838 2.91856 0.830405 2.94406 0.837683 3.01576 0.844677 3.04225 0.851398 3.1166 0.857853 3.143 0.86405 3.22501 0.869999 3.25033 0.875705 3.33554 0.881179 3.35968 0.886428 3.44722 0.89146 3.47074 0.896281 3.5598 0.900901 3.58354 0.905326 3.68172 0.909563 3.70646 0.91362 3.80557 0.917503 3.83168 0.92122 3.93593 0.924775 3.96279 0.928177 4.07265 0.931431 4.09891 0.934542 4.20584 0.937517 4.23088 0.940362 4.3473 0.94308 4.37156 0.945679 4.49668 0.948162 4.52112 0.950534 4.61895 0.952801 4.70901 0.954966 4.73564 0.957034 4.82447 0.95901 4.85272 0.960896 4.91693 0.962697 4.94522 0.964417 5.02303 0.966059 5.05012 0.967626 5.13727 0.969123 5.25298 0.970551 5.27937 0.971914 5.46453 0.973215 5.49219 0.974456 5.71971 0.97564 5.74978 0.976771 5.93176 0.977849 6.09858 0.978878 6.12958 0.97986 6.32414 0.980796 6.35369 0.981689 6.49477 0.982542 6.62398 0.983354 6.65369 0.984129 6.80021 0.984869 6.83261 0.985574 6.96046 0.986247 6.99544 0.986888 7.08988 0.9875 7.17653 0.988083 7.21003 0.98864 7.30407 0.98917 7.33733 0.989676 7.40896 0.990158 7.47135 0.990618 7.50963 0.991057 7.5709 0.991475 7.61097 0.991873 7.66049 0.992253 7.70077 0.992616 7.73947 0.992961 7.78329 0.993291 7.82435 0.993605 7.86799