ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET Summary Report Surface Area Single point surface area at P/Po = 0.291398515: 6.3947 m²/g BET Surface Area: 6.5343 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å width: 4.755 m²/g Pore Volume BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å width: 0.002804 cm³/g Pore Size BJH Adsorption average pore width (4V/A): 23.591 Å ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET Isotherm Tabular Report Quantity Relative Absolute Adsorbed Elapsed Saturation Pressure Pressure (cm³/g Time Pressure (P/Po) (mmHg) STP) (h:min) (mmHg) ----- 1.#QNAN0000 1.#QNAN0 1.#QNB 00:59 739.176270 0.011074975 8.186358 1.1528 01:20 1.#QNAN0 0.032807615 24.250610 1.3272 01:22 1.#QNAN0 0.056409557 41.696606 1.4328 01:24 1.#QNAN0 0.069956419 51.710125 1.4842 01:25 1.#QNAN0 0.090330379 66.770073 1.5520 01:26 1.#QNAN0 0.110464959 81.653076 1.6114 01:28 1.#QNAN0 0.130525616 96.481438 1.6676 01:29 1.#QNAN0 0.151098125 111.688148 1.7231 01:30 1.#QNAN0 0.170696307 126.174660 1.7736 01:32 1.#QNAN0 0.190820524 141.050003 1.8238 01:33 1.#QNAN0 0.211013203 155.975952 1.8740 01:34 1.#QNAN0 0.230890024 170.668427 1.9224 01:36 1.#QNAN0 0.251028783 185.554520 1.9726 01:37 1.#QNAN0 0.271241280 200.495117 2.0232 01:38 1.#QNAN0 0.291398515 215.394867 2.0731 01:39 1.#QNAN0 0.311467707 230.229538 2.1236 01:41 1.#QNAN0 0.350999334 259.450378 2.2235 01:42 1.#QNAN0 0.372332310 275.219208 2.2792 01:44 1.#QNAN0 0.391561437 289.432922 2.3280 01:45 1.#QNAN0 0.412388578 304.827850 2.3822 01:47 1.#QNAN0 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET Isotherm Linear Plot 000-596 rep595 cook 6CS-3 - Adsorption Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 0.011075 1.15283 0.0328076 1.32721 0.0564096 1.43284 0.0699564 1.48417 0.0903304 1.55199 0.110465 1.61136 0.130526 1.66756 0.151098 1.72308 0.170696 1.77359 0.190821 1.82379 0.211013 1.87403 0.23089 1.92239 0.251029 1.97256 0.271241 2.02321 0.291399 2.07306 0.311468 2.12356 0.350999 2.22347 0.372332 2.27925 0.391561 2.32801 0.412389 2.38222 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET Isotherm Log Plot 000-596 rep595 cook 6CS-3 - Adsorption Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 0.011075 1.15283 0.0328076 1.32721 0.0564096 1.43284 0.0699564 1.48417 0.0903304 1.55199 0.110465 1.61136 0.130526 1.66756 0.151098 1.72308 0.170696 1.77359 0.190821 1.82379 0.211013 1.87403 0.23089 1.92239 0.251029 1.97256 0.271241 2.02321 0.291399 2.07306 0.311468 2.12356 0.350999 2.22347 0.372332 2.27925 0.391561 2.32801 0.412389 2.38222 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET BET Surface Area Report BET Surface Area: 6.5343 ± 0.0282 m²/g Slope: 0.662462 ± 0.002824 g/cm³ STP Y-Intercept: 0.003746 ± 0.000527 g/cm³ STP C: 177.860322 Qm: 1.5010 cm³/g STP Correlation Coefficient: 0.9999000 Molecular Cross-Sectional Area: 0.1620 nm² Quantity Relative Adsorbed Pressure (cm³/g 1/[Q(Po/P (P/Po) STP) - 1)] --- 0.056409557 1.4328 0.041723 0.069956419 1.4842 0.050681 0.090330379 1.5520 0.063982 0.110464959 1.6114 0.077067 0.130525616 1.6676 0.090024 0.151098125 1.7231 0.103299 0.170696307 1.7736 0.116053 0.190820524 1.8238 0.129302 0.211013203 1.8740 0.142713 0.230890024 1.9224 0.156162 0.251028783 1.9726 0.169913 0.271241280 2.0232 0.183963 0.291398515 2.0731 0.198369 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET BET Surface Area Plot 000-596 rep595 cook 6CS-3 Relative Pressure (P/Po) 1/[Q(Po/P - 1)] 0.0564096 0.0417226 0.0699564 0.0506805 0.0903304 0.0639824 0.110465 0.0770672 0.130526 0.090024 0.151098 0.103299 0.170696 0.116053 0.190821 0.129302 0.211013 0.142713 0.23089 0.156162 0.251029 0.169913 0.271241 0.183963 0.291399 0.198369 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET t-Plot Reports Primary Data 4053- At least two data points must be selected for t-Plot calculations. 4053- At least two data points must be selected for t-Plot calculations. 4053- At least two data points must be selected for t-Plot calculations. ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET BJH Adsorption Pore Distribution Report Faas Correction Halsey t = 3.54 [ -5 / ln(P/Po) ] ^ 0.333 Width Range: 17.000 Å to 3000.000 Å Adsorbate Property Factor: 9.53000 Å Density Conversion Factor: 0.0015468 Fraction of Pores Open at Both Ends: 0.00 Incremental Cumulative Cumulative Average Pore Pore Incremental Pore Pore Width Width Volume Volume Pore Area Area Range (Å) (Å) (cm³/g) (cm³/g) (m²/g) (m²/g) ------ 33.1 - 31.7 32.4 0.000199 0.000199 0.246 0.246 31.7 - 30.4 31.0 0.000179 0.000378 0.231 0.477 30.4 - 29.1 29.7 0.000206 0.000584 0.277 0.755 29.1 - 26.8 27.8 0.000371 0.000955 0.533 1.287 26.8 - 25.7 26.2 0.000187 0.001142 0.285 1.572 25.7 - 24.7 25.2 0.000184 0.001327 0.293 1.865 24.7 - 23.6 24.1 0.000187 0.001514 0.311 2.176 23.6 - 22.6 23.1 0.000185 0.001699 0.320 2.496 22.6 - 21.7 22.1 0.000176 0.001875 0.318 2.814 21.7 - 20.7 21.2 0.000182 0.002057 0.344 3.158 20.7 - 19.8 20.2 0.000180 0.002237 0.355 3.513 19.8 - 18.9 19.3 0.000179 0.002416 0.372 3.885 18.9 - 17.9 18.3 0.000195 0.002611 0.426 4.311 17.9 - 16.9 17.4 0.000193 0.002804 0.443 4.755 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET BJH Adsorption dV/dw Pore Volume Halsey : Faas Correction 000-596 rep595 cook 6CS-3 Pore Width (Å) Pore Volume (cm³/g·Å) 32.3518 0.000139564 31.0218 0.000143565 29.7318 0.000156202 27.8468 0.000162164 26.2471 0.000171174 25.1711 0.000173888 24.1271 0.000182134 23.1144 0.00018538 22.1356 0.000182863 21.1736 0.00019001 20.2208 0.000190036 19.2909 0.000195878 18.3453 0.000202547 17.3831 0.000201439 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET BJH Adsorption dV/dw Pore Volume Halsey : Faas Correction 000-596 rep595 cook 6CS-3 Pore Width (Å) Pore Volume (cm³/g·Å) 32.3518 0.000139564 31.0218 0.000143565 29.7318 0.000156202 27.8468 0.000162164 26.2471 0.000171174 25.1711 0.000173888 24.1271 0.000182134 23.1144 0.00018538 22.1356 0.000182863 21.1736 0.00019001 20.2208 0.000190036 19.2909 0.000195878 18.3453 0.000202547 17.3831 0.000201439 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET BJH Adsorption dV/dlog(w) Pore Volume Halsey : Faas Correction 000-596 rep595 cook 6CS-3 Pore Width (Å) dV/dlog(w) Pore Volume (cm³/g·Å) 32.3518 0.0104075 31.0218 0.010264 29.7318 0.0107052 27.8468 0.0104366 26.2471 0.0103552 25.1711 0.0100884 24.1271 0.0101289 23.1144 0.00987694 22.1356 0.00933048 21.1736 0.00927482 20.2208 0.00885943 19.2909 0.00871223 18.3453 0.00856999 17.3831 0.00807747 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET BJH Adsorption Cumulative Pore Area Halsey : Faas Correction 000-596 rep595 cook 6CS-3 Pore Width (Å) Pore Area (m²/g) 31.6784 0.246001 30.4288 0.47732 29.1091 0.754638 26.8231 1.28715 25.7298 1.57233 24.6702 1.86513 23.6412 2.17587 22.644 2.49576 21.6823 2.81355 20.7227 3.15799 19.778 3.51315 18.8623 3.88505 17.8972 4.31127 16.941 4.75451 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET BJH Adsorption dA/dw Pore Area Halsey : Faas Correction 000-596 rep595 cook 6CS-3 Pore Width (Å) Pore Area (m²/g·Å) 32.3518 0.172558 31.0218 0.185114 29.7318 0.210148 27.8468 0.232937 26.2471 0.260866 25.1711 0.276329 24.1271 0.301958 23.1144 0.320804 22.1356 0.330441 21.1736 0.358956 20.2208 0.375922 19.2909 0.406156 18.3453 0.441631 17.3831 0.463527 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET BJH Adsorption dA/dlog(w) Pore Area Halsey : Faas Correction 000-596 rep595 cook 6CS-3 Pore Width (Å) dA/dlog(w) Pore Area (m²/g·Å) 32.3518 12.8679 31.0218 13.2345 29.7318 14.4023 27.8468 14.9915 26.2471 15.7811 25.1711 16.0317 24.1271 16.7925 23.1144 17.0923 22.1356 16.8606 21.1736 17.5214 20.2208 17.5254 19.2909 18.065 18.3453 18.686 17.3831 18.5869 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET BJH Desorption Reports Primary Data 1045- Fewer than 2 points available for BJH Desorption calculations. 1045- Fewer than 2 points available for BJH Desorption calculations. ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET Horvath-Kawazoe Reports Primary Data 4036- Fewer than 2 points available for Horvath-Kawazoe calculations. 4037- Computations failed while processing the primary data set. No reports will be produced. 4036- Fewer than 2 points available for Horvath-Kawazoe calculations. 4037- Computations failed while processing the primary data set. No reports will be produced. ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET Porosity Distribution by Original Density Functional Theory Model: N2 @ 77K on Carbon, Slit Pores Method: Non-negative Regularization; No Smoothing Standard Deviation of Fit: 0.00951, cm³/g STP Volume in Pores < 14.83 Å : 0.00089 cm³/g Total Volume in Pores <= 34.31 Å : 0.00176 cm³/g Area in Pores > 34.31 Å : 1.980 m²/g Total Area in Pores >= 14.83 Å : 2.693 m²/g Pore Size Table Cumulative Incremental Cumulative Pore Width Volume Volume Area Incremental (Å) (cm³/g) (cm³/g) (m²/g) Area (m²/g) ----- 14.83 0.00009 0.00009 0.117 0.117 15.91 0.00018 0.00010 0.237 0.120 17.16 0.00020 0.00002 0.255 0.018 18.59 0.00020 0.00000 0.255 0.000 20.02 0.00020 0.00000 0.255 0.000 21.62 0.00020 0.00000 0.255 0.000 23.41 0.00022 0.00003 0.277 0.022 25.20 0.00032 0.00009 0.351 0.073 27.34 0.00046 0.00014 0.455 0.104 29.49 0.00059 0.00013 0.546 0.092 31.81 0.00072 0.00013 0.629 0.082 34.31 0.00087 0.00014 0.713 0.084 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET Porosity Distribution by Original Density Functional Theory Model: N2 @ 77K on Carbon, Slit Pores Method: Non-negative Regularization; No Smoothing Standard Deviation of Fit: 0.00951, cm³/g STP Isotherm Table Fitted Experimental Quantity Absolute Quantity Adsorbed Residual Relative Adsorbed (cm³/g (cm³/g Relative Pressure (cm³/g STP) STP) STP) Residual ----- 0.011783670 1.1598 1.1617 -0.0020 -0.001699 0.014515520 1.1861 1.1839 0.0022 0.001848 0.017706521 1.2159 1.2276 -0.0117 -0.009587 0.021398440 1.2484 1.2490 -0.0006 -0.000477 0.025631230 1.2820 1.2706 0.0114 0.008928 0.030442240 1.3142 1.3171 -0.0029 -0.002198 0.035865448 1.3424 1.3402 0.0022 0.001648 0.041930798 1.3713 1.3691 0.0022 0.001607 0.048663601 1.4013 1.3952 0.0061 0.004337 0.056084011 1.4316 1.4237 0.0079 0.005506 0.064206667 1.4631 1.4551 0.0080 0.005457 0.073040441 1.4949 1.4894 0.0055 0.003703 0.082588248 1.5274 1.5259 0.0014 0.000940 0.092847057 1.5596 1.5634 -0.0038 -0.002422 0.103808001 1.5922 1.6002 -0.0080 -0.005028 0.115456402 1.6255 1.6353 -0.0098 -0.006042 0.127772301 1.6600 1.6682 -0.0082 -0.004966 0.140730694 1.6954 1.6990 -0.0036 -0.002114 0.154301897 1.7315 1.7357 -0.0042 -0.002415 0.168452203 1.7680 1.7629 0.0050 0.002849 0.183144197 1.8047 1.8178 -0.0131 -0.007279 0.198337302 1.8425 1.8427 -0.0002 -0.000126 0.213988706 1.8814 1.8671 0.0143 0.007583 0.230053306 1.9203 1.9376 -0.0173 -0.009010 0.246484801 1.9612 1.9613 -0.0001 -0.000045 0.263235897 2.0032 1.9852 0.0180 0.008983 0.280259013 2.0455 2.0545 -0.0090 -0.004390 0.297506303 2.0884 2.0791 0.0093 0.004447 0.314930797 2.1323 2.1499 -0.0176 -0.008259 0.332486212 2.1766 2.1761 0.0005 0.000219 0.350127310 2.2213 2.2036 0.0177 0.007951 0.367810607 2.2675 2.2832 -0.0157 -0.006912 0.385494202 2.3125 2.3123 0.0002 0.000071 0.403138310 2.3581 2.3422 0.0160 0.006766 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET Cumulative Surface Area vs. Pore Width Cumulative Surface Area Pore Width (Angstroms) Cumulative Surface Area (m²/g) 14.8329 0.116847 15.9052 0.236943 17.1561 0.255179 18.5858 0.255179 20.0155 0.255179 21.6239 0.255179 23.411 0.277417 25.198 0.350653 27.3426 0.454929 29.4871 0.546476 31.8103 0.628856 34.3122 0.713263 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET Incremental Surface Area vs. Pore Width Incremental Surface Area Pore Width (Angstroms) Incremental Surface Area (m²/g) 14.8329 0.116847 15.9052 0.120096 17.1561 0.0182355 18.5858 0 20.0155 0 21.6239 0 23.411 0.0222381 25.198 0.0732362 27.3426 0.104276 29.4871 0.0915473 31.8103 0.0823804 34.3122 0.0844067 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET Differential Surface Area vs. Pore Width Differential Surface Area Pore Width (Angstroms) Differential Surface Area (m²/g) 14.8329 3.85483 15.9052 3.80091 17.1561 0.539167 18.5858 0 20.0155 0 21.6239 0 23.411 0.669483 25.198 2.17253 27.3426 3.05503 29.4871 2.78562 31.8103 2.50331 34.3122 2.56702 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET Cumulative Pore Volume vs. Pore Width Cumulative Pore Volume Pore Width (Angstroms) Cumulative Pore Volume (cm³/g) 14.8329 8.66592e-005 15.9052 0.000182166 17.1561 0.000197809 18.5858 0.000197809 20.0155 0.000197809 21.6239 0.000197809 23.411 0.00022384 25.198 0.00031611 27.3426 0.000458668 29.4871 0.000593641 31.8103 0.000724669 34.3122 0.000869478 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET Incremental Pore Volume vs. Pore Width Incremental Pore Volume Pore Width (Angstroms) Incremental Pore Volume (cm³/g) 14.8329 8.66592e-005 15.9052 9.5507e-005 17.1561 1.56425e-005 18.5858 0 20.0155 0 21.6239 0 23.411 2.60308e-005 25.198 9.22705e-005 27.3426 0.000142558 29.4871 0.000134973 31.8103 0.000131027 34.3122 0.000144809 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET Differential Pore Volume vs. Pore Width Differential Pore Volume Pore Width (Angstroms) Differential Pore Volume (cm³/g) 14.8329 0.00285892 15.9052 0.0030227 17.1561 0.0004625 18.5858 0 20.0155 0 21.6239 0 23.411 0.000783662 25.198 0.00273718 27.3426 0.00417662 29.4871 0.00410698 31.8103 0.00398155 34.3122 0.00440401 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET Standard Deviation of Fit: 0.00951, cm³/g STP Goodness of Fit Input Data Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 0.011075 1.15283 0.0328076 1.32721 0.0564096 1.43284 0.0699564 1.48417 0.0903304 1.55199 0.110465 1.61136 0.130526 1.66756 0.151098 1.72308 0.170696 1.77359 0.190821 1.82379 0.211013 1.87403 0.23089 1.92239 0.251029 1.97256 0.271241 2.02321 0.291399 2.07306 0.311468 2.12356 0.350999 2.22347 0.372332 2.27925 0.391561 2.32801 0.412389 2.38222 Model Fit Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 0.0117837 1.16173 0.0145155 1.18394 0.0177065 1.22756 0.0213984 1.24897 0.0256312 1.27057 0.0304422 1.31711 0.0358654 1.34023 0.0419308 1.36913 0.0486636 1.3952 0.056084 1.4237 0.0642067 1.45507 0.0730404 1.48938 0.0825882 1.52594 0.0928471 1.5634 0.103808 1.60022 0.115456 1.6353 0.127772 1.66821 0.140731 1.69897 0.154302 1.73568 0.168452 1.76293 0.183144 1.8178 0.198337 1.84274 0.213989 1.8671 0.230053 1.93762 0.246485 1.9613 0.263236 1.98517 0.280259 2.05449 0.297506 2.07911 0.314931 2.1499 0.332486 2.17612 0.350127 2.2036 0.367811 2.28317 0.385494 2.31232 0.403138 2.34219 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-596 rep595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-596.SMP Started: 8/18/2017 12:28:02PM Analysis Adsorptive: N2 Completed: 8/18/2017 2:28:50PM Analysis Bath Temp.: -196.034 °C Report Time: 8/22/2017 11:39:28AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.5068 cm³ Measured Cold Free Space: 48.2110 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: No Comments: tube 15 ann cook 6 CS-3 core sed for BET Standard Deviation of Fit: 0.00951, cm³/g STP Goodness of Fit Input Data Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 0.011075 1.15283 0.0328076 1.32721 0.0564096 1.43284 0.0699564 1.48417 0.0903304 1.55199 0.110465 1.61136 0.130526 1.66756 0.151098 1.72308 0.170696 1.77359 0.190821 1.82379 0.211013 1.87403 0.23089 1.92239 0.251029 1.97256 0.271241 2.02321 0.291399 2.07306 0.311468 2.12356 0.350999 2.22347 0.372332 2.27925 0.391561 2.32801 0.412389 2.38222 Model Fit Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 0.0117837 1.16173 0.0145155 1.18394 0.0177065 1.22756 0.0213984 1.24897 0.0256312 1.27057 0.0304422 1.31711 0.0358654 1.34023 0.0419308 1.36913 0.0486636 1.3952 0.056084 1.4237 0.0642067 1.45507 0.0730404 1.48938 0.0825882 1.52594 0.0928471 1.5634 0.103808 1.60022 0.115456 1.6353 0.127772 1.66821 0.140731 1.69897 0.154302 1.73568 0.168452 1.76293 0.183144 1.8178 0.198337 1.84274 0.213989 1.8671 0.230053 1.93762 0.246485 1.9613 0.263236 1.98517 0.280259 2.05449 0.297506 2.07911 0.314931 2.1499 0.332486 2.17612 0.350127 2.2036 0.367811 2.28317 0.385494 2.31232 0.403138 2.34219