ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 Summary Report Surface Area Single point surface area at P/Po = 0.291361977: 3.8455 m²/g BET Surface Area: 3.9350 m²/g t-Plot External Surface Area: 4.5286 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å width: 2.617 m²/g BJH Desorption cumulative surface area of pores between 17.000 Å and 3000.000 Å width: 4.0837 m²/g Pore Volume Single point desorption total pore volume of pores less than 1036.230 Å width at P/Po = 0.980953071: 0.010115 cm³/g t-Plot micropore volume: -0.000162 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å width: 0.010075 cm³/g BJH Desorption cumulative volume of pores between 17.000 Å and 3000.000 Å width: 0.010811 cm³/g Pore Size Desorption average pore width (4V/A by BET): 102.8166 Å BJH Adsorption average pore width (4V/A): 153.964 Å BJH Desorption average pore width (4V/A): 105.896 Å Horvath-Kawazoe Maximum pore volume at P/Po = 0.010500365: 0.001032 cm³/g Median pore width: 7.502 Å ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 Isotherm Tabular Report Quantity Relative Absolute Adsorbed Elapsed Saturation Pressure Pressure (cm³/g Time Pressure (P/Po) (mmHg) STP) (h:min) (mmHg) ----- 1.#QNAN0000 1.#QNAN0 1.#QNB 00:53 758.474731 0.000003650 0.002766 0.0188 01:48 1.#QNAN0 0.000002589 0.001961 0.0393 02:29 1.#QNAN0 0.000004248 0.003215 0.0582 03:09 1.#QNAN0 0.000008405 0.006359 0.0740 03:50 1.#QNAN0 0.000018119 0.013706 0.0934 04:00 1.#QNAN0 0.000032507 0.024586 0.1119 04:11 1.#QNAN0 0.000051649 0.039058 0.1295 04:22 1.#QNAN0 0.000084977 0.064253 0.1522 04:31 1.#QNAN0 0.000126458 0.095603 0.1738 04:41 1.#QNAN0 0.000175701 0.132815 0.1943 04:50 1.#QNAN0 0.000214566 0.162172 0.2080 04:59 1.#QNAN0 0.000256517 0.193855 0.2210 05:08 1.#QNAN0 0.000301351 0.227707 0.2335 05:17 1.#QNAN0 0.000348876 0.263584 0.2455 05:26 1.#QNAN0 0.000398922 0.301360 0.2570 05:34 1.#QNAN0 0.000451195 0.340810 0.2680 05:42 1.#QNAN0 0.000505642 0.381887 0.2786 05:51 1.#QNAN0 0.000562150 0.424517 0.2888 05:59 1.#QNAN0 0.000620517 0.468540 0.2986 06:07 1.#QNAN0 0.000703493 0.531139 0.3116 06:14 1.#QNAN0 0.000786910 0.594060 0.3237 06:21 1.#QNAN0 0.000866718 0.654244 0.3344 06:28 1.#QNAN0 0.000943298 0.711969 0.3440 06:36 1.#QNAN0 0.001014707 0.765789 0.3525 06:43 1.#QNAN0 0.001082352 0.816758 0.3602 06:50 1.#QNAN0 0.001146620 0.865169 0.3671 06:57 1.#QNAN0 0.001205861 0.909777 0.3735 07:04 1.#QNAN0 0.001260052 0.950580 0.3791 07:10 1.#QNAN0 0.001311568 0.989345 0.3842 07:17 1.#QNAN0 0.001356672 1.023265 0.3885 07:24 1.#QNAN0 0.001400845 1.056476 0.3926 07:31 1.#QNAN0 0.001443173 1.088289 0.3964 07:38 1.#QNAN0 0.001482492 1.117828 0.3999 07:45 1.#QNAN0 0.001519455 1.145583 0.4031 07:52 1.#QNAN0 0.001553499 1.171133 0.4060 07:59 1.#QNAN0 0.001584492 1.194378 0.4085 08:06 1.#QNAN0 0.001614353 1.216782 0.4109 08:12 1.#QNAN0 0.001641804 1.237348 0.4131 08:19 1.#QNAN0 0.001666429 1.255781 0.4150 08:26 1.#QNAN0 0.001688980 1.272647 0.4167 08:33 1.#QNAN0 0.001765990 1.330541 0.4227 08:40 1.#QNAN0 0.001843556 1.388821 0.4286 08:48 1.#QNAN0 0.001922061 1.447817 0.4343 08:55 1.#QNAN0 0.002001504 1.507506 0.4399 09:02 1.#QNAN0 0.002081273 1.567407 0.4454 09:10 1.#QNAN0 0.002162176 1.628172 0.4507 09:17 1.#QNAN0 0.002243470 1.689218 0.4559 09:24 1.#QNAN0 0.002324956 1.750397 0.4609 09:31 1.#QNAN0 0.002407422 1.812301 0.4659 09:38 1.#QNAN0 0.002490269 1.874480 0.4707 09:45 1.#QNAN0 0.002573574 1.936962 0.4754 09:53 1.#QNAN0 0.002657869 2.000176 0.4801 10:01 1.#QNAN0 0.002742470 2.063635 0.4846 10:08 1.#QNAN0 0.002827754 2.127564 0.4890 10:16 1.#QNAN0 0.002913379 2.191735 0.4933 10:24 1.#QNAN0 0.002998961 2.255891 0.4976 10:31 1.#QNAN0 0.003085144 2.320486 0.5017 10:38 1.#QNAN0 0.003171953 2.385505 0.5057 10:46 1.#QNAN0 0.003258965 2.450697 0.5097 10:53 1.#QNAN0 0.003346858 2.516502 0.5135 11:01 1.#QNAN0 0.003435079 2.582575 0.5173 11:08 1.#QNAN0 0.003523767 2.648986 0.5210 11:15 1.#QNAN0 0.003612286 2.715179 0.5245 11:24 1.#QNAN0 0.003701659 2.782036 0.5281 11:32 1.#QNAN0 0.003791394 2.849190 0.5315 11:39 1.#QNAN0 0.003881702 2.916762 0.5349 11:46 1.#QNAN0 0.003971481 2.983880 0.5382 11:54 1.#QNAN0 0.004061989 3.051529 0.5414 12:02 1.#QNAN0 0.004152540 3.119241 0.5446 12:09 1.#QNAN0 0.004244444 3.187954 0.5477 12:16 1.#QNAN0 0.004335841 3.256273 0.5508 12:23 1.#QNAN0 0.004427601 3.324803 0.5537 12:31 1.#QNAN0 0.004519815 3.393658 0.5566 12:39 1.#QNAN0 0.004613092 3.463295 0.5595 12:47 1.#QNAN0 0.004706364 3.532913 0.5623 12:55 1.#QNAN0 0.004799776 3.602619 0.5650 13:03 1.#QNAN0 0.004893104 3.672246 0.5677 13:11 1.#QNAN0 0.004986243 3.741714 0.5703 13:19 1.#QNAN0 0.005080367 3.811906 0.5729 13:27 1.#QNAN0 0.005174292 3.881933 0.5754 13:35 1.#QNAN0 0.005268591 3.952223 0.5779 13:43 1.#QNAN0 0.005363999 4.023387 0.5803 13:50 1.#QNAN0 0.005458085 4.093486 0.5826 13:58 1.#QNAN0 0.005553003 4.164193 0.5848 14:06 1.#QNAN0 0.005648221 4.235108 0.5871 14:14 1.#QNAN0 0.005743474 4.306033 0.5893 14:22 1.#QNAN0 0.005839179 4.377281 0.5915 14:30 1.#QNAN0 0.005935612 4.449121 0.5936 14:37 1.#QNAN0 0.006030767 4.519925 0.5956 14:45 1.#QNAN0 0.006126270 4.591038 0.5976 14:52 1.#QNAN0 0.006222677 4.662747 0.5995 15:00 1.#QNAN0 0.006319815 4.734988 0.6015 15:08 1.#QNAN0 0.006417260 4.807441 0.6034 15:16 1.#QNAN0 0.006514815 4.880031 0.6053 15:23 1.#QNAN0 0.006612585 4.952694 0.6071 15:31 1.#QNAN0 0.006710002 5.025150 0.6088 15:38 1.#QNAN0 1.#QNAN0000 1.#QNAN0 1.#QNB 15:41 748.871948 0.007457731 5.584233 0.6234 15:49 1.#QNAN0 0.008221870 6.155869 0.6335 15:55 1.#QNAN0 0.008976293 6.720131 0.6458 16:01 1.#QNAN0 0.009741631 7.292465 0.6561 16:07 1.#QNAN0 0.010500365 7.860214 0.6674 16:09 1.#QNAN0 0.029753052 22.271467 0.7796 16:11 1.#QNAN0 0.057347716 42.926659 0.8652 16:12 1.#QNAN0 0.070266757 52.595451 0.8961 16:14 1.#QNAN0 0.090399380 67.663956 0.9401 16:15 1.#QNAN0 0.111008250 83.088486 0.9778 16:16 1.#QNAN0 0.130695271 97.821152 1.0123 16:18 1.#QNAN0 0.150683177 112.779800 1.0465 16:19 1.#QNAN0 0.170810545 127.842392 1.0775 16:20 1.#QNAN0 0.190939088 142.903336 1.1062 16:22 1.#QNAN0 0.211045193 157.948914 1.1338 16:23 1.#QNAN0 0.230968614 172.857330 1.1627 16:24 1.#QNAN0 0.251167518 187.968735 1.1897 16:26 1.#QNAN0 0.271473802 203.162582 1.2196 16:27 1.#QNAN0 0.291361977 218.043091 1.2466 16:28 1.#QNAN0 0.311637578 233.209686 1.2742 16:30 1.#QNAN0 0.331696291 248.216721 1.3016 16:31 1.#QNAN0 0.351590299 263.096222 1.3289 16:33 1.#QNAN0 0.372578307 278.797546 1.3596 16:34 1.#QNAN0 0.392640190 293.801117 1.3881 16:36 1.#QNAN0 0.412718790 308.820831 1.4181 16:37 1.#QNAN0 0.433408208 324.297150 1.4469 16:38 1.#QNAN0 0.453262297 339.143036 1.4753 16:40 1.#QNAN0 0.473299256 354.124878 1.5039 16:42 1.#QNAN0 0.493149444 368.971497 1.5328 16:43 1.#QNAN0 0.513520393 384.201691 1.5621 16:45 1.#QNAN0 0.533931761 399.467072 1.5928 16:46 1.#QNAN0 0.553950807 414.432434 1.6211 16:48 1.#QNAN0 0.573789760 429.268463 1.6519 16:49 1.#QNAN0 0.594244439 444.558197 1.6856 16:51 1.#QNAN0 0.614113854 459.415924 1.7201 16:52 1.#QNAN0 0.634571262 474.706146 1.7576 16:54 1.#QNAN0 0.654378048 489.515930 1.7960 16:55 1.#QNAN0 0.674723952 504.721191 1.8376 16:57 1.#QNAN0 0.694662133 519.628174 1.8854 16:58 1.#QNAN0 0.714701588 534.602661 1.9351 17:00 1.#QNAN0 0.734858687 549.672302 1.9923 17:01 1.#QNAN0 0.755032695 564.754150 2.0545 17:02 1.#QNAN0 0.774988589 579.663940 2.1274 17:04 1.#QNAN0 0.795432623 594.946655 2.2102 17:05 1.#QNAN0 0.815383061 609.859741 2.3064 17:06 1.#QNAN0 0.835576097 624.944702 2.4192 17:08 1.#QNAN0 0.855728506 640.007751 2.5554 17:09 1.#QNAN0 0.875840619 655.040222 2.7218 17:10 1.#QNAN0 0.895959154 670.067261 2.9303 17:12 1.#QNAN0 0.916094854 685.116272 3.2006 17:13 1.#QNAN0 0.936048710 700.018616 3.5679 17:15 1.#QNAN0 0.956017097 714.941406 4.1048 17:16 1.#QNAN0 0.975596408 729.562134 5.0476 17:18 1.#QNAN0 0.995117384 744.127502 7.2336 17:21 1.#QNAN0 0.980953071 733.514282 6.5390 17:23 1.#QNAN0 0.962798668 719.918152 5.4471 17:25 1.#QNAN0 0.941291757 703.816101 4.6291 17:27 1.#QNAN0 0.919691426 687.645142 4.1032 17:29 1.#QNAN0 0.898854903 672.056030 3.7380 17:30 1.#QNAN0 0.878309856 656.685303 3.4717 17:31 1.#QNAN0 0.857736016 641.284119 3.2547 17:33 1.#QNAN0 0.837546795 626.180542 3.0799 17:34 1.#QNAN0 0.817353472 611.074341 2.9279 17:35 1.#QNAN0 0.797144438 595.948120 2.7987 17:37 1.#QNAN0 0.776751085 580.693481 2.6868 17:38 1.#QNAN0 0.756666319 565.669983 2.5905 17:39 1.#QNAN0 0.736729964 550.749817 2.5057 17:41 1.#QNAN0 1.#QNAN0000 1.#QNAN0 1.#QNB 17:43 747.538086 0.716365668 535.510620 2.4245 17:45 1.#QNAN0 0.714096500 533.814331 2.4136 17:47 1.#QNAN0 0.693622474 518.509216 2.3475 17:48 1.#QNAN0 0.673933903 503.791260 2.2895 17:50 1.#QNAN0 0.653664364 488.639008 2.2356 17:51 1.#QNAN0 0.633604702 473.643646 2.1854 17:53 1.#QNAN0 0.613455350 458.581238 2.1399 17:54 1.#QNAN0 0.593343269 443.546692 2.0960 17:55 1.#QNAN0 0.573205715 428.493103 2.0527 17:57 1.#QNAN0 0.553270893 413.591064 2.0122 17:58 1.#QNAN0 0.533262751 398.634216 1.9744 18:00 1.#QNAN0 0.513030730 383.510010 1.9397 18:02 1.#QNAN0 0.493187354 368.676331 1.8761 18:04 1.#QNAN0 0.472374079 353.117615 1.6915 18:05 1.#QNAN0 0.451468419 337.489838 1.5456 18:06 1.#QNAN0 0.431589281 322.629425 1.4724 18:08 1.#QNAN0 0.411918795 307.924988 1.4262 18:09 1.#QNAN0 0.391698001 292.809174 1.3895 18:11 1.#QNAN0 0.371535788 277.737152 1.3556 18:12 1.#QNAN0 0.351450693 262.722778 1.3247 18:14 1.#QNAN0 0.331279540 247.644073 1.2940 18:15 1.#QNAN0 0.311164419 232.607254 1.2635 18:16 1.#QNAN0 0.291146255 217.642914 1.2340 18:17 1.#QNAN0 0.271110230 202.665222 1.2030 18:19 1.#QNAN0 0.251186145 187.771210 1.1722 18:20 1.#QNAN0 0.230987048 172.671616 1.1420 18:21 1.#QNAN0 0.210957392 157.698685 1.1134 18:23 1.#QNAN0 0.190869622 142.682312 1.0813 18:24 1.#QNAN0 0.170737804 127.633011 1.0492 18:26 1.#QNAN0 0.150713618 112.664169 1.0159 18:27 1.#QNAN0 0.130638238 97.657059 0.9825 18:29 1.#QNAN0 0.110568983 82.654526 0.9461 18:30 1.#QNAN0 0.090482132 67.638840 0.9053 18:32 1.#QNAN0 0.070421699 52.642902 0.8588 18:35 1.#QNAN0 0.050304440 37.604485 0.8080 18:36 1.#QNAN0 0.030523101 22.817181 0.7341 18:38 1.#QNAN0 0.010427848 7.795213 0.6037 18:41 1.#QNAN0 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 Isotherm Linear Plot 000-628 Cook 3FB-3-1 - Adsorption Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 3.64992e-006 0.0187699 2.58913e-006 0.0393232 4.24767e-006 0.0582452 8.40488e-006 0.0739597 1.8119e-005 0.0934065 3.2507e-005 0.111934 5.16491e-005 0.129501 8.49771e-005 0.152199 0.000126458 0.173793 0.000175701 0.194299 0.000214566 0.207972 0.000256517 0.221025 0.000301351 0.233518 0.000348876 0.245504 0.000398922 0.256976 0.000451195 0.267998 0.000505642 0.278586 0.00056215 0.288783 0.000620517 0.298617 0.000703493 0.311649 0.00078691 0.323686 0.000866718 0.334404 0.000943298 0.344024 0.00101471 0.352527 0.00108235 0.360187 0.00114662 0.367131 0.00120586 0.373482 0.00126005 0.379061 0.00131157 0.384164 0.00135667 0.388479 0.00140084 0.392622 0.00144317 0.396444 0.00148249 0.399911 0.00151945 0.403085 0.0015535 0.405963 0.00158449 0.408512 0.00161435 0.410942 0.0016418 0.413125 0.00166643 0.415028 0.00168898 0.416715 0.00176599 0.422745 0.00184356 0.428599 0.00192206 0.434317 0.0020015 0.439897 0.00208127 0.445355 0.00216218 0.450684 0.00224347 0.455886 0.00232496 0.460949 0.00240742 0.465902 0.00249027 0.470718 0.00257357 0.475438 0.00265787 0.480077 0.00274247 0.484575 0.00282775 0.489005 0.00291338 0.493349 0.00299896 0.497568 0.00308514 0.501702 0.00317195 0.505731 0.00325896 0.509673 0.00334686 0.513504 0.00343508 0.517274 0.00352377 0.520955 0.00361229 0.52453 0.00370166 0.528058 0.00379139 0.531534 0.0038817 0.534918 0.00397148 0.538204 0.00406199 0.54141 0.00415254 0.544565 0.00424444 0.547731 0.00433584 0.550781 0.0044276 0.553707 0.00451981 0.55663 0.00461309 0.5595 0.00470636 0.562295 0.00479978 0.565023 0.0048931 0.567708 0.00498624 0.570344 0.00508037 0.572906 0.00517429 0.575433 0.00526859 0.577861 0.005364 0.580253 0.00545809 0.582556 0.005553 0.584847 0.00564822 0.587092 0.00574347 0.58932 0.00583918 0.591465 0.00593561 0.593552 0.00603077 0.595572 0.00612627 0.597563 0.00622268 0.599534 0.00631982 0.601512 0.00641726 0.603421 0.00651482 0.605276 0.00661258 0.607085 0.00671 0.608836 0.00745773 0.623378 0.00822187 0.63352 0.00897629 0.645843 0.00974163 0.656112 0.0105004 0.667355 0.0297531 0.779559 0.0573477 0.865162 0.0702668 0.896066 0.0903994 0.940093 0.111008 0.977787 0.130695 1.0123 0.150683 1.04651 0.170811 1.07747 0.190939 1.10621 0.211045 1.13381 0.230969 1.16275 0.251168 1.18975 0.271474 1.21961 0.291362 1.24658 0.311638 1.27423 0.331696 1.30162 0.35159 1.32891 0.372578 1.35958 0.39264 1.38809 0.412719 1.41814 0.433408 1.44691 0.453262 1.47527 0.473299 1.50394 0.493149 1.53281 0.51352 1.56206 0.533932 1.59278 0.553951 1.62111 0.57379 1.65189 0.594244 1.68559 0.614114 1.72014 0.634571 1.75756 0.654378 1.796 0.674724 1.83762 0.694662 1.88539 0.714702 1.9351 0.734859 1.99227 0.755033 2.0545 0.774989 2.12739 0.795433 2.21018 0.815383 2.30636 0.835576 2.41917 0.855729 2.55541 0.875841 2.72179 0.895959 2.93035 0.916095 3.20059 0.936049 3.56791 0.956017 4.10478 0.975596 5.04761 0.995117 7.23359 000-628 Cook 3FB-3-1 - Desorption Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 0.995117 7.23359 0.980953 6.53904 0.962799 5.44708 0.941292 4.6291 0.919691 4.10321 0.898855 3.73803 0.87831 3.47171 0.857736 3.25472 0.837547 3.07995 0.817353 2.92787 0.797144 2.79867 0.776751 2.68677 0.756666 2.5905 0.73673 2.50566 0.716366 2.42445 0.714097 2.41365 0.693622 2.3475 0.673934 2.28953 0.653664 2.23557 0.633605 2.18536 0.613455 2.13994 0.593343 2.09601 0.573206 2.05273 0.553271 2.01221 0.533263 1.97439 0.513031 1.93969 0.493187 1.87608 0.472374 1.69154 0.451468 1.54563 0.431589 1.47238 0.411919 1.42624 0.391698 1.3895 0.371536 1.35563 0.351451 1.32468 0.33128 1.29396 0.311164 1.2635 0.291146 1.23405 0.27111 1.20297 0.251186 1.17216 0.230987 1.14204 0.210957 1.11345 0.19087 1.08132 0.170738 1.04923 0.150714 1.01592 0.130638 0.98246 0.110569 0.946103 0.0904821 0.90529 0.0704217 0.858815 0.0503044 0.808034 0.0305231 0.734094 0.0104278 0.603731 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 Isotherm Log Plot 000-628 Cook 3FB-3-1 - Adsorption Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 3.64992e-006 0.0187699 2.58913e-006 0.0393232 4.24767e-006 0.0582452 8.40488e-006 0.0739597 1.8119e-005 0.0934065 3.2507e-005 0.111934 5.16491e-005 0.129501 8.49771e-005 0.152199 0.000126458 0.173793 0.000175701 0.194299 0.000214566 0.207972 0.000256517 0.221025 0.000301351 0.233518 0.000348876 0.245504 0.000398922 0.256976 0.000451195 0.267998 0.000505642 0.278586 0.00056215 0.288783 0.000620517 0.298617 0.000703493 0.311649 0.00078691 0.323686 0.000866718 0.334404 0.000943298 0.344024 0.00101471 0.352527 0.00108235 0.360187 0.00114662 0.367131 0.00120586 0.373482 0.00126005 0.379061 0.00131157 0.384164 0.00135667 0.388479 0.00140084 0.392622 0.00144317 0.396444 0.00148249 0.399911 0.00151945 0.403085 0.0015535 0.405963 0.00158449 0.408512 0.00161435 0.410942 0.0016418 0.413125 0.00166643 0.415028 0.00168898 0.416715 0.00176599 0.422745 0.00184356 0.428599 0.00192206 0.434317 0.0020015 0.439897 0.00208127 0.445355 0.00216218 0.450684 0.00224347 0.455886 0.00232496 0.460949 0.00240742 0.465902 0.00249027 0.470718 0.00257357 0.475438 0.00265787 0.480077 0.00274247 0.484575 0.00282775 0.489005 0.00291338 0.493349 0.00299896 0.497568 0.00308514 0.501702 0.00317195 0.505731 0.00325896 0.509673 0.00334686 0.513504 0.00343508 0.517274 0.00352377 0.520955 0.00361229 0.52453 0.00370166 0.528058 0.00379139 0.531534 0.0038817 0.534918 0.00397148 0.538204 0.00406199 0.54141 0.00415254 0.544565 0.00424444 0.547731 0.00433584 0.550781 0.0044276 0.553707 0.00451981 0.55663 0.00461309 0.5595 0.00470636 0.562295 0.00479978 0.565023 0.0048931 0.567708 0.00498624 0.570344 0.00508037 0.572906 0.00517429 0.575433 0.00526859 0.577861 0.005364 0.580253 0.00545809 0.582556 0.005553 0.584847 0.00564822 0.587092 0.00574347 0.58932 0.00583918 0.591465 0.00593561 0.593552 0.00603077 0.595572 0.00612627 0.597563 0.00622268 0.599534 0.00631982 0.601512 0.00641726 0.603421 0.00651482 0.605276 0.00661258 0.607085 0.00671 0.608836 0.00745773 0.623378 0.00822187 0.63352 0.00897629 0.645843 0.00974163 0.656112 0.0105004 0.667355 0.0297531 0.779559 0.0573477 0.865162 0.0702668 0.896066 0.0903994 0.940093 0.111008 0.977787 0.130695 1.0123 0.150683 1.04651 0.170811 1.07747 0.190939 1.10621 0.211045 1.13381 0.230969 1.16275 0.251168 1.18975 0.271474 1.21961 0.291362 1.24658 0.311638 1.27423 0.331696 1.30162 0.35159 1.32891 0.372578 1.35958 0.39264 1.38809 0.412719 1.41814 0.433408 1.44691 0.453262 1.47527 0.473299 1.50394 0.493149 1.53281 0.51352 1.56206 0.533932 1.59278 0.553951 1.62111 0.57379 1.65189 0.594244 1.68559 0.614114 1.72014 0.634571 1.75756 0.654378 1.796 0.674724 1.83762 0.694662 1.88539 0.714702 1.9351 0.734859 1.99227 0.755033 2.0545 0.774989 2.12739 0.795433 2.21018 0.815383 2.30636 0.835576 2.41917 0.855729 2.55541 0.875841 2.72179 0.895959 2.93035 0.916095 3.20059 0.936049 3.56791 0.956017 4.10478 0.975596 5.04761 0.995117 7.23359 000-628 Cook 3FB-3-1 - Desorption Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 0.995117 7.23359 0.980953 6.53904 0.962799 5.44708 0.941292 4.6291 0.919691 4.10321 0.898855 3.73803 0.87831 3.47171 0.857736 3.25472 0.837547 3.07995 0.817353 2.92787 0.797144 2.79867 0.776751 2.68677 0.756666 2.5905 0.73673 2.50566 0.716366 2.42445 0.714097 2.41365 0.693622 2.3475 0.673934 2.28953 0.653664 2.23557 0.633605 2.18536 0.613455 2.13994 0.593343 2.09601 0.573206 2.05273 0.553271 2.01221 0.533263 1.97439 0.513031 1.93969 0.493187 1.87608 0.472374 1.69154 0.451468 1.54563 0.431589 1.47238 0.411919 1.42624 0.391698 1.3895 0.371536 1.35563 0.351451 1.32468 0.33128 1.29396 0.311164 1.2635 0.291146 1.23405 0.27111 1.20297 0.251186 1.17216 0.230987 1.14204 0.210957 1.11345 0.19087 1.08132 0.170738 1.04923 0.150714 1.01592 0.130638 0.98246 0.110569 0.946103 0.0904821 0.90529 0.0704217 0.858815 0.0503044 0.808034 0.0305231 0.734094 0.0104278 0.603731 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 BET Surface Area Report BET Surface Area: 3.9350 ± 0.0259 m²/g Slope: 1.100966 ± 0.007152 g/cm³ STP Y-Intercept: 0.005311 ± 0.001336 g/cm³ STP C: 208.308471 Qm: 0.9039 cm³/g STP Correlation Coefficient: 0.9997680 Molecular Cross-Sectional Area: 0.1620 nm² Quantity Relative Adsorbed Pressure (cm³/g 1/[Q(Po/P (P/Po) STP) - 1)] --- 0.057347716 0.8652 0.070318 0.070266757 0.8961 0.084343 0.090399380 0.9401 0.105717 0.111008250 0.9778 0.127707 0.130695271 1.0123 0.148518 0.150683177 1.0465 0.169532 0.170810545 1.0775 0.191185 0.190939088 1.1062 0.213342 0.211045193 1.1338 0.235930 0.230968614 1.1627 0.258299 0.251167518 1.1897 0.281919 0.271473802 1.2196 0.305536 0.291361977 1.2466 0.329830 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 BET Surface Area Plot 000-628 Cook 3FB-3-1 Relative Pressure (P/Po) 1/[Q(Po/P - 1)] 0.0573477 0.0703181 0.0702668 0.0843435 0.0903994 0.105717 0.111008 0.127707 0.130695 0.148518 0.150683 0.169532 0.170811 0.191185 0.190939 0.213342 0.211045 0.23593 0.230969 0.258299 0.251168 0.281919 0.271474 0.305536 0.291362 0.32983 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 t-Plot Report Micropore Volume: -0.000162 cm³/g Micropore Area: * External Surface Area: 4.5286 m²/g Slope: 0.292775 ± 0.007682 cm³/g·Å STP Y-Intercept: -0.104916 ± 0.023177 cm³/g STP Correlation Coefficient: 0.998969 Surface Area Correction Factor: 1.000 Density Conversion Factor: 0.0015468 Total Surface Area (BET): 3.9350 m²/g Thickness Range: 2.6000 Å to 3.5000 Å Thickness Equation: Harkins and Jura t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 Quantity Relative Statistical Adsorbed Pressure Thickness (cm³/g (P/Po) (Å) STP) --- 0.000003650 1.5990 0.0188 0.000002589 1.5776 0.0393 0.000004248 1.6087 0.0582 0.000008405 1.6547 0.0740 0.000018119 1.7115 0.0934 0.000032507 1.7589 0.1119 0.000051649 1.7994 0.1295 0.000084977 1.8462 0.1522 0.000126458 1.8862 0.1738 0.000175701 1.9215 0.1943 0.000214566 1.9439 0.2080 0.000256517 1.9645 0.2210 0.000301351 1.9838 0.2335 0.000348876 2.0018 0.2455 0.000398922 2.0187 0.2570 0.000451195 2.0346 0.2680 0.000505642 2.0496 0.2786 0.000562150 2.0639 0.2888 0.000620517 2.0776 0.2986 0.000703493 2.0952 0.3116 0.000786910 2.1114 0.3237 0.000866718 2.1257 0.3344 0.000943298 2.1384 0.3440 0.001014707 2.1496 0.3525 0.001082352 2.1596 0.3602 0.001146620 2.1687 0.3671 0.001205861 2.1767 0.3735 0.001260052 2.1838 0.3791 0.001311568 2.1903 0.3842 0.001356672 2.1958 0.3885 0.001400845 2.2011 0.3926 0.001443173 2.2060 0.3964 0.001482492 2.2105 0.3999 0.001519455 2.2147 0.4031 0.001553499 2.2184 0.4060 0.001584492 2.2218 0.4085 0.001614353 2.2250 0.4109 0.001641804 2.2279 0.4131 0.001666429 2.2304 0.4150 0.001688980 2.2327 0.4167 0.001765990 2.2405 0.4227 0.001843556 2.2480 0.4286 0.001922061 2.2554 0.4343 0.002001504 2.2626 0.4399 0.002081273 2.2697 0.4454 0.002162176 2.2767 0.4507 0.002243470 2.2835 0.4559 0.002324956 2.2901 0.4609 0.002407422 2.2966 0.4659 0.002490269 2.3030 0.4707 0.002573574 2.3093 0.4754 0.002657869 2.3154 0.4801 0.002742470 2.3215 0.4846 0.002827754 2.3275 0.4890 0.002913379 2.3333 0.4933 0.002998961 2.3391 0.4976 0.003085144 2.3447 0.5017 0.003171953 2.3503 0.5057 0.003258965 2.3558 0.5097 0.003346858 2.3612 0.5135 0.003435079 2.3665 0.5173 0.003523767 2.3718 0.5210 0.003612286 2.3769 0.5245 0.003701659 2.3820 0.5281 0.003791394 2.3871 0.5315 0.003881702 2.3921 0.5349 0.003971481 2.3969 0.5382 0.004061989 2.4018 0.5414 0.004152540 2.4065 0.5446 0.004244444 2.4113 0.5477 0.004335841 2.4159 0.5508 0.004427601 2.4205 0.5537 0.004519815 2.4251 0.5566 0.004613092 2.4296 0.5595 0.004706364 2.4341 0.5623 0.004799776 2.4385 0.5650 0.004893104 2.4428 0.5677 0.004986243 2.4471 0.5703 0.005080367 2.4514 0.5729 0.005174292 2.4556 0.5754 0.005268591 2.4597 0.5779 0.005363999 2.4639 0.5803 0.005458085 2.4679 0.5826 0.005553003 2.4720 0.5848 0.005648221 2.4760 0.5871 0.005743474 2.4799 0.5893 0.005839179 2.4838 0.5915 0.005935612 2.4877 0.5936 0.006030767 2.4915 0.5956 0.006126270 2.4953 0.5976 0.006222677 2.4991 0.5995 0.006319815 2.5029 0.6015 0.006417260 2.5066 0.6034 0.006514815 2.5103 0.6053 0.006612585 2.5139 0.6071 0.006710002 2.5176 0.6088 0.007457731 2.5441 0.6234 0.008221870 2.5695 0.6335 0.008976293 2.5929 0.6458 0.009741631 2.6153 0.6561 0.010500365 2.6364 0.6674 0.029753052 2.9942 0.7796 0.057347716 3.3119 0.8652 0.070266757 3.4327 0.8961 0.090399380 3.6027 0.9401 0.111008250 3.7617 0.9778 0.130695271 3.9044 1.0123 0.150683177 4.0429 1.0465 0.170810545 4.1779 1.0775 0.190939088 4.3100 1.1062 0.211045193 4.4401 1.1338 0.230968614 4.5680 1.1627 0.251167518 4.6973 1.1897 0.271473802 4.8276 1.2196 0.291361977 4.9561 1.2466 0.311637578 5.0883 1.2742 0.331696291 5.2208 1.3016 0.351590299 5.3545 1.3289 0.372578307 5.4982 1.3596 0.392640190 5.6387 1.3881 0.412718790 5.7828 1.4181 0.433408208 5.9355 1.4469 0.453262297 6.0864 1.4753 0.473299256 6.2437 1.5039 0.493149444 6.4050 1.5328 0.513520393 6.5767 1.5621 0.533931761 6.7559 1.5928 0.553950807 6.9393 1.6211 0.573789760 7.1293 1.6519 0.594244439 7.3349 1.6856 * The micropore area is not reported because either the micropore volume is negative or the calculated external surface area is larger than the total surface area. ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 t-Plot Harkins and Jura 000-628 Cook 3FB-3-1 Thickness (Å) Quantity Adsorbed (cm³/g STP) 2.61531 0.656112 2.63639 0.667355 2.9942 0.779559 3.31186 0.865162 3.43272 0.896066 Not Fitted Points Thickness (Å) Quantity Adsorbed (cm³/g STP) 1.59899 0.0187699 1.57764 0.0393232 1.60871 0.0582452 1.65471 0.0739597 1.71152 0.0934065 1.75891 0.111934 1.79937 0.129501 1.84616 0.152199 1.88625 0.173793 1.92147 0.194299 1.94386 0.207972 1.96454 0.221025 1.98378 0.233518 2.00177 0.245504 2.01867 0.256976 2.03458 0.267998 2.04963 0.278586 2.06394 0.288783 2.07756 0.298617 2.09525 0.311649 2.11143 0.323686 2.12569 0.334404 2.13843 0.344024 2.14959 0.352527 2.15961 0.360187 2.16868 0.367131 2.1767 0.373482 2.18377 0.379061 2.19028 0.384164 2.19581 0.388479 2.2011 0.392622 2.20604 0.396444 2.21054 0.399911 2.21468 0.403085 2.21842 0.405963 2.22178 0.408512 2.22496 0.410942 2.22785 0.413125 2.23041 0.415028 2.23273 0.416715 2.24047 0.422745 2.24801 0.428599 2.2554 0.434317 2.26265 0.439897 2.26971 0.445355 2.27666 0.450684 2.28345 0.455886 2.29007 0.460949 2.2966 0.465902 2.30299 0.470718 2.30925 0.475438 2.31544 0.480077 2.3215 0.484575 2.32747 0.489005 2.33333 0.493349 2.33906 0.497568 2.34471 0.501702 2.35028 0.505731 2.35575 0.509673 2.36117 0.513504 2.3665 0.517274 2.37176 0.520955 2.37692 0.52453 2.38203 0.528058 2.38707 0.531534 2.39206 0.534918 2.39693 0.538204 2.40176 0.54141 2.40652 0.544565 2.41126 0.547731 2.41591 0.550781 2.42051 0.553707 2.42506 0.55663 2.4296 0.5595 2.43406 0.562295 2.43847 0.565023 2.44282 0.567708 2.4471 0.570344 2.45136 0.572906 2.45556 0.575433 2.45972 0.577861 2.46388 0.580253 2.46793 0.582556 2.47196 0.584847 2.47595 0.587092 2.4799 0.58932 2.48383 0.591465 2.48773 0.593552 2.49154 0.595572 2.49532 0.597563 2.49909 0.599534 2.50286 0.601512 2.50659 0.603421 2.51028 0.605276 2.51395 0.607085 2.51756 0.608836 2.54415 0.623378 2.56945 0.63352 2.59288 0.645843 3.60274 0.940093 3.76174 0.977787 3.90435 1.0123 4.04286 1.04651 4.17793 1.07747 4.31004 1.10621 4.44012 1.13381 4.56801 1.16275 4.69734 1.18975 4.82764 1.21961 4.95606 1.24658 5.08828 1.27423 5.22084 1.30162 5.35446 1.32891 5.4982 1.35958 5.63871 1.38809 5.78284 1.41814 5.9355 1.44691 6.08645 1.47527 6.24373 1.50394 6.40498 1.53281 6.57674 1.56206 6.7559 1.59278 6.93928 1.62111 7.12931 1.65189 7.33488 1.68559 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 BJH Adsorption Pore Distribution Report Faas Correction Halsey t = 3.54 [ -5 / ln(P/Po) ] ^ 0.333 Width Range: 17.000 Å to 3000.000 Å Adsorbate Property Factor: 9.53000 Å Density Conversion Factor: 0.0015468 Fraction of Pores Open at Both Ends: 0.00 Incremental Cumulative Cumulative Average Pore Pore Incremental Pore Width Volume Volume Pore Area Area Pore Width Range (Å) (Å) (cm³/g) (cm³/g) (m²/g) (m²/g) ------ 3960.0 - 807.7 927.6 0.003662 0.003662 0.158 0.158 807.7 - 452.5 535.1 0.001565 0.005227 0.117 0.275 452.5 - 313.1 357.3 0.000896 0.006122 0.100 0.375 313.1 - 239.5 266.2 0.000618 0.006740 0.093 0.468 239.5 - 193.5 211.4 0.000456 0.007196 0.086 0.554 193.5 - 162.2 175.0 0.000353 0.007549 0.081 0.635 162.2 - 139.6 149.1 0.000281 0.007830 0.075 0.710 139.6 - 122.3 129.7 0.000230 0.008060 0.071 0.781 122.3 - 108.7 114.6 0.000189 0.008248 0.066 0.847 108.7 - 97.8 102.6 0.000160 0.008409 0.063 0.910 97.8 - 88.6 92.7 0.000136 0.008545 0.059 0.968 88.6 - 81.0 84.5 0.000120 0.008665 0.057 1.025 81.0 - 74.5 77.5 0.000100 0.008764 0.051 1.076 74.5 - 68.9 71.5 0.000091 0.008855 0.051 1.127 68.9 - 64.0 66.3 0.000078 0.008933 0.047 1.174 64.0 - 59.7 61.7 0.000076 0.009009 0.049 1.223 59.7 - 55.8 57.6 0.000063 0.009071 0.044 1.267 55.8 - 52.4 54.0 0.000058 0.009130 0.043 1.310 52.4 - 49.2 50.7 0.000056 0.009186 0.044 1.355 49.2 - 46.4 47.7 0.000052 0.009238 0.044 1.398 46.4 - 43.8 45.0 0.000050 0.009288 0.045 1.443 43.8 - 41.4 42.5 0.000045 0.009334 0.043 1.485 41.4 - 39.3 40.3 0.000040 0.009374 0.040 1.525 39.3 - 37.2 38.2 0.000046 0.009420 0.049 1.574 37.2 - 35.3 36.2 0.000044 0.009464 0.048 1.622 35.3 - 33.6 34.4 0.000044 0.009508 0.052 1.674 33.6 - 31.9 32.7 0.000044 0.009552 0.054 1.727 31.9 - 30.4 31.1 0.000044 0.009596 0.057 1.784 30.4 - 28.9 29.6 0.000044 0.009640 0.060 1.844 28.9 - 27.5 28.2 0.000049 0.009690 0.070 1.914 27.5 - 26.2 26.8 0.000045 0.009735 0.067 1.981 26.2 - 24.9 25.5 0.000050 0.009784 0.078 2.059 24.9 - 23.7 24.3 0.000042 0.009826 0.069 2.128 23.7 - 22.6 23.1 0.000042 0.009868 0.072 2.199 22.6 - 21.5 22.0 0.000042 0.009909 0.075 2.275 21.5 - 20.4 20.9 0.000040 0.009949 0.076 2.351 20.4 - 19.4 19.9 0.000047 0.009995 0.094 2.445 19.4 - 18.4 18.9 0.000037 0.010032 0.078 2.523 18.4 - 17.4 17.9 0.000042 0.010075 0.094 2.617 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 BJH Adsorption dV/dw Pore Volume Halsey : Faas Correction 000-628 Cook 3FB-3-1 Pore Width (Å) Pore Volume (cm³/g·Å) 927.648 1.16164e-006 535.108 4.40504e-006 357.313 6.42386e-006 266.2 8.39344e-006 211.401 9.92201e-006 174.983 1.12882e-005 149.097 1.24023e-005 129.713 1.32923e-005 114.627 1.38654e-005 102.625 1.47469e-005 92.7106 1.47683e-005 84.4593 1.58633e-005 77.4908 1.52625e-005 71.4709 1.62403e-005 66.2522 1.58381e-005 61.688 1.76079e-005 57.6043 1.60753e-005 53.9745 1.70616e-005 50.6907 1.77515e-005 47.7206 1.85488e-005 45.0099 1.91136e-005 42.5365 1.93446e-005 40.2814 1.83072e-005 38.1666 2.26028e-005 36.1903 2.28834e-005 34.377 2.55514e-005 32.6928 2.68733e-005 31.1127 2.88683e-005 29.5977 2.95013e-005 28.1636 3.57315e-005 26.8242 3.45176e-005 25.5201 3.81558e-005 24.2875 3.5517e-005 23.132 3.65532e-005 22.0117 3.7582e-005 20.9384 3.79469e-005 19.8978 4.51507e-005 18.8811 3.70118e-005 17.8996 4.38533e-005 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 BJH Adsorption dV/dw Pore Volume Halsey : Faas Correction 000-628 Cook 3FB-3-1 Pore Width (Å) Pore Volume (cm³/g·Å) 927.648 1.16164e-006 535.108 4.40504e-006 357.313 6.42386e-006 266.2 8.39344e-006 211.401 9.92201e-006 174.983 1.12882e-005 149.097 1.24023e-005 129.713 1.32923e-005 114.627 1.38654e-005 102.625 1.47469e-005 92.7106 1.47683e-005 84.4593 1.58633e-005 77.4908 1.52625e-005 71.4709 1.62403e-005 66.2522 1.58381e-005 61.688 1.76079e-005 57.6043 1.60753e-005 53.9745 1.70616e-005 50.6907 1.77515e-005 47.7206 1.85488e-005 45.0099 1.91136e-005 42.5365 1.93446e-005 40.2814 1.83072e-005 38.1666 2.26028e-005 36.1903 2.28834e-005 34.377 2.55514e-005 32.6928 2.68733e-005 31.1127 2.88683e-005 29.5977 2.95013e-005 28.1636 3.57315e-005 26.8242 3.45176e-005 25.5201 3.81558e-005 24.2875 3.5517e-005 23.132 3.65532e-005 22.0117 3.7582e-005 20.9384 3.79469e-005 19.8978 4.51507e-005 18.8811 3.70118e-005 17.8996 4.38533e-005 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 BJH Adsorption dV/dlog(w) Pore Volume Halsey : Faas Correction 000-628 Cook 3FB-3-1 Pore Width (Å) dV/dlog(w) Pore Volume (cm³/g·Å) 927.648 0.00530359 535.108 0.00621804 357.313 0.00559857 266.2 0.0053074 211.401 0.00492698 174.983 0.00461106 149.097 0.00430106 129.713 0.00400126 114.627 0.00368264 102.625 0.00350231 92.7106 0.00316666 84.4593 0.00309618 77.4908 0.00273204 71.4709 0.00268019 66.2522 0.00242215 61.688 0.00250662 57.6043 0.0021367 53.9745 0.00212433 50.6907 0.00207569 47.7206 0.00204139 45.0099 0.00198405 42.5365 0.00189735 40.2814 0.00170032 38.1666 0.00198904 36.1903 0.00190935 34.377 0.00202493 32.6928 0.00202532 31.1127 0.00207042 29.5977 0.00201294 28.1636 0.00231971 26.8242 0.00213431 25.5201 0.00224479 24.2875 0.00198839 23.132 0.0019491 22.0117 0.00190699 20.9384 0.00183159 19.8978 0.00207118 18.8811 0.00161114 17.8996 0.00180979 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 BJH Adsorption Cumulative Pore Area Halsey : Faas Correction 000-628 Cook 3FB-3-1 Pore Width (Å) Pore Area (m²/g) 807.706 0.157897 452.487 0.274864 313.055 0.375134 239.461 0.467953 193.488 0.554261 162.236 0.634905 139.557 0.710363 122.287 0.781154 108.677 0.847005 97.8 0.909522 88.5965 0.968165 81.0457 1.02489 74.5256 1.07626 68.8945 1.12744 64.0004 1.17424 59.7001 1.22334 55.7955 1.26693 52.3873 1.31002 49.2105 1.35452 46.4097 1.39807 43.7778 1.44277 41.4359 1.48537 39.2557 1.52501 37.1985 1.57374 35.2917 1.62197 33.5578 1.67352 31.9177 1.72744 30.3896 1.78416 28.8887 1.844 27.5118 1.91388 26.2058 1.98109 24.9063 2.05881 23.7305 2.12759 22.594 2.19943 21.4894 2.27487 20.4437 2.35067 19.4096 2.44453 18.4093 2.52296 17.4453 2.61744 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 BJH Adsorption dA/dw Pore Area Halsey : Faas Correction 000-628 Cook 3FB-3-1 Pore Width (Å) Pore Area (m²/g·Å) 927.648 5.00896e-005 535.108 0.000329282 357.313 0.000719129 266.2 0.00126122 211.401 0.00187738 174.983 0.00258041 149.097 0.00332729 129.713 0.00409898 114.627 0.00483846 102.625 0.00574785 92.7106 0.00637181 84.4593 0.00751287 77.4908 0.00787836 71.4709 0.00908915 66.2522 0.00956231 61.688 0.0114174 57.6043 0.0111626 53.9745 0.0126442 50.6907 0.0140077 47.7206 0.0155478 45.0099 0.0169861 42.5365 0.0181911 40.2814 0.0181793 38.1666 0.0236885 36.1903 0.0252923 34.377 0.0297308 32.6928 0.0328797 31.1127 0.0371145 29.5977 0.0398698 28.1636 0.0507486 26.8242 0.0514723 25.5201 0.059805 24.2875 0.0584943 23.132 0.063208 22.0117 0.0682946 20.9384 0.0724925 19.8978 0.0907653 18.8811 0.0784104 17.8996 0.0979984 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 BJH Adsorption dA/dlog(w) Pore Area Halsey : Faas Correction 000-628 Cook 3FB-3-1 Pore Width (Å) dA/dlog(w) Pore Area (m²/g·Å) 927.648 0.22869 535.108 0.464806 357.313 0.626742 266.2 0.797505 211.401 0.932253 174.983 1.05406 149.097 1.15389 129.713 1.23388 114.627 1.28509 102.625 1.36509 92.7106 1.36626 84.4593 1.46635 77.4908 1.41025 71.4709 1.50002 66.2522 1.46238 61.688 1.62536 57.6043 1.48371 53.9745 1.57432 50.6907 1.63793 47.7206 1.71112 45.0099 1.76321 42.5365 1.7842 40.2814 1.68844 38.1666 2.08459 36.1903 2.11034 34.377 2.35614 32.6928 2.478 31.1127 2.66183 29.5977 2.7204 28.1636 3.29463 26.8242 3.18266 25.5201 3.51847 24.2875 3.27476 23.132 3.3704 22.0117 3.46542 20.9384 3.49901 19.8978 4.16364 18.8811 3.41324 17.8996 4.04432 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 BJH Desorption Pore Distribution Report Faas Correction Halsey t = 3.54 [ -5 / ln(P/Po) ] ^ 0.333 Width Range: 17.000 Å to 3000.000 Å Adsorbate Property Factor: 9.53000 Å Density Conversion Factor: 0.0015468 Fraction of Pores Open at Both Ends: 0.00 Incremental Cumulative Cumulative Average Pore Pore Incremental Pore Width Volume Volume Pore Area Area Pore Width Range (Å) (Å) (cm³/g) (cm³/g) (m²/g) (m²/g) ------ 3961.8 - 1032.8 1212.0 0.001152 0.001152 0.038 0.038 1032.8 - 535.3 637.5 0.001857 0.003009 0.117 0.155 535.3 - 342.4 397.0 0.001415 0.004425 0.143 0.297 342.4 - 251.9 283.0 0.000919 0.005344 0.130 0.427 251.9 - 200.8 220.3 0.000644 0.005988 0.117 0.544 200.8 - 167.4 180.9 0.000471 0.006460 0.104 0.648 167.4 - 143.4 153.4 0.000387 0.006847 0.101 0.749 143.4 - 125.6 133.2 0.000313 0.007159 0.094 0.843 125.6 - 111.7 117.8 0.000274 0.007434 0.093 0.936 111.7 - 100.5 105.4 0.000233 0.007666 0.088 1.024 100.5 - 91.2 95.3 0.000201 0.007867 0.084 1.109 91.2 - 83.4 86.9 0.000172 0.008039 0.079 1.188 83.4 - 76.9 79.9 0.000151 0.008190 0.076 1.263 76.9 - 71.2 73.8 0.000146 0.008336 0.079 1.343 71.2 - 70.6 70.9 0.000021 0.008357 0.012 1.354 70.6 - 65.6 67.9 0.000114 0.008471 0.067 1.422 65.6 - 61.4 63.3 0.000099 0.008570 0.063 1.484 61.4 - 57.5 59.3 0.000091 0.008661 0.061 1.546 57.5 - 54.1 55.7 0.000085 0.008746 0.061 1.607 54.1 - 50.9 52.4 0.000075 0.008821 0.057 1.664 50.9 - 48.1 49.4 0.000073 0.008895 0.059 1.723 48.1 - 45.5 46.7 0.000074 0.008968 0.063 1.786 45.5 - 43.2 44.3 0.000069 0.009037 0.062 1.848 43.2 - 41.0 42.0 0.000063 0.009100 0.060 1.908 41.0 - 39.0 39.9 0.000055 0.009155 0.055 1.963 39.0 - 37.1 38.0 0.000141 0.009295 0.148 2.111 37.1 - 35.3 36.2 0.000494 0.009789 0.547 2.658 35.3 - 33.6 34.4 0.000379 0.010169 0.441 3.099 33.6 - 32.1 32.8 0.000162 0.010331 0.198 3.296 32.1 - 30.7 31.3 0.000080 0.010411 0.102 3.398 30.7 - 29.3 29.9 0.000049 0.010460 0.066 3.464 29.3 - 28.0 28.6 0.000041 0.010502 0.058 3.522 28.0 - 26.7 27.3 0.000033 0.010534 0.048 3.570 26.7 - 25.5 26.1 0.000032 0.010567 0.050 3.620 25.5 - 24.4 24.9 0.000032 0.010599 0.051 3.671 24.4 - 23.3 23.8 0.000029 0.010628 0.049 3.720 23.3 - 22.3 22.8 0.000034 0.010662 0.061 3.781 22.3 - 21.2 21.7 0.000033 0.010696 0.062 3.842 21.2 - 20.2 20.7 0.000029 0.010725 0.056 3.898 20.2 - 19.3 19.7 0.000022 0.010747 0.045 3.944 19.3 - 18.3 18.8 0.000034 0.010781 0.072 4.015 18.3 - 17.4 17.8 0.000030 0.010811 0.068 4.084 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 BJH Desorption Cumulative Pore Volume Halsey : Faas Correction BJH Desorption Cumulative Pore Volume Pore Width (Å) Pore Volume (cm³/g) 1032.81 0.00115223 535.317 0.00300931 342.403 0.0044246 251.888 0.0053441 200.82 0.00598849 167.356 0.00645987 143.369 0.00684686 125.621 0.00715945 111.706 0.00743355 100.482 0.00766612 91.1563 0.00786685 83.4495 0.00803891 76.9205 0.00818998 71.161 0.00833606 70.5677 0.0083568 65.5936 0.00847087 61.3704 0.00857017 57.4969 0.00866131 54.0603 0.00874622 50.9439 0.00882112 48.1191 0.00889452 45.5365 0.00896827 43.1894 0.00903686 41.0162 0.00909957 38.9815 0.00915456 37.1256 0.00929522 35.3102 0.00978949 33.6063 0.0101687 32.0845 0.0103308 30.6629 0.0104107 29.2794 0.0104601 27.9702 0.0105015 26.7283 0.0105344 25.5369 0.0105668 24.3982 0.0105988 23.3083 0.0106279 22.2554 0.0106624 21.241 0.0106958 20.2407 0.0107246 19.2716 0.010747 18.317 0.0107807 17.3719 0.0108112 BJH Desorption dV/dw Pore Volume Pore Width (Å) Pore Volume (cm³/g·Å) 1211.96 3.93385e-007 637.502 3.73288e-006 396.965 7.33641e-006 283.023 1.01585e-005 220.335 1.26182e-005 180.871 1.40859e-005 153.387 1.61339e-005 133.236 1.76133e-005 117.781 1.96973e-005 105.448 2.07211e-005 95.3229 2.1524e-005 86.929 2.23255e-005 79.8915 2.31386e-005 73.7924 2.53632e-005 70.8616 3.49598e-005 67.8783 2.29329e-005 63.325 2.35136e-005 59.2921 2.35267e-005 55.6594 2.47095e-005 52.3977 2.40337e-005 49.4403 2.59857e-005 46.7469 2.85563e-005 44.2922 2.92199e-005 42.0388 2.88594e-005 39.9396 2.70235e-005 38.0016 7.57938e-005 36.1655 0.000272266 34.4096 0.000222567 32.8046 0.000106533 31.3364 5.61672e-005 29.9341 3.57375e-005 28.59 3.16119e-005 27.3164 2.64686e-005 26.1009 2.71781e-005 24.9371 2.81502e-005 23.8241 2.6642e-005 22.7533 3.27668e-005 21.7204 3.29415e-005 20.7125 2.88205e-005 19.7281 2.31186e-005 18.7657 3.53218e-005 17.8149 3.21839e-005 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 BJH Desorption dV/dw Pore Volume Halsey : Faas Correction 000-628 Cook 3FB-3-1 Pore Width (Å) Pore Volume (cm³/g·Å) 1211.96 3.93385e-007 637.502 3.73288e-006 396.965 7.33641e-006 283.023 1.01585e-005 220.335 1.26182e-005 180.871 1.40859e-005 153.387 1.61339e-005 133.236 1.76133e-005 117.781 1.96973e-005 105.448 2.07211e-005 95.3229 2.1524e-005 86.929 2.23255e-005 79.8915 2.31386e-005 73.7924 2.53632e-005 70.8616 3.49598e-005 67.8783 2.29329e-005 63.325 2.35136e-005 59.2921 2.35267e-005 55.6594 2.47095e-005 52.3977 2.40337e-005 49.4403 2.59857e-005 46.7469 2.85563e-005 44.2922 2.92199e-005 42.0388 2.88594e-005 39.9396 2.70235e-005 38.0016 7.57938e-005 36.1655 0.000272266 34.4096 0.000222567 32.8046 0.000106533 31.3364 5.61672e-005 29.9341 3.57375e-005 28.59 3.16119e-005 27.3164 2.64686e-005 26.1009 2.71781e-005 24.9371 2.81502e-005 23.8241 2.6642e-005 22.7533 3.27668e-005 21.7204 3.29415e-005 20.7125 2.88205e-005 19.7281 2.31186e-005 18.7657 3.53218e-005 17.8149 3.21839e-005 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 BJH Desorption dV/dlog(w) Pore Volume Halsey : Faas Correction 000-628 Cook 3FB-3-1 Pore Width (Å) dV/dlog(w) Pore Volume (cm³/g·Å) 1211.96 0.00197342 637.502 0.00650672 396.965 0.00729258 283.023 0.00689642 220.335 0.00654859 180.871 0.00595421 153.387 0.00576016 133.236 0.00544667 117.781 0.00537579 105.448 0.00505725 95.3229 0.00474513 86.929 0.00448501 79.8915 0.00426978 73.7924 0.00432187 70.8616 0.0057044 67.8783 0.0035934 63.325 0.00343578 59.2921 0.00321851 55.6594 0.00317256 52.3977 0.00290459 49.4403 0.00296288 46.7469 0.00307831 44.2922 0.0029841 42.0388 0.00279716 39.9396 0.00248835 38.0016 0.00663985 36.1655 0.0227008 34.4096 0.0176556 32.8046 0.00805557 31.3364 0.00405686 29.9341 0.00246585 28.59 0.00208321 27.3164 0.00166655 26.1009 0.00163509 24.9371 0.00161807 23.8241 0.00146303 22.7533 0.00171855 21.7204 0.00164932 20.7125 0.00137613 19.7281 0.00105146 18.7657 0.00152824 17.8149 0.00132207 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 BJH Desorption Cumulative Pore Area Halsey : Faas Correction 000-628 Cook 3FB-3-1 Pore Width (Å) Pore Area (m²/g) 1032.81 0.0380288 535.317 0.154551 342.403 0.297162 251.888 0.427117 200.82 0.5441 167.356 0.648346 143.369 0.749266 125.621 0.843112 111.706 0.936197 100.482 1.02442 91.1563 1.10865 83.4495 1.18782 76.9205 1.26346 71.161 1.34265 70.5677 1.35435 65.5936 1.42158 61.3704 1.4843 57.4969 1.54578 54.0603 1.60681 50.9439 1.66398 48.1191 1.72337 45.5365 1.78648 43.1894 1.84841 41.0162 1.90809 38.9815 1.96316 37.1256 2.11122 35.3102 2.65789 33.6063 3.09874 32.0845 3.29642 30.6629 3.39834 29.2794 3.46441 27.9702 3.52231 26.7283 3.57045 25.5369 3.62007 24.3982 3.67149 23.3083 3.72024 22.2554 3.78089 21.241 3.84243 20.2407 3.89811 19.2716 3.94353 18.317 4.0154 17.3719 4.0837 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 BJH Desorption dA/dw Pore Area Halsey : Faas Correction 000-628 Cook 3FB-3-1 Pore Width (Å) Pore Area (m²/g·Å) 1211.96 1.29835e-005 637.502 0.000234219 396.965 0.000739251 283.023 0.00143572 220.335 0.00229072 180.871 0.00311512 153.387 0.00420737 133.236 0.00528783 117.781 0.00668946 105.448 0.00786019 95.3229 0.00903202 86.929 0.010273 79.8915 0.011585 73.7924 0.0137484 70.8616 0.0197341 67.8783 0.0135141 63.325 0.0148527 59.2921 0.0158717 55.6594 0.0177576 52.3977 0.0183471 49.4403 0.0210239 46.7469 0.0244348 44.2922 0.0263883 42.0388 0.0274598 39.9396 0.0270644 38.0016 0.0797796 36.1655 0.301133 34.4096 0.258727 32.8046 0.1299 31.3364 0.0716958 29.9341 0.0477549 28.59 0.0442279 27.3164 0.0387585 26.1009 0.0416509 24.9371 0.0451539 23.8241 0.0447313 22.7533 0.0576037 21.7204 0.0606645 20.7125 0.0556584 19.7281 0.0468744 18.7657 0.0752902 17.8149 0.0722629 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 BJH Desorption dA/dlog(w) Pore Area Halsey : Faas Correction 000-628 Cook 3FB-3-1 Pore Width (Å) dA/dlog(w) Pore Area (m²/g·Å) 1211.96 0.0651317 637.502 0.408264 396.965 0.734834 283.023 0.974681 220.335 1.18884 180.871 1.31678 153.387 1.50213 133.236 1.63519 117.781 1.82569 105.448 1.91838 95.3229 1.99118 86.929 2.06376 79.8915 2.13779 73.7924 2.34272 70.8616 3.22002 67.8783 2.11755 63.325 2.17025 59.2921 2.17129 55.6594 2.27998 52.3977 2.21734 49.4403 2.39713 46.7469 2.63402 44.2922 2.69492 42.0388 2.66151 39.9396 2.49211 38.0016 6.98903 36.1655 25.1077 34.4096 20.524 32.8046 9.82248 31.3364 5.17847 29.9341 3.29504 28.59 2.9146 27.3164 2.44036 26.1009 2.5058 24.9371 2.59544 23.8241 2.4564 22.7533 3.02119 21.7204 3.03736 20.7125 2.65759 19.7281 2.1319 18.7657 3.25752 17.8149 2.96847 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 Horvath-Kawazoe Report Slit Pore Geometry (Original H-K) Maximum Pore Volume: 0.001032 cm³/g at Relative Pressure: 0.010500365 Median Pore Width: 7.502 Å Relative Pressure Range: 3.650e-06 to 1.050e-02 Diameter of Adsorptive Molecule: 3.000 Å Diameter of Adsorptive at Zero Interaction Energy: 2.574 Å Diameter of Sample Atom: 3.040 Å Diameter of Sample Atom at Zero Interaction Energy: 2.609 Å Interaction Parameter: 3.49e-43 erg·cm^4 Density Conversion Factor: 0.0015468 Quantity Cumulative Differential Absolute Relative Adsorbed Pore Pore Pore Pressure Pressure (cm³/g Width Volume Volume (mmHg) (P/Po) STP) (Å) (cm³/g) (cm³/g·Å) ------ 0.00277 0.000003650 0.01877 5.094 0.0000 0.0000 0.00196 0.000002589 0.03932 5.005 0.0001 -0.0004 0.00322 0.000004248 0.05825 5.135 0.0001 0.0002 0.00636 0.000008405 0.07396 5.331 0.0001 0.0001 0.01371 0.000018119 0.09341 5.576 0.0001 0.0001 0.02459 0.000032507 0.11193 5.784 0.0002 0.0001 0.03906 0.000051649 0.12950 5.964 0.0002 0.0002 0.06425 0.000084977 0.15220 6.174 0.0002 0.0002 0.09560 0.000126458 0.17379 6.357 0.0003 0.0002 0.13281 0.000175701 0.19430 6.520 0.0003 0.0002 0.16217 0.000214566 0.20797 6.624 0.0003 0.0002 0.19385 0.000256517 0.22102 6.722 0.0003 0.0002 0.22771 0.000301351 0.23352 6.814 0.0004 0.0002 0.26358 0.000348876 0.24550 6.899 0.0004 0.0002 0.30136 0.000398922 0.25698 6.981 0.0004 0.0002 0.34081 0.000451195 0.26800 7.057 0.0004 0.0002 0.38189 0.000505642 0.27859 7.131 0.0004 0.0002 0.42452 0.000562150 0.28878 7.201 0.0004 0.0002 0.46854 0.000620517 0.29862 7.268 0.0005 0.0002 0.53114 0.000703493 0.31165 7.355 0.0005 0.0002 0.59406 0.000786910 0.32369 7.435 0.0005 0.0002 0.65424 0.000866718 0.33440 7.506 0.0005 0.0002 0.71197 0.000943298 0.34402 7.570 0.0005 0.0002 0.76579 0.001014707 0.35253 7.627 0.0005 0.0002 0.81676 0.001082352 0.36019 7.678 0.0006 0.0002 0.86517 0.001146620 0.36713 7.724 0.0006 0.0002 0.90978 0.001205861 0.37348 7.765 0.0006 0.0002 0.95058 0.001260052 0.37906 7.801 0.0006 0.0002 0.98934 0.001311568 0.38416 7.833 0.0006 0.0002 1.02326 0.001356672 0.38848 7.863 0.0006 0.0002 1.05648 0.001400845 0.39262 7.890 0.0006 0.0002 1.08829 0.001443173 0.39644 7.915 0.0006 0.0002 1.11783 0.001482492 0.39991 7.938 0.0006 0.0002 1.14558 0.001519455 0.40308 7.960 0.0006 0.0002 1.17113 0.001553499 0.40596 7.980 0.0006 0.0002 1.19438 0.001584492 0.40851 7.996 0.0006 0.0002 1.21678 0.001614353 0.41094 8.013 0.0006 0.0002 1.23735 0.001641804 0.41313 8.029 0.0006 0.0002 1.25578 0.001666429 0.41503 8.042 0.0006 0.0002 1.27265 0.001688980 0.41671 8.053 0.0006 0.0002 1.33054 0.001765990 0.42274 8.094 0.0007 0.0002 1.38882 0.001843556 0.42860 8.134 0.0007 0.0002 1.44782 0.001922061 0.43432 8.172 0.0007 0.0002 1.50751 0.002001504 0.43990 8.210 0.0007 0.0002 1.56741 0.002081273 0.44536 8.248 0.0007 0.0002 1.62817 0.002162176 0.45068 8.284 0.0007 0.0002 1.68922 0.002243470 0.45589 8.321 0.0007 0.0002 1.75040 0.002324956 0.46095 8.355 0.0007 0.0002 1.81230 0.002407422 0.46590 8.390 0.0007 0.0002 1.87448 0.002490269 0.47072 8.424 0.0007 0.0002 1.93696 0.002573574 0.47544 8.459 0.0007 0.0002 2.00018 0.002657869 0.48008 8.491 0.0007 0.0002 2.06363 0.002742470 0.48458 8.524 0.0007 0.0002 2.12756 0.002827754 0.48901 8.556 0.0008 0.0002 2.19173 0.002913379 0.49335 8.588 0.0008 0.0002 2.25589 0.002998961 0.49757 8.618 0.0008 0.0002 2.32049 0.003085144 0.50170 8.650 0.0008 0.0002 2.38551 0.003171953 0.50573 8.680 0.0008 0.0002 2.45070 0.003258965 0.50967 8.710 0.0008 0.0002 2.51650 0.003346858 0.51350 8.739 0.0008 0.0002 2.58258 0.003435079 0.51727 8.768 0.0008 0.0002 2.64899 0.003523767 0.52096 8.797 0.0008 0.0002 2.71518 0.003612286 0.52453 8.825 0.0008 0.0002 2.78204 0.003701659 0.52806 8.854 0.0008 0.0002 2.84919 0.003791394 0.53153 8.881 0.0008 0.0002 2.91676 0.003881702 0.53492 8.908 0.0008 0.0002 2.98388 0.003971481 0.53820 8.936 0.0008 0.0002 3.05153 0.004061989 0.54141 8.962 0.0008 0.0002 3.11924 0.004152540 0.54456 8.989 0.0008 0.0002 3.18795 0.004244444 0.54773 9.015 0.0008 0.0002 3.25627 0.004335841 0.55078 9.042 0.0009 0.0002 3.32480 0.004427601 0.55371 9.066 0.0009 0.0002 3.39366 0.004519815 0.55663 9.092 0.0009 0.0002 3.46330 0.004613092 0.55950 9.117 0.0009 0.0002 3.53291 0.004706364 0.56230 9.141 0.0009 0.0002 3.60262 0.004799776 0.56502 9.168 0.0009 0.0002 3.67225 0.004893104 0.56771 9.192 0.0009 0.0002 3.74171 0.004986243 0.57034 9.215 0.0009 0.0002 3.81191 0.005080367 0.57291 9.240 0.0009 0.0002 3.88193 0.005174292 0.57543 9.263 0.0009 0.0002 3.95222 0.005268591 0.57786 9.287 0.0009 0.0002 4.02339 0.005363999 0.58025 9.311 0.0009 0.0002 4.09349 0.005458085 0.58256 9.334 0.0009 0.0002 4.16419 0.005553003 0.58485 9.357 0.0009 0.0002 4.23511 0.005648221 0.58709 9.379 0.0009 0.0002 4.30603 0.005743474 0.58932 9.402 0.0009 0.0002 4.37728 0.005839179 0.59147 9.424 0.0009 0.0001 4.44912 0.005935612 0.59355 9.447 0.0009 0.0001 4.51992 0.006030767 0.59557 9.468 0.0009 0.0001 4.59104 0.006126270 0.59756 9.490 0.0009 0.0001 4.66275 0.006222677 0.59953 9.512 0.0009 0.0001 4.73499 0.006319815 0.60151 9.533 0.0009 0.0001 4.80744 0.006417260 0.60342 9.554 0.0009 0.0001 4.88003 0.006514815 0.60528 9.576 0.0009 0.0001 4.95269 0.006612585 0.60709 9.597 0.0009 0.0001 5.02515 0.006710002 0.60884 9.617 0.0009 0.0001 5.58423 0.007457731 0.62338 9.772 0.0010 0.0001 6.15587 0.008221870 0.63352 9.920 0.0010 0.0001 6.72013 0.008976293 0.64584 10.059 0.0010 0.0001 7.29247 0.009741631 0.65611 10.193 0.0010 0.0001 7.86021 0.010500365 0.66735 10.320 0.0010 0.0001 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 Horvath-Kawazoe Cumulative Pore Volume Plot Slit Pore Geometry (Original H-K) 000-628 Cook 3FB-3-1 Pore Width (Å) Pore Volume (cm³/g) 5.09425 2.90332e-005 5.00477 6.08251e-005 5.13526 9.00936e-005 5.33146 0.000114401 5.57591 0.000144481 5.78356 0.00017314 5.96356 0.000200312 6.17424 0.000235421 6.35668 0.000268824 6.52018 0.000300542 6.62439 0.000321692 6.722 0.000341881 6.81376 0.000361205 6.89949 0.000379745 6.98099 0.00039749 7.05715 0.000414539 7.13086 0.000430917 7.20104 0.000446689 7.26761 0.000461901 7.35522 0.000482058 7.43527 0.000500677 7.5065 0.000517256 7.56978 0.000532136 7.62707 0.000545289 7.67827 0.000557138 7.72436 0.000567879 7.76526 0.000577702 7.80092 0.000586332 7.83344 0.000594226 7.8628 0.0006009 7.89006 0.000607307 7.9152 0.00061322 7.93821 0.000618583 7.96016 0.000623492 7.97996 0.000627944 7.99649 0.000631886 8.01305 0.000635645 8.02852 0.000639022 8.0418 0.000641965 8.05288 0.000644574 8.09393 0.000653902 8.13401 0.000662956 8.172 0.000671802 8.21012 0.000680432 8.24837 0.000688876 8.2845 0.000697118 8.32073 0.000705164 8.35482 0.000712996 8.39014 0.000720658 8.42443 0.000728106 8.45882 0.000735408 8.49102 0.000742583 8.52446 0.000749541 8.55569 0.000756393 8.58815 0.000763112 8.61839 0.000769638 8.64986 0.000776032 8.68026 0.000782264 8.70956 0.000788362 8.73893 0.000794288 8.76838 0.00080012 8.79672 0.000805814 8.82513 0.000811343 8.8536 0.0008168 8.88096 0.000822176 8.90838 0.000827411 8.93586 0.000832494 8.96221 0.000837453 8.98861 0.000842333 9.01507 0.000847231 9.04159 0.000851947 9.06576 0.000856474 9.09239 0.000860995 9.11666 0.000865434 9.14097 0.000869759 9.16777 0.000873977 9.19218 0.00087813 9.21542 0.000882209 9.23993 0.000886171 9.26327 0.00089008 9.28664 0.000893836 9.3113 0.000897535 9.33353 0.000901097 9.35704 0.000904642 9.37935 0.000908115 9.40171 0.000911559 9.4241 0.000914878 9.44654 0.000918106 9.46776 0.000921231 9.49028 0.00092431 9.51158 0.000927359 9.53292 0.000930419 9.55429 0.000933372 9.5757 0.000936241 9.59715 0.000939039 9.61737 0.000941748 9.77179 0.00096424 9.92041 0.000979929 10.0591 0.000998989 10.1927 0.00101487 10.3197 0.00103226 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:58AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 Horvath-Kawazoe Differential Pore Volume Plot Slit Pore Geometry (Original H-K) 000-628 Cook 3FB-3-1 Pore Width (Å) dV/dw (cm³/g·Å) 5.09425 5.69921e-006 5.00477 -0.000355309 5.13526 0.000224303 5.33146 0.000123886 5.57591 0.000123055 5.78356 0.00013802 5.96356 0.000150955 6.17424 0.000166643 6.35668 0.000183086 6.52018 0.000193994 6.62439 0.000202958 6.722 0.000206835 6.81376 0.000210591 6.89949 0.000216267 6.98099 0.000217716 7.05715 0.000223859 7.13086 0.000222202 7.20104 0.000224738 7.26761 0.000228517 7.35522 0.000230069 7.43527 0.000232613 7.5065 0.000232747 7.56978 0.000235147 7.62707 0.000229573 7.67827 0.000231407 7.72436 0.000233058 7.76526 0.000240158 7.80092 0.000242009 7.83344 0.000242716 7.8628 0.000227333 7.89006 0.000235069 7.9152 0.000235205 7.93821 0.000233121 7.96016 0.000223562 7.97996 0.000224865 7.99649 0.000238466 8.01305 0.000227055 8.02852 0.000218239 8.0418 0.000221623 8.05288 0.00023543 8.09393 0.000227247 8.13401 0.000225908 8.172 0.000232837 8.21012 0.000226389 8.24837 0.000220738 8.2845 0.000228172 8.32073 0.000222033 8.35482 0.000229792 8.39014 0.000216902 8.42443 0.000217219 8.45882 0.000212292 8.49102 0.000222851 8.52446 0.000208085 8.55569 0.000219454 8.58815 0.000206929 8.61839 0.000215857 8.64986 0.000203131 8.68026 0.000205058 8.70956 0.000208094 8.73893 0.000201752 8.76838 0.000198045 8.79672 0.000200917 8.82513 0.000194646 8.8536 0.000191627 8.88096 0.000196533 8.90838 0.000190904 8.93586 0.00018499 8.96221 0.000188186 8.98861 0.000184834 9.01507 0.000185077 9.04159 0.000177845 9.06576 0.000187353 9.09239 0.000169732 9.11666 0.000182955 9.14097 0.000177861 9.16777 0.000157414 9.19218 0.000170096 9.21542 0.000175498 9.23993 0.000161645 9.26327 0.000167547 9.28664 0.000160664 9.3113 0.000150055 9.33353 0.000160229 9.35704 0.000150767 9.37935 0.000155622 9.40171 0.000154103 9.4241 0.00014819 9.44654 0.000143885 9.46776 0.000147213 9.49028 0.000136772 9.51158 0.000143095 9.53292 0.000143405 9.55429 0.000138196 9.5757 0.000133987 9.59715 0.000130478 9.61737 0.000133948 9.77179 0.000145659 9.92041 0.000105562 10.0591 0.000137447 10.1927 0.00011889 10.3197 0.000136895 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:59AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 Porosity Distribution by Original Density Functional Theory Model: N2 @ 77K on Carbon, Slit Pores Method: Non-negative Regularization; No Smoothing Standard Deviation of Fit: 0.02329, cm³/g STP Volume in Pores < 5.00 Å : 0.00004 cm³/g Total Volume in Pores <= 2525.70 Å : 0.00662 cm³/g Area in Pores > 2525.70 Å : 1.161 m²/g Total Area in Pores >= 5.00 Å : 2.494 m²/g Pore Size Table Cumulative Incremental Cumulative Pore Width Volume Volume Area Incremental (Å) (cm³/g) (cm³/g) (m²/g) Area (m²/g) ----- 5.00 0.00000 0.00000 0.000 0.000 5.36 0.00000 0.00000 0.000 0.000 5.90 0.00000 0.00000 0.000 0.000 6.43 0.00000 0.00000 0.000 0.000 6.79 0.00000 0.00000 0.000 0.000 7.33 0.00000 0.00000 0.000 0.000 8.04 0.00000 0.00000 0.000 0.000 8.58 0.00000 0.00000 0.000 0.000 9.29 0.00000 0.00000 0.000 0.000 10.01 0.00000 0.00000 0.000 0.000 10.90 0.00000 0.00000 0.000 0.000 11.79 0.00000 0.00000 0.000 0.000 12.69 0.00024 0.00024 0.379 0.379 13.58 0.00040 0.00016 0.611 0.232 14.83 0.00047 0.00007 0.711 0.099 15.91 0.00047 0.00000 0.711 0.000 17.16 0.00047 0.00000 0.711 0.000 18.59 0.00047 0.00000 0.711 0.000 20.02 0.00047 0.00000 0.711 0.000 21.62 0.00047 0.00000 0.711 0.000 23.41 0.00047 0.00000 0.711 0.000 25.20 0.00047 0.00000 0.711 0.000 27.34 0.00051 0.00004 0.740 0.029 29.49 0.00056 0.00004 0.770 0.030 31.81 0.00059 0.00004 0.793 0.024 34.31 0.00063 0.00003 0.813 0.019 36.99 0.00064 0.00002 0.822 0.009 40.03 0.00066 0.00002 0.831 0.009 43.25 0.00068 0.00002 0.841 0.011 46.64 0.00071 0.00003 0.854 0.013 50.40 0.00075 0.00003 0.867 0.013 54.33 0.00078 0.00004 0.881 0.014 58.80 0.00082 0.00003 0.892 0.011 63.44 0.00086 0.00004 0.904 0.012 68.45 0.00090 0.00005 0.917 0.013 73.99 0.00095 0.00005 0.931 0.014 79.88 0.00102 0.00006 0.947 0.016 86.32 0.00111 0.00009 0.969 0.022 93.11 0.00122 0.00011 0.992 0.023 100.61 0.00131 0.00009 1.010 0.018 108.66 0.00140 0.00009 1.027 0.017 117.23 0.00150 0.00010 1.044 0.017 126.53 0.00161 0.00011 1.061 0.018 136.71 0.00173 0.00012 1.079 0.018 147.61 0.00186 0.00013 1.097 0.018 159.41 0.00200 0.00014 1.114 0.017 172.10 0.00214 0.00014 1.131 0.017 185.86 0.00228 0.00014 1.146 0.015 200.69 0.00243 0.00015 1.161 0.015 216.60 0.00259 0.00016 1.175 0.015 233.93 0.00274 0.00015 1.188 0.013 252.52 0.00291 0.00016 1.201 0.013 272.71 0.00309 0.00018 1.215 0.013 294.51 0.00322 0.00013 1.224 0.009 317.92 0.00334 0.00012 1.231 0.008 343.30 0.00347 0.00013 1.239 0.007 370.64 0.00355 0.00008 1.243 0.005 400.31 0.00365 0.00010 1.248 0.005 432.30 0.00376 0.00011 1.253 0.005 466.79 0.00390 0.00015 1.259 0.006 503.96 0.00416 0.00025 1.269 0.010 544.17 0.00447 0.00031 1.281 0.012 587.60 0.00473 0.00026 1.290 0.009 634.42 0.00497 0.00024 1.297 0.007 684.99 0.00525 0.00029 1.305 0.008 739.68 0.00545 0.00020 1.311 0.005 798.65 0.00562 0.00018 1.315 0.004 862.45 0.00583 0.00021 1.320 0.005 931.26 0.00600 0.00017 1.324 0.004 1005.60 0.00611 0.00011 1.326 0.002 1085.66 0.00621 0.00010 1.328 0.002 1172.33 0.00633 0.00012 1.330 0.002 1265.80 0.00640 0.00007 1.331 0.001 1366.77 0.00646 0.00006 1.332 0.001 1475.96 0.00651 0.00006 1.332 0.001 1593.55 0.00655 0.00004 1.333 0.000 1720.79 0.00658 0.00003 1.333 0.000 1858.04 0.00659 0.00001 1.333 0.000 2006.19 0.00659 0.00000 1.333 0.000 2166.32 0.00659 0.00000 1.333 0.000 2339.13 0.00659 0.00000 1.333 0.000 2525.70 0.00659 0.00000 1.333 0.000 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:59AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 Porosity Distribution by Original Density Functional Theory Model: N2 @ 77K on Carbon, Slit Pores Method: Non-negative Regularization; No Smoothing Standard Deviation of Fit: 0.02329, cm³/g STP Isotherm Table Fitted Experimental Quantity Absolute Quantity Adsorbed Residual Relative Adsorbed (cm³/g (cm³/g Relative Pressure (cm³/g STP) STP) STP) Residual ----- 0.000005075 0.0625 0.0281 0.0344 0.550335 0.000008995 0.0752 0.0319 0.0433 0.575440 0.000015520 0.0890 0.0381 0.0509 0.571564 0.000026102 0.1044 0.0485 0.0559 0.535506 0.000042841 0.1220 0.0660 0.0561 0.459482 0.000068697 0.1419 0.0958 0.0461 0.325011 0.000107744 0.1647 0.1448 0.0199 0.120528 0.000165451 0.1904 0.2107 -0.0203 -0.106812 0.000249000 0.2188 0.2748 -0.0560 -0.255769 0.000367617 0.2499 0.3266 -0.0767 -0.306763 0.000532902 0.2836 0.3674 -0.0838 -0.295669 0.000759152 0.3198 0.4005 -0.0807 -0.252251 0.001063641 0.3581 0.4279 -0.0698 -0.194980 0.001466847 0.3985 0.4515 -0.0530 -0.132875 0.001992604 0.4393 0.4722 -0.0330 -0.075030 0.002668156 0.4806 0.4911 -0.0104 -0.021702 0.003524104 0.5210 0.5089 0.0121 0.023263 0.004594232 0.5589 0.5270 0.0319 0.057144 0.005915212 0.5931 0.5761 0.0170 0.028727 0.007526182 0.6245 0.6022 0.0223 0.035653 0.009468212 0.6525 0.6590 -0.0065 -0.010025 0.011783670 0.6817 0.6777 0.0040 0.005826 0.014515520 0.7074 0.6943 0.0130 0.018440 0.017706521 0.7304 0.7290 0.0014 0.001925 0.021398440 0.7498 0.7444 0.0055 0.007274 0.025631230 0.7661 0.7594 0.0067 0.008739 0.030442240 0.7818 0.7745 0.0073 0.009323 0.035865448 0.8000 0.7903 0.0097 0.012120 0.041930798 0.8201 0.8069 0.0131 0.016024 0.048663601 0.8413 0.8250 0.0163 0.019362 0.056084011 0.8620 0.8449 0.0172 0.019896 0.064206667 0.8819 0.8668 0.0150 0.017051 0.073040441 0.9024 0.8910 0.0114 0.012607 0.082588248 0.9239 0.9169 0.0070 0.007628 0.092847057 0.9448 0.9435 0.0013 0.001326 0.103808001 0.9650 0.9699 -0.0049 -0.005047 0.115456402 0.9856 0.9950 -0.0094 -0.009547 0.127772301 1.0072 1.0187 -0.0115 -0.011371 0.140730694 1.0297 1.0407 -0.0111 -0.010745 0.154301897 1.0524 1.0614 -0.0090 -0.008533 0.168452203 1.0740 1.0809 -0.0069 -0.006421 0.183144197 1.0952 1.0995 -0.0043 -0.003943 0.198337302 1.1164 1.1175 -0.0011 -0.000992 0.213988706 1.1380 1.1350 0.0030 0.002612 0.230053306 1.1615 1.1654 -0.0039 -0.003397 0.246484801 1.1834 1.1826 0.0008 0.000683 0.263235897 1.2077 1.1999 0.0078 0.006477 0.280259013 1.2315 1.2322 -0.0006 -0.000515 0.297506303 1.2550 1.2502 0.0048 0.003811 0.314930797 1.2787 1.2818 -0.0031 -0.002424 0.332486212 1.3027 1.3013 0.0014 0.001113 0.350127310 1.3269 1.3216 0.0052 0.003951 0.367810607 1.3526 1.3547 -0.0021 -0.001572 0.385494202 1.3779 1.3769 0.0010 0.000732 0.403138310 1.4039 1.3997 0.0041 0.002943 0.420704991 1.4293 1.4287 0.0006 0.000422 0.438158900 1.4537 1.4516 0.0021 0.001418 0.455466807 1.4784 1.4806 -0.0022 -0.001477 0.472598106 1.5029 1.5024 0.0005 0.000335 0.489524394 1.5275 1.5236 0.0040 0.002610 0.506219923 1.5516 1.5528 -0.0012 -0.000780 0.522661209 1.5757 1.5726 0.0031 0.001978 0.538827300 1.5998 1.6031 -0.0033 -0.002085 0.554699600 1.6222 1.6222 0.0000 0.000004 0.570261598 1.6462 1.6412 0.0051 0.003074 0.585499227 1.6710 1.6732 -0.0023 -0.001364 0.600400090 1.6961 1.6924 0.0037 0.002178 0.614954293 1.7216 1.7270 -0.0053 -0.003088 0.629153311 1.7474 1.7469 0.0005 0.000300 0.642990828 1.7737 1.7675 0.0061 0.003466 0.656461716 1.8001 1.8018 -0.0017 -0.000938 0.669562697 1.8264 1.8237 0.0028 0.001512 0.682291925 1.8552 1.8622 -0.0070 -0.003747 0.694648683 1.8854 1.8848 0.0006 0.000319 0.706633508 1.9147 1.9074 0.0074 0.003853 0.718248010 1.9445 1.9492 -0.0047 -0.002407 0.729494929 1.9765 1.9710 0.0055 0.002798 0.740377605 2.0086 2.0141 -0.0055 -0.002744 0.750900388 2.0411 2.0348 0.0062 0.003059 0.761068285 2.0753 2.0833 -0.0079 -0.003829 0.770887017 2.1117 2.1031 0.0086 0.004074 0.780362606 2.1482 2.1655 -0.0173 -0.008065 0.789501607 2.1851 2.1851 -0.0000 -0.000003 0.798311174 2.2229 2.2049 0.0180 0.008106 0.806798697 2.2631 2.2732 -0.0102 -0.004493 0.814971626 2.3042 2.2936 0.0107 0.004631 0.822837889 2.3460 2.3564 -0.0105 -0.004461 0.830405474 2.3887 2.3778 0.0109 0.004567 0.837682605 2.4320 2.4434 -0.0114 -0.004682 0.844677329 2.4773 2.4656 0.0118 0.004755 0.851397991 2.5241 2.5364 -0.0123 -0.004884 0.857852995 2.5712 2.5585 0.0127 0.004931 0.864050388 2.6201 2.6344 -0.0144 -0.005478 0.869998574 2.6703 2.6556 0.0147 0.005494 0.875705481 2.7206 2.7362 -0.0156 -0.005727 0.881179392 2.7722 2.7563 0.0159 0.005721 0.886428118 2.8258 2.8431 -0.0172 -0.006103 0.891459525 2.8802 2.8627 0.0175 0.006075 0.896281302 2.9340 2.9517 -0.0177 -0.006045 0.900900900 2.9894 2.9715 0.0180 0.006007 0.905325770 3.0472 3.0662 -0.0190 -0.006230 0.909563184 3.1059 3.0867 0.0192 0.006177 0.913620114 3.1643 3.1822 -0.0179 -0.005661 0.917503417 3.2219 3.2038 0.0181 0.005615 0.921219707 3.2830 3.3037 -0.0207 -0.006313 0.924775481 3.3468 3.3259 0.0209 0.006242 0.928177178 3.4115 3.4326 -0.0211 -0.006188 0.931430817 3.4755 3.4542 0.0213 0.006116 0.934542298 3.5377 3.5577 -0.0200 -0.005656 0.937517405 3.5985 3.5784 0.0201 0.005595 0.940361619 3.6638 3.6882 -0.0244 -0.006657 0.943080306 3.7327 3.7082 0.0245 0.006566 0.945678592 3.8031 3.8282 -0.0251 -0.006603 0.948161721 3.8735 3.8483 0.0252 0.006510 0.950534225 3.9427 3.9426 0.0001 0.000013 0.952800930 4.0097 4.0308 -0.0211 -0.005267 0.954966187 4.0738 4.0526 0.0212 0.005204 0.957034409 4.1334 4.1470 -0.0136 -0.003298 0.959009588 4.1838 4.1701 0.0137 0.003273 0.960896015 4.2298 4.2414 -0.0116 -0.002744 0.962697208 4.2762 4.2645 0.0117 0.002726 0.964416981 4.3265 4.3439 -0.0174 -0.004023 0.966058910 4.3835 4.3660 0.0175 0.003983 0.967626274 4.4488 4.4488 0.0000 0.000006 0.969122529 4.5238 4.5557 -0.0318 -0.007038 0.970550597 4.6091 4.5772 0.0319 0.006920 0.971913695 4.7048 4.7465 -0.0418 -0.008876 0.973214507 4.8108 4.7690 0.0418 0.008693 0.974455774 4.9269 4.9775 -0.0506 -0.010260 0.975640416 5.0525 5.0019 0.0506 0.010018 0.976770699 5.1791 5.1791 0.0000 0.000001 0.977849126 5.2999 5.3449 -0.0450 -0.008496 0.978878021 5.4151 5.3700 0.0451 0.008324 0.979859591 5.5250 5.5655 -0.0405 -0.007323 0.980795979 5.6299 5.5894 0.0405 0.007193 0.981689274 5.7299 5.7299 -0.0000 -0.000000 0.982541502 5.8253 5.8588 -0.0335 -0.005751 0.983354270 5.9163 5.8828 0.0335 0.005666 0.984129488 6.0032 6.0315 -0.0283 -0.004720 0.984869003 6.0860 6.0576 0.0284 0.004658 0.985574186 6.1649 6.1885 -0.0236 -0.003822 0.986246824 6.2403 6.2167 0.0236 0.003778 0.986888289 6.3121 6.3121 -0.0000 -0.000001 0.987500012 6.3806 6.3998 -0.0192 -0.003005 0.988083303 6.4459 6.4267 0.0192 0.002975 0.988639593 6.5082 6.5245 -0.0163 -0.002508 0.989170074 6.5676 6.5513 0.0163 0.002486 0.989675879 6.6242 6.6243 -0.0000 -0.000001 0.990158200 6.6783 6.6886 -0.0104 -0.001552 0.990618110 6.7298 6.7194 0.0104 0.001540 0.991056621 6.7789 6.7862 -0.0073 -0.001078 0.991474688 6.8257 6.8184 0.0073 0.001071 0.991873324 6.8703 6.8703 -0.0000 -0.000001 0.992253423 6.9129 6.9176 -0.0047 -0.000686 0.992615700 6.9534 6.9487 0.0047 0.000682 0.992961228 6.9921 6.9886 0.0035 0.000502 0.993290603 7.0290 7.0216 0.0074 0.001056 0.993604600 7.0642 7.0566 0.0076 0.001069 0.993903875 7.0977 7.0929 0.0048 0.000679 0.994189322 7.1297 7.1293 0.0003 0.000049 0.994461298 7.1601 7.1653 -0.0052 -0.000723 0.994720697 7.1892 7.1922 -0.0031 -0.000428 0.994967878 7.2168 7.2323 -0.0155 -0.002143 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:59AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 Cumulative Surface Area vs. Pore Width Cumulative Surface Area Pore Width (Angstroms) Cumulative Surface Area (m²/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 0.379029 13.5819 0.611101 14.8329 0.710561 15.9052 0.710561 17.1561 0.710561 18.5858 0.710561 20.0155 0.710561 21.6239 0.710561 23.411 0.710561 25.198 0.710561 27.3426 0.739958 29.4871 0.769806 31.8103 0.793379 34.3122 0.812796 36.9929 0.821688 40.0309 0.830549 43.2477 0.841473 46.6432 0.85398 50.3961 0.867245 54.3277 0.881038 58.7954 0.891842 63.4419 0.904032 68.4458 0.917473 73.9858 0.931139 79.8832 0.947091 86.3167 0.969024 93.1077 0.991702 100.613 1.00958 108.655 1.02652 117.233 1.04372 126.526 1.06123 136.713 1.07888 147.614 1.09688 159.409 1.11394 172.097 1.13071 185.858 1.14599 200.691 1.16063 216.596 1.17523 233.931 1.18825 252.517 1.20126 272.711 1.21459 294.513 1.22362 317.924 1.23115 343.301 1.23855 370.644 1.24311 400.309 1.24806 432.298 1.25297 466.789 1.25927 503.961 1.2693 544.171 1.28084 587.597 1.28961 634.419 1.29708 684.994 1.30546 739.679 1.31075 798.653 1.31515 862.452 1.31991 931.255 1.32358 1005.6 1.32582 1085.66 1.3276 1172.33 1.32958 1265.8 1.33074 1366.77 1.33158 1475.96 1.33235 1593.55 1.33284 1720.79 1.33315 1858.04 1.33323 2006.19 1.33323 2166.32 1.33323 2339.13 1.33323 2525.7 1.33323 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:59AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 Incremental Surface Area vs. Pore Width Incremental Surface Area Pore Width (Angstroms) Incremental Surface Area (m²/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 0.379029 13.5819 0.232071 14.8329 0.0994602 15.9052 0 17.1561 0 18.5858 0 20.0155 0 21.6239 0 23.411 0 25.198 0 27.3426 0.0293975 29.4871 0.0298472 31.8103 0.0235737 34.3122 0.0194172 36.9929 0.00889169 40.0309 0.00886084 43.2477 0.0109243 46.6432 0.0125071 50.3961 0.0132649 54.3277 0.0137927 58.7954 0.0108045 63.4419 0.0121897 68.4458 0.0134411 73.9858 0.0136658 79.8832 0.0159516 86.3167 0.0219333 93.1077 0.0226785 100.613 0.0178764 108.655 0.0169446 117.233 0.0171924 126.526 0.0175094 136.713 0.0176511 147.614 0.0180064 159.409 0.0170622 172.097 0.0167688 185.858 0.015278 200.691 0.0146395 216.596 0.014594 233.931 0.0130217 252.517 0.0130119 272.711 0.0133319 294.513 0.00902527 317.924 0.00752996 343.301 0.00740789 370.644 0.00455117 400.309 0.00495208 432.298 0.00490893 466.789 0.00630632 503.961 0.0100318 544.171 0.011531 587.597 0.00877568 634.419 0.00746739 684.994 0.00838356 739.679 0.00528944 798.653 0.00439451 862.452 0.00475963 931.255 0.00367438 1005.6 0.00223649 1085.66 0.00178069 1172.33 0.00198499 1265.8 0.00115951 1366.77 0.00083934 1475.96 0.00076817 1593.55 0.000493305 1720.79 0.000306631 1858.04 8.21911e-005 2006.19 0 2166.32 0 2339.13 0 2525.7 0 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:59AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 Differential Surface Area vs. Pore Width Differential Surface Area Pore Width (Angstroms) Differential Surface Area (m²/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 12.3725 13.5819 6.84376 14.8329 2.90071 15.9052 0 17.1561 0 18.5858 0 20.0155 0 21.6239 0 23.411 0 25.198 0 27.3426 0.861279 29.4871 0.908197 31.8103 0.716337 34.3122 0.592435 36.9929 0.265635 40.0309 0.261208 43.2477 0.329083 46.6432 0.376527 50.3961 0.400551 54.3277 0.412049 58.7954 0.320825 63.4419 0.369369 68.4458 0.402596 73.9858 0.407273 79.8832 0.476545 86.3167 0.65935 93.1077 0.681432 100.613 0.533101 108.655 0.510415 117.233 0.519959 126.526 0.524568 136.713 0.527317 147.614 0.539895 159.409 0.512022 172.097 0.503051 185.858 0.457745 200.691 0.44049 216.596 0.438524 233.931 0.390811 252.517 0.390661 272.711 0.399068 294.513 0.270942 317.924 0.226226 343.301 0.22235 370.644 0.136425 400.309 0.148206 432.298 0.147139 466.789 0.189341 503.961 0.301191 544.171 0.345847 587.597 0.263371 634.419 0.224222 684.994 0.251505 739.679 0.158671 798.653 0.131785 862.452 0.142695 931.255 0.110193 1005.6 0.0671363 1085.66 0.0534527 1172.33 0.059546 1265.8 0.0347971 1366.77 0.0251638 1475.96 0.0230436 1593.55 0.014802 1720.79 0.00919581 1858.04 0.00246658 2006.19 0 2166.32 0 2339.13 0 2525.7 0 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:59AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 Cumulative Pore Volume vs. Pore Width Cumulative Pore Volume Pore Width (Angstroms) Cumulative Pore Volume (cm³/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 0.000240463 13.5819 0.000398062 14.8329 0.000471826 15.9052 0.000471826 17.1561 0.000471826 18.5858 0.000471826 20.0155 0.000471826 21.6239 0.000471826 23.411 0.000471826 25.198 0.000471826 27.3426 0.000512016 29.4871 0.000556022 31.8103 0.000593516 34.3122 0.000626828 36.9929 0.000643275 40.0309 0.00066101 43.2477 0.000684633 46.6432 0.000713801 50.3961 0.000747226 54.3277 0.000784692 58.7954 0.000816455 63.4419 0.000855122 68.4458 0.000901121 73.9858 0.000951675 79.8832 0.00101539 86.3167 0.00111005 93.1077 0.00121563 100.613 0.00130556 108.655 0.00139761 117.233 0.00149839 126.526 0.00160916 136.713 0.00172982 147.614 0.00186272 159.409 0.00199871 172.097 0.002143 185.858 0.00228498 200.691 0.00243188 216.596 0.00258993 233.931 0.00274224 252.517 0.00290653 272.711 0.00308831 294.513 0.00322122 317.924 0.00334092 343.301 0.00346807 370.644 0.00355241 400.309 0.00365153 432.298 0.00375764 466.789 0.00390483 503.961 0.00415761 544.171 0.00447135 587.597 0.00472918 634.419 0.00496605 684.994 0.00525318 739.679 0.00544881 798.653 0.00562429 862.452 0.00582954 931.255 0.00600063 1005.6 0.00611308 1085.66 0.00620974 1172.33 0.00632609 1265.8 0.00639948 1366.77 0.00645684 1475.96 0.00651353 1593.55 0.00655283 1720.79 0.00657922 1858.04 0.00658685 2006.19 0.00658685 2166.32 0.00658685 2339.13 0.00658685 2525.7 0.00658685 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:59AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 Incremental Pore Volume vs. Pore Width Incremental Pore Volume Pore Width (Angstroms) Incremental Pore Volume (cm³/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 0.000240463 13.5819 0.000157599 14.8329 7.37641e-005 15.9052 0 17.1561 0 18.5858 0 20.0155 0 21.6239 0 23.411 0 25.198 0 27.3426 4.01902e-005 29.4871 4.40054e-005 31.8103 3.74943e-005 34.3122 3.33123e-005 36.9929 1.64465e-005 40.0309 1.77354e-005 43.2477 2.36226e-005 46.6432 2.91684e-005 50.3961 3.34249e-005 54.3277 3.74663e-005 58.7954 3.17629e-005 63.4419 3.86669e-005 68.4458 4.59993e-005 73.9858 5.05537e-005 79.8832 6.37131e-005 86.3167 9.46607e-005 93.1077 0.000105577 100.613 8.99305e-005 108.655 9.20561e-005 117.233 0.000100776 126.526 0.00011077 136.713 0.000120656 147.614 0.0001329 159.409 0.000135993 172.097 0.000144294 185.858 0.000141977 200.691 0.000146901 216.596 0.000158051 233.931 0.000152309 252.517 0.000164287 272.711 0.000181787 294.513 0.000132903 317.924 0.000119698 343.301 0.000127157 370.644 8.4343e-005 400.309 9.91183e-005 432.298 0.000106106 466.789 0.000147186 503.961 0.000252781 544.171 0.000313741 587.597 0.000257828 634.419 0.000236873 684.994 0.000287134 739.679 0.000195624 798.653 0.000175485 862.452 0.000205248 931.255 0.000171089 1005.6 0.00011245 1085.66 9.66615e-005 1172.33 0.000116354 1265.8 7.33853e-005 1366.77 5.73593e-005 1475.96 5.66895e-005 1593.55 3.93054e-005 1720.79 2.63824e-005 1858.04 7.63573e-006 2006.19 0 2166.32 0 2339.13 0 2525.7 0 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:59AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 Differential Pore Volume vs. Pore Width Differential Pore Volume Pore Width (Angstroms) Differential Pore Volume (cm³/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 0.00784935 13.5819 0.00464757 14.8329 0.0021513 15.9052 0 17.1561 0 18.5858 0 20.0155 0 21.6239 0 23.411 0 25.198 0 27.3426 0.00117748 29.4871 0.001339 31.8103 0.00113934 34.3122 0.00101639 36.9929 0.000491329 40.0309 0.000522821 43.2477 0.000711604 46.6432 0.000878121 50.3961 0.00100931 54.3277 0.00111928 58.7954 0.000943152 63.4419 0.00117167 68.4458 0.0013778 73.9858 0.00150662 79.8832 0.0019034 86.3167 0.00284565 93.1077 0.00317233 100.613 0.00268186 108.655 0.00277297 117.233 0.00304783 126.526 0.00331858 136.713 0.00360455 147.614 0.00398481 159.409 0.00408105 172.097 0.00432869 185.858 0.00425378 200.691 0.00442012 216.596 0.00474913 233.931 0.00457113 252.517 0.00493242 272.711 0.0054415 294.513 0.00398981 317.924 0.00359614 343.301 0.00381664 370.644 0.00252824 400.309 0.00296641 432.298 0.00318039 466.789 0.00441913 503.961 0.00758942 544.171 0.00940998 587.597 0.00773781 634.419 0.00711254 684.994 0.00861397 739.679 0.0058683 798.653 0.00526254 862.452 0.00615336 931.255 0.00513091 1005.6 0.00337561 1085.66 0.00290157 1172.33 0.00349039 1265.8 0.00220231 1366.77 0.00171965 1475.96 0.00170058 1593.55 0.00117939 1720.79 0.000791205 1858.04 0.00022915 2006.19 0 2166.32 0 2339.13 0 2525.7 0 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:59AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 Standard Deviation of Fit: 0.02329, cm³/g STP Goodness of Fit Input Data Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 3.64992e-006 0.0187699 2.58913e-006 0.0393232 4.24767e-006 0.0582452 8.40488e-006 0.0739597 1.8119e-005 0.0934065 3.2507e-005 0.111934 5.16491e-005 0.129501 8.49771e-005 0.152199 0.000126458 0.173793 0.000175701 0.194299 0.000214566 0.207972 0.000256517 0.221025 0.000301351 0.233518 0.000348876 0.245504 0.000398922 0.256976 0.000451195 0.267998 0.000505642 0.278586 0.00056215 0.288783 0.000620517 0.298617 0.000703493 0.311649 0.00078691 0.323686 0.000866718 0.334404 0.000943298 0.344024 0.00101471 0.352527 0.00108235 0.360187 0.00114662 0.367131 0.00120586 0.373482 0.00126005 0.379061 0.00131157 0.384164 0.00135667 0.388479 0.00140084 0.392622 0.00144317 0.396444 0.00148249 0.399911 0.00151945 0.403085 0.0015535 0.405963 0.00158449 0.408512 0.00161435 0.410942 0.0016418 0.413125 0.00166643 0.415028 0.00168898 0.416715 0.00176599 0.422745 0.00184356 0.428599 0.00192206 0.434317 0.0020015 0.439897 0.00208127 0.445355 0.00216218 0.450684 0.00224347 0.455886 0.00232496 0.460949 0.00240742 0.465902 0.00249027 0.470718 0.00257357 0.475438 0.00265787 0.480077 0.00274247 0.484575 0.00282775 0.489005 0.00291338 0.493349 0.00299896 0.497568 0.00308514 0.501702 0.00317195 0.505731 0.00325896 0.509673 0.00334686 0.513504 0.00343508 0.517274 0.00352377 0.520955 0.00361229 0.52453 0.00370166 0.528058 0.00379139 0.531534 0.0038817 0.534918 0.00397148 0.538204 0.00406199 0.54141 0.00415254 0.544565 0.00424444 0.547731 0.00433584 0.550781 0.0044276 0.553707 0.00451981 0.55663 0.00461309 0.5595 0.00470636 0.562295 0.00479978 0.565023 0.0048931 0.567708 0.00498624 0.570344 0.00508037 0.572906 0.00517429 0.575433 0.00526859 0.577861 0.005364 0.580253 0.00545809 0.582556 0.005553 0.584847 0.00564822 0.587092 0.00574347 0.58932 0.00583918 0.591465 0.00593561 0.593552 0.00603077 0.595572 0.00612627 0.597563 0.00622268 0.599534 0.00631982 0.601512 0.00641726 0.603421 0.00651482 0.605276 0.00661258 0.607085 0.00671 0.608836 0.00745773 0.623378 0.00822187 0.63352 0.00897629 0.645843 0.00974163 0.656112 0.0105004 0.667355 0.0297531 0.779559 0.0573477 0.865162 0.0702668 0.896066 0.0903994 0.940093 0.111008 0.977787 0.130695 1.0123 0.150683 1.04651 0.170811 1.07747 0.190939 1.10621 0.211045 1.13381 0.230969 1.16275 0.251168 1.18975 0.271474 1.21961 0.291362 1.24658 0.311638 1.27423 0.331696 1.30162 0.35159 1.32891 0.372578 1.35958 0.39264 1.38809 0.412719 1.41814 0.433408 1.44691 0.453262 1.47527 0.473299 1.50394 0.493149 1.53281 0.51352 1.56206 0.533932 1.59278 0.553951 1.62111 0.57379 1.65189 0.594244 1.68559 0.614114 1.72014 0.634571 1.75756 0.654378 1.796 0.674724 1.83762 0.694662 1.88539 0.714702 1.9351 0.734859 1.99227 0.755033 2.0545 0.774989 2.12739 0.795433 2.21018 0.815383 2.30636 0.835576 2.41917 0.855729 2.55541 0.875841 2.72179 0.895959 2.93035 0.916095 3.20059 0.936049 3.56791 0.956017 4.10478 0.975596 5.04761 0.995117 7.23359 Model Fit Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 5.07465e-006 0.0281132 8.99464e-006 0.0319145 1.552e-005 0.038147 2.61021e-005 0.0485068 4.28409e-005 0.0659665 6.86973e-005 0.0957656 0.000107744 0.144846 0.000165451 0.210715 0.000249 0.274763 0.000367617 0.326581 0.000532902 0.367443 0.000759152 0.400458 0.00106364 0.427949 0.00146685 0.4515 0.0019926 0.472238 0.00266816 0.491061 0.0035241 0.50885 0.00459423 0.526988 0.00591521 0.576077 0.00752618 0.602245 0.00946821 0.659003 0.0117837 0.677705 0.0145155 0.694325 0.0177065 0.728968 0.0213984 0.744367 0.0256312 0.759393 0.0304422 0.77455 0.0358654 0.79026 0.0419308 0.806936 0.0486636 0.825 0.056084 0.844862 0.0642067 0.866841 0.0730404 0.890983 0.0825882 0.916856 0.0928471 0.943518 0.103808 0.969853 0.115456 0.995025 0.127772 1.01866 0.140731 1.04073 0.154302 1.06141 0.168452 1.08093 0.183144 1.09954 0.198337 1.1175 0.213989 1.13501 0.230053 1.1654 0.246485 1.18255 0.263236 1.19985 0.280259 1.23215 0.297506 1.25017 0.314931 1.28183 0.332486 1.30125 0.350127 1.32165 0.367811 1.35473 0.385494 1.3769 0.403138 1.39973 0.420705 1.42868 0.438159 1.45164 0.455467 1.48061 0.472598 1.50243 0.489524 1.52355 0.50622 1.55277 0.522661 1.5726 0.538827 1.60315 0.5547 1.62221 0.570262 1.64118 0.585499 1.67324 0.6004 1.69241 0.614954 1.72695 0.629153 1.74692 0.642991 1.76754 0.656462 1.80178 0.669563 1.82366 0.682292 1.86217 0.694649 1.88476 0.706634 1.90737 0.718248 1.94915 0.729495 1.97097 0.740378 2.01412 0.7509 2.03483 0.761068 2.08325 0.770887 2.10314 0.780363 2.16554 0.789502 2.18511 0.798311 2.20486 0.806799 2.27323 0.814972 2.29358 0.822838 2.35642 0.830405 2.37779 0.837683 2.44338 0.844677 2.46557 0.851398 2.53644 0.857853 2.55852 0.86405 2.63443 0.869999 2.65559 0.875705 2.73616 0.881179 2.7563 0.886428 2.84308 0.89146 2.86267 0.896281 2.95173 0.900901 2.97145 0.905326 3.0662 0.909563 3.08672 0.91362 3.1822 0.917503 3.20381 0.92122 3.3037 0.924775 3.3259 0.928177 3.43257 0.931431 3.45424 0.934542 3.55773 0.937517 3.57836 0.940362 3.68823 0.94308 3.70818 0.945679 3.82821 0.948162 3.84828 0.950534 3.94262 0.952801 4.0308 0.954966 4.05261 0.957034 4.14703 0.95901 4.17013 0.960896 4.24142 0.962697 4.26452 0.964417 4.34393 0.966059 4.36601 0.967626 4.44882 0.969123 4.55567 0.970551 4.57716 0.971914 4.74652 0.973215 4.76902 0.974456 4.97749 0.97564 5.00192 0.976771 5.1791 0.977849 5.3449 0.978878 5.37001 0.97986 5.56546 0.980796 5.58937 0.981689 5.7299 0.982542 5.85883 0.983354 5.88282 0.984129 6.03149 0.984869 6.05761 0.985574 6.1885 0.986247 6.21668 0.986888 6.31209 0.9875 6.39976 0.988083 6.42673 0.98864 6.52452 0.98917 6.55128 0.989676 6.62425 0.990158 6.68862 0.990618 6.71939 0.991057 6.78617 0.991475 6.81837 0.991873 6.87032 0.992253 6.91762 0.992616 6.94871 0.992961 6.98863 0.993291 7.0216 0.993605 7.05664 0.993904 7.09288 0.994189 7.12932 0.994461 7.1653 0.994721 7.19224 0.994968 7.23231 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-628 Cook 3FB-3-1 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-628.SMP Started: 1/2/2018 11:03:47AM Analysis Adsorptive: N2 Completed: 1/3/2018 5:58:21AM Analysis Bath Temp.: -195.892 °C Report Time: 10/2/2019 10:00:59AM Thermal Correction: No Sample Mass: 0.4411 g Warm Free Space: 16.1032 cm³ Measured Cold Free Space: 47.5087 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: Yes Comments: Ann Cook Gulf sediment sample 3FB-3-1; same degas and analysis conditions as for Cook sample 6cs-3 Standard Deviation of Fit: 0.02329, cm³/g STP Goodness of Fit Input Data Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 3.64992e-006 0.0187699 2.58913e-006 0.0393232 4.24767e-006 0.0582452 8.40488e-006 0.0739597 1.8119e-005 0.0934065 3.2507e-005 0.111934 5.16491e-005 0.129501 8.49771e-005 0.152199 0.000126458 0.173793 0.000175701 0.194299 0.000214566 0.207972 0.000256517 0.221025 0.000301351 0.233518 0.000348876 0.245504 0.000398922 0.256976 0.000451195 0.267998 0.000505642 0.278586 0.00056215 0.288783 0.000620517 0.298617 0.000703493 0.311649 0.00078691 0.323686 0.000866718 0.334404 0.000943298 0.344024 0.00101471 0.352527 0.00108235 0.360187 0.00114662 0.367131 0.00120586 0.373482 0.00126005 0.379061 0.00131157 0.384164 0.00135667 0.388479 0.00140084 0.392622 0.00144317 0.396444 0.00148249 0.399911 0.00151945 0.403085 0.0015535 0.405963 0.00158449 0.408512 0.00161435 0.410942 0.0016418 0.413125 0.00166643 0.415028 0.00168898 0.416715 0.00176599 0.422745 0.00184356 0.428599 0.00192206 0.434317 0.0020015 0.439897 0.00208127 0.445355 0.00216218 0.450684 0.00224347 0.455886 0.00232496 0.460949 0.00240742 0.465902 0.00249027 0.470718 0.00257357 0.475438 0.00265787 0.480077 0.00274247 0.484575 0.00282775 0.489005 0.00291338 0.493349 0.00299896 0.497568 0.00308514 0.501702 0.00317195 0.505731 0.00325896 0.509673 0.00334686 0.513504 0.00343508 0.517274 0.00352377 0.520955 0.00361229 0.52453 0.00370166 0.528058 0.00379139 0.531534 0.0038817 0.534918 0.00397148 0.538204 0.00406199 0.54141 0.00415254 0.544565 0.00424444 0.547731 0.00433584 0.550781 0.0044276 0.553707 0.00451981 0.55663 0.00461309 0.5595 0.00470636 0.562295 0.00479978 0.565023 0.0048931 0.567708 0.00498624 0.570344 0.00508037 0.572906 0.00517429 0.575433 0.00526859 0.577861 0.005364 0.580253 0.00545809 0.582556 0.005553 0.584847 0.00564822 0.587092 0.00574347 0.58932 0.00583918 0.591465 0.00593561 0.593552 0.00603077 0.595572 0.00612627 0.597563 0.00622268 0.599534 0.00631982 0.601512 0.00641726 0.603421 0.00651482 0.605276 0.00661258 0.607085 0.00671 0.608836 0.00745773 0.623378 0.00822187 0.63352 0.00897629 0.645843 0.00974163 0.656112 0.0105004 0.667355 0.0297531 0.779559 0.0573477 0.865162 0.0702668 0.896066 0.0903994 0.940093 0.111008 0.977787 0.130695 1.0123 0.150683 1.04651 0.170811 1.07747 0.190939 1.10621 0.211045 1.13381 0.230969 1.16275 0.251168 1.18975 0.271474 1.21961 0.291362 1.24658 0.311638 1.27423 0.331696 1.30162 0.35159 1.32891 0.372578 1.35958 0.39264 1.38809 0.412719 1.41814 0.433408 1.44691 0.453262 1.47527 0.473299 1.50394 0.493149 1.53281 0.51352 1.56206 0.533932 1.59278 0.553951 1.62111 0.57379 1.65189 0.594244 1.68559 0.614114 1.72014 0.634571 1.75756 0.654378 1.796 0.674724 1.83762 0.694662 1.88539 0.714702 1.9351 0.734859 1.99227 0.755033 2.0545 0.774989 2.12739 0.795433 2.21018 0.815383 2.30636 0.835576 2.41917 0.855729 2.55541 0.875841 2.72179 0.895959 2.93035 0.916095 3.20059 0.936049 3.56791 0.956017 4.10478 0.975596 5.04761 0.995117 7.23359 Model Fit Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 5.07465e-006 0.0281132 8.99464e-006 0.0319145 1.552e-005 0.038147 2.61021e-005 0.0485068 4.28409e-005 0.0659665 6.86973e-005 0.0957656 0.000107744 0.144846 0.000165451 0.210715 0.000249 0.274763 0.000367617 0.326581 0.000532902 0.367443 0.000759152 0.400458 0.00106364 0.427949 0.00146685 0.4515 0.0019926 0.472238 0.00266816 0.491061 0.0035241 0.50885 0.00459423 0.526988 0.00591521 0.576077 0.00752618 0.602245 0.00946821 0.659003 0.0117837 0.677705 0.0145155 0.694325 0.0177065 0.728968 0.0213984 0.744367 0.0256312 0.759393 0.0304422 0.77455 0.0358654 0.79026 0.0419308 0.806936 0.0486636 0.825 0.056084 0.844862 0.0642067 0.866841 0.0730404 0.890983 0.0825882 0.916856 0.0928471 0.943518 0.103808 0.969853 0.115456 0.995025 0.127772 1.01866 0.140731 1.04073 0.154302 1.06141 0.168452 1.08093 0.183144 1.09954 0.198337 1.1175 0.213989 1.13501 0.230053 1.1654 0.246485 1.18255 0.263236 1.19985 0.280259 1.23215 0.297506 1.25017 0.314931 1.28183 0.332486 1.30125 0.350127 1.32165 0.367811 1.35473 0.385494 1.3769 0.403138 1.39973 0.420705 1.42868 0.438159 1.45164 0.455467 1.48061 0.472598 1.50243 0.489524 1.52355 0.50622 1.55277 0.522661 1.5726 0.538827 1.60315 0.5547 1.62221 0.570262 1.64118 0.585499 1.67324 0.6004 1.69241 0.614954 1.72695 0.629153 1.74692 0.642991 1.76754 0.656462 1.80178 0.669563 1.82366 0.682292 1.86217 0.694649 1.88476 0.706634 1.90737 0.718248 1.94915 0.729495 1.97097 0.740378 2.01412 0.7509 2.03483 0.761068 2.08325 0.770887 2.10314 0.780363 2.16554 0.789502 2.18511 0.798311 2.20486 0.806799 2.27323 0.814972 2.29358 0.822838 2.35642 0.830405 2.37779 0.837683 2.44338 0.844677 2.46557 0.851398 2.53644 0.857853 2.55852 0.86405 2.63443 0.869999 2.65559 0.875705 2.73616 0.881179 2.7563 0.886428 2.84308 0.89146 2.86267 0.896281 2.95173 0.900901 2.97145 0.905326 3.0662 0.909563 3.08672 0.91362 3.1822 0.917503 3.20381 0.92122 3.3037 0.924775 3.3259 0.928177 3.43257 0.931431 3.45424 0.934542 3.55773 0.937517 3.57836 0.940362 3.68823 0.94308 3.70818 0.945679 3.82821 0.948162 3.84828 0.950534 3.94262 0.952801 4.0308 0.954966 4.05261 0.957034 4.14703 0.95901 4.17013 0.960896 4.24142 0.962697 4.26452 0.964417 4.34393 0.966059 4.36601 0.967626 4.44882 0.969123 4.55567 0.970551 4.57716 0.971914 4.74652 0.973215 4.76902 0.974456 4.97749 0.97564 5.00192 0.976771 5.1791 0.977849 5.3449 0.978878 5.37001 0.97986 5.56546 0.980796 5.58937 0.981689 5.7299 0.982542 5.85883 0.983354 5.88282 0.984129 6.03149 0.984869 6.05761 0.985574 6.1885 0.986247 6.21668 0.986888 6.31209 0.9875 6.39976 0.988083 6.42673 0.98864 6.52452 0.98917 6.55128 0.989676 6.62425 0.990158 6.68862 0.990618 6.71939 0.991057 6.78617 0.991475 6.81837 0.991873 6.87032 0.992253 6.91762 0.992616 6.94871 0.992961 6.98863 0.993291 7.0216 0.993605 7.05664 0.993904 7.09288 0.994189 7.12932 0.994461 7.1653 0.994721 7.19224 0.994968 7.23231