ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET Summary Report Surface Area Single point surface area at P/Po = 0.291258978: 6.4355 m²/g BET Surface Area: 6.5722 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å width: 4.743 m²/g Pore Volume BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å width: 0.002807 cm³/g Pore Size BJH Adsorption average pore width (4V/A): 23.674 Å ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET Isotherm Tabular Report Quantity Relative Absolute Adsorbed Elapsed Saturation Pressure Pressure (cm³/g Time Pressure (P/Po) (mmHg) STP) (h:min) (mmHg) ----- 1.#QNAN0000 1.#QNAN0 1.#QNB 00:57 739.056641 0.011061777 8.175280 1.1674 01:17 1.#QNAN0 0.032475681 24.001368 1.3406 01:19 1.#QNAN0 0.056379547 41.667679 1.4486 01:21 1.#QNAN0 0.069927250 51.680199 1.5010 01:22 1.#QNAN0 0.090418904 66.824692 1.5678 01:23 1.#QNAN0 0.110448567 81.627747 1.6270 01:25 1.#QNAN0 0.130521658 96.462898 1.6822 01:26 1.#QNAN0 0.150652725 111.340897 1.7362 01:27 1.#QNAN0 0.171237205 126.553993 1.7894 01:29 1.#QNAN0 0.190779583 140.996918 1.8383 01:30 1.#QNAN0 0.210867406 155.842957 1.8881 01:31 1.#QNAN0 0.231046485 170.756439 1.9380 01:33 1.#QNAN0 0.251063718 185.550308 1.9874 01:34 1.#QNAN0 0.271327159 200.526138 2.0368 01:35 1.#QNAN0 0.291258978 215.256882 2.0859 01:37 1.#QNAN0 0.312214709 230.744354 2.1380 01:38 1.#QNAN0 0.351083898 259.470886 2.2347 01:39 1.#QNAN0 0.371384832 274.474426 2.2881 01:41 1.#QNAN0 0.391565728 289.389252 2.3393 01:42 1.#QNAN0 0.412737565 305.036438 2.3939 01:44 1.#QNAN0 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET Isotherm Linear Plot 000-595 cook 6CS-3 - Adsorption Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 0.0110618 1.16742 0.0324757 1.34058 0.0563795 1.44859 0.0699273 1.50104 0.0904189 1.56778 0.110449 1.62698 0.130522 1.68221 0.150653 1.73616 0.171237 1.7894 0.19078 1.83834 0.210867 1.88806 0.231046 1.93801 0.251064 1.98736 0.271327 2.03683 0.291259 2.08588 0.312215 2.13796 0.351084 2.23474 0.371385 2.28806 0.391566 2.33934 0.412738 2.39385 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET Isotherm Log Plot 000-595 cook 6CS-3 - Adsorption Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 0.0110618 1.16742 0.0324757 1.34058 0.0563795 1.44859 0.0699273 1.50104 0.0904189 1.56778 0.110449 1.62698 0.130522 1.68221 0.150653 1.73616 0.171237 1.7894 0.19078 1.83834 0.210867 1.88806 0.231046 1.93801 0.251064 1.98736 0.271327 2.03683 0.291259 2.08588 0.312215 2.13796 0.351084 2.23474 0.371385 2.28806 0.391566 2.33934 0.412738 2.39385 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET BET Surface Area Report BET Surface Area: 6.5722 ± 0.0300 m²/g Slope: 0.658948 ± 0.002971 g/cm³ STP Y-Intercept: 0.003421 ± 0.000555 g/cm³ STP C: 193.616713 Qm: 1.5097 cm³/g STP Correlation Coefficient: 0.9998882 Molecular Cross-Sectional Area: 0.1620 nm² Quantity Relative Adsorbed Pressure (cm³/g 1/[Q(Po/P (P/Po) STP) - 1)] --- 0.056379547 1.4486 0.041246 0.069927250 1.5010 0.050088 0.090418904 1.5678 0.063406 0.110448567 1.6270 0.076315 0.130521658 1.6822 0.089237 0.150652725 1.7362 0.102165 0.171237205 1.7894 0.115468 0.190779583 1.8383 0.128245 0.210867406 1.8881 0.141528 0.231046485 1.9380 0.155040 0.251063718 1.9874 0.168679 0.271327159 2.0368 0.182813 0.291258978 2.0859 0.197016 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET BET Surface Area Plot 000-595 cook 6CS-3 Relative Pressure (P/Po) 1/[Q(Po/P - 1)] 0.0563795 0.0412456 0.0699273 0.0500884 0.0904189 0.0634065 0.110449 0.0763146 0.130522 0.0892367 0.150653 0.102165 0.171237 0.115468 0.19078 0.128245 0.210867 0.141528 0.231046 0.15504 0.251064 0.168679 0.271327 0.182813 0.291259 0.197016 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET t-Plot Reports Primary Data 4053- At least two data points must be selected for t-Plot calculations. 4053- At least two data points must be selected for t-Plot calculations. 4053- At least two data points must be selected for t-Plot calculations. ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET BJH Adsorption Pore Distribution Report Faas Correction Halsey t = 3.54 [ -5 / ln(P/Po) ] ^ 0.333 Width Range: 17.000 Å to 3000.000 Å Adsorbate Property Factor: 9.53000 Å Density Conversion Factor: 0.0015468 Fraction of Pores Open at Both Ends: 0.00 Incremental Cumulative Cumulative Average Pore Pore Incremental Pore Pore Width Width Volume Volume Pore Area Area Range (Å) (Å) (cm³/g) (cm³/g) (m²/g) (m²/g) ------ 33.2 - 31.8 32.4 0.000201 0.000201 0.248 0.248 31.8 - 30.4 31.1 0.000190 0.000391 0.244 0.492 30.4 - 29.2 29.8 0.000198 0.000589 0.266 0.758 29.2 - 26.9 28.0 0.000361 0.000949 0.516 1.274 26.9 - 25.8 26.3 0.000194 0.001143 0.295 1.569 25.8 - 24.8 25.2 0.000182 0.001326 0.289 1.858 24.8 - 23.7 24.2 0.000184 0.001509 0.303 2.161 23.7 - 22.7 23.2 0.000183 0.001692 0.316 2.476 22.7 - 21.8 22.2 0.000184 0.001877 0.332 2.808 21.8 - 20.8 21.2 0.000182 0.002058 0.342 3.151 20.8 - 19.9 20.3 0.000177 0.002236 0.349 3.499 19.9 - 18.9 19.4 0.000191 0.002427 0.395 3.894 18.9 - 18.0 18.4 0.000191 0.002618 0.415 4.310 18.0 - 17.0 17.5 0.000189 0.002807 0.434 4.743 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET BJH Adsorption dV/dw Pore Volume Halsey : Faas Correction 000-595 cook 6CS-3 Pore Width (Å) Pore Volume (cm³/g·Å) 32.4416 0.000138624 31.0675 0.000144771 29.7866 0.000157909 27.9526 0.000160269 26.3401 0.000169826 25.2489 0.000174154 24.2087 0.000177888 23.1981 0.000184605 22.2137 0.000188838 21.2481 0.000190437 20.3129 0.000193043 19.3687 0.000198941 18.4149 0.00020233 17.4612 0.000197811 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET BJH Adsorption dV/dw Pore Volume Halsey : Faas Correction 000-595 cook 6CS-3 Pore Width (Å) Pore Volume (cm³/g·Å) 32.4416 0.000138624 31.0675 0.000144771 29.7866 0.000157909 27.9526 0.000160269 26.3401 0.000169826 25.2489 0.000174154 24.2087 0.000177888 23.1981 0.000184605 22.2137 0.000188838 21.2481 0.000190437 20.3129 0.000193043 19.3687 0.000198941 18.4149 0.00020233 17.4612 0.000197811 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET BJH Adsorption dV/dlog(w) Pore Volume Halsey : Faas Correction 000-595 cook 6CS-3 Pore Width (Å) dV/dlog(w) Pore Volume (cm³/g·Å) 32.4416 0.0103664 31.0675 0.0103664 29.7866 0.010841 27.9526 0.0103525 26.3401 0.0103109 25.2489 0.0101348 24.2087 0.00992625 23.1981 0.00987112 22.2137 0.00966967 21.2481 0.00932824 20.3129 0.00903986 19.3687 0.00888537 18.4149 0.00859267 17.4612 0.00796761 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET BJH Adsorption Cumulative Pore Area Halsey : Faas Correction 000-595 cook 6CS-3 Pore Width (Å) Pore Area (m²/g) 31.7573 0.24782 30.4474 0.491986 29.1929 0.758005 26.9432 1.27396 25.801 1.56852 24.7533 1.85758 23.7216 2.16084 22.7303 2.47637 21.754 2.80836 20.7995 3.15055 19.8819 3.49935 18.9202 3.89449 17.9757 4.30958 17.0188 4.74317 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET BJH Adsorption dA/dw Pore Area Halsey : Faas Correction 000-595 cook 6CS-3 Pore Width (Å) Pore Area (m²/g·Å) 32.4416 0.170922 31.0675 0.186396 29.7866 0.212055 27.9526 0.229344 26.3401 0.257897 25.2489 0.275899 24.2087 0.293925 23.1981 0.318311 22.2137 0.340038 21.2481 0.358502 20.3129 0.380139 19.3687 0.410849 18.4149 0.439492 17.4612 0.453143 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET BJH Adsorption dA/dlog(w) Pore Area Halsey : Faas Correction 000-595 cook 6CS-3 Pore Width (Å) dA/dlog(w) Pore Area (m²/g·Å) 32.4416 12.7816 31.0675 13.3469 29.7866 14.5582 27.9526 14.8144 26.3401 15.6581 25.2489 16.0558 24.2087 16.4011 23.1981 17.0206 22.2137 17.4121 21.2481 17.5606 20.3129 17.8013 19.3687 18.3499 18.4149 18.6646 17.4612 18.2521 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET BJH Desorption Reports Primary Data 1045- Fewer than 2 points available for BJH Desorption calculations. 1045- Fewer than 2 points available for BJH Desorption calculations. ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET Horvath-Kawazoe Reports Primary Data 4036- Fewer than 2 points available for Horvath-Kawazoe calculations. 4037- Computations failed while processing the primary data set. No reports will be produced. 4036- Fewer than 2 points available for Horvath-Kawazoe calculations. 4037- Computations failed while processing the primary data set. No reports will be produced. ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET Porosity Distribution by Original Density Functional Theory Model: N2 @ 77K on Carbon, Slit Pores Method: Non-negative Regularization; No Smoothing Standard Deviation of Fit: 0.00951, cm³/g STP Volume in Pores < 14.83 Å : 0.00099 cm³/g Total Volume in Pores <= 34.31 Å : 0.00184 cm³/g Area in Pores > 34.31 Å : 1.893 m²/g Total Area in Pores >= 14.83 Å : 2.580 m²/g Pore Size Table Cumulative Incremental Cumulative Pore Width Volume Volume Area Incremental (Å) (cm³/g) (cm³/g) (m²/g) Area (m²/g) ----- 14.83 0.00008 0.00008 0.103 0.103 15.91 0.00016 0.00008 0.209 0.106 17.16 0.00017 0.00001 0.223 0.014 18.59 0.00017 0.00000 0.223 0.000 20.02 0.00017 0.00000 0.223 0.000 21.62 0.00017 0.00000 0.223 0.000 23.41 0.00020 0.00003 0.245 0.022 25.20 0.00029 0.00009 0.320 0.075 27.34 0.00044 0.00015 0.427 0.107 29.49 0.00057 0.00013 0.517 0.090 31.81 0.00070 0.00013 0.600 0.083 34.31 0.00085 0.00015 0.687 0.087 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET Porosity Distribution by Original Density Functional Theory Model: N2 @ 77K on Carbon, Slit Pores Method: Non-negative Regularization; No Smoothing Standard Deviation of Fit: 0.00951, cm³/g STP Isotherm Table Fitted Experimental Quantity Absolute Quantity Adsorbed Residual Relative Adsorbed (cm³/g (cm³/g Relative Pressure (cm³/g STP) STP) STP) Residual ----- 0.011783670 1.1745 1.1760 -0.0015 -0.001288 0.014515520 1.2011 1.1993 0.0018 0.001457 0.017706521 1.2311 1.2416 -0.0106 -0.008582 0.021398440 1.2637 1.2643 -0.0006 -0.000474 0.025631230 1.2975 1.2871 0.0104 0.007983 0.030442240 1.3295 1.3318 -0.0023 -0.001766 0.035865448 1.3575 1.3558 0.0017 0.001264 0.041930798 1.3864 1.3842 0.0022 0.001616 0.048663601 1.4166 1.4108 0.0058 0.004080 0.056084011 1.4474 1.4397 0.0077 0.005334 0.064206667 1.4798 1.4713 0.0086 0.005780 0.073040441 1.5117 1.5056 0.0061 0.004042 0.082588248 1.5433 1.5420 0.0013 0.000832 0.092847057 1.5751 1.5792 -0.0041 -0.002610 0.103808001 1.6079 1.6158 -0.0078 -0.004870 0.115456402 1.6409 1.6506 -0.0097 -0.005888 0.127772301 1.6748 1.6832 -0.0085 -0.005046 0.140730694 1.7097 1.7137 -0.0040 -0.002329 0.154301897 1.7458 1.7501 -0.0044 -0.002493 0.168452203 1.7823 1.7771 0.0052 0.002929 0.183144197 1.8193 1.8326 -0.0133 -0.007286 0.198337302 1.8570 1.8573 -0.0002 -0.000131 0.213988706 1.8958 1.8814 0.0144 0.007600 0.230053306 1.9356 1.9527 -0.0171 -0.008834 0.246484801 1.9761 1.9760 0.0001 0.000056 0.263235897 2.0171 1.9995 0.0176 0.008722 0.280259013 2.0587 2.0678 -0.0091 -0.004421 0.297506303 2.1014 2.0920 0.0094 0.004480 0.314930797 2.1447 2.1623 -0.0176 -0.008206 0.332486212 2.1884 2.1879 0.0005 0.000217 0.350127310 2.2323 2.2147 0.0177 0.007910 0.367810607 2.2788 2.2953 -0.0165 -0.007237 0.385494202 2.3238 2.3235 0.0003 0.000128 0.403138310 2.3691 2.3525 0.0167 0.007032 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET Cumulative Surface Area vs. Pore Width Cumulative Surface Area Pore Width (Angstroms) Cumulative Surface Area (m²/g) 14.8329 0.102888 15.9052 0.20909 17.1561 0.222706 18.5858 0.222706 20.0155 0.222706 21.6239 0.222706 23.411 0.244742 25.198 0.320094 27.3426 0.426708 29.4871 0.517166 31.8103 0.59971 34.3122 0.687066 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET Incremental Surface Area vs. Pore Width Incremental Surface Area Pore Width (Angstroms) Incremental Surface Area (m²/g) 14.8329 0.102888 15.9052 0.106202 17.1561 0.013616 18.5858 0 20.0155 0 21.6239 0 23.411 0.0220356 25.198 0.0753526 27.3426 0.106614 29.4871 0.0904578 31.8103 0.0825439 34.3122 0.0873558 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET Differential Surface Area vs. Pore Width Differential Surface Area Pore Width (Angstroms) Differential Surface Area (m²/g) 14.8329 3.39432 15.9052 3.36118 17.1561 0.402583 18.5858 0 20.0155 0 21.6239 0 23.411 0.663387 25.198 2.23531 27.3426 3.12354 29.4871 2.75247 31.8103 2.50827 34.3122 2.65671 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET Cumulative Pore Volume vs. Pore Width Cumulative Pore Volume Pore Width (Angstroms) Cumulative Pore Volume (cm³/g) 14.8329 7.63067e-005 15.9052 0.000160764 17.1561 0.000172444 18.5858 0.000172444 20.0155 0.000172444 21.6239 0.000172444 23.411 0.000198238 25.198 0.000293175 27.3426 0.00043893 29.4871 0.000572297 31.8103 0.000703584 34.3122 0.000853453 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET Incremental Pore Volume vs. Pore Width Incremental Pore Volume Pore Width (Angstroms) Incremental Pore Volume (cm³/g) 14.8329 7.63067e-005 15.9052 8.44577e-005 17.1561 1.16799e-005 18.5858 0 20.0155 0 21.6239 0 23.411 2.57938e-005 25.198 9.49369e-005 27.3426 0.000145755 29.4871 0.000133367 31.8103 0.000131287 34.3122 0.000149869 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET Differential Pore Volume vs. Pore Width Differential Pore Volume Pore Width (Angstroms) Differential Pore Volume (cm³/g) 14.8329 0.00251738 15.9052 0.002673 17.1561 0.000345338 18.5858 0 20.0155 0 21.6239 0 23.411 0.000776526 25.198 0.00281628 27.3426 0.00427027 29.4871 0.00405811 31.8103 0.00398945 34.3122 0.00455788 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET Standard Deviation of Fit: 0.00951, cm³/g STP Goodness of Fit Input Data Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 0.0110618 1.16742 0.0324757 1.34058 0.0563795 1.44859 0.0699273 1.50104 0.0904189 1.56778 0.110449 1.62698 0.130522 1.68221 0.150653 1.73616 0.171237 1.7894 0.19078 1.83834 0.210867 1.88806 0.231046 1.93801 0.251064 1.98736 0.271327 2.03683 0.291259 2.08588 0.312215 2.13796 0.351084 2.23474 0.371385 2.28806 0.391566 2.33934 0.412738 2.39385 Model Fit Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 0.0117837 1.17604 0.0145155 1.19934 0.0177065 1.24165 0.0213984 1.26433 0.0256312 1.2871 0.0304422 1.33182 0.0358654 1.35578 0.0419308 1.38421 0.0486636 1.41083 0.056084 1.4397 0.0642067 1.47127 0.0730404 1.5056 0.0825882 1.54203 0.0928471 1.57925 0.103808 1.61578 0.115456 1.65057 0.127772 1.68321 0.140731 1.71372 0.154302 1.75011 0.168452 1.77713 0.183144 1.83259 0.198337 1.85729 0.213989 1.88138 0.230053 1.95265 0.246485 1.97599 0.263236 1.99949 0.280259 2.06784 0.297506 2.09198 0.314931 2.16232 0.332486 2.18791 0.350127 2.21469 0.367811 2.29526 0.385494 2.32353 0.403138 2.35247 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-595 cook 6CS-3 Operator: jms saw Submitter: File: C:\...\DOCUME~1\000-595.SMP Started: 8/18/2017 9:43:07AM Analysis Adsorptive: N2 Completed: 8/18/2017 11:40:59AM Analysis Bath Temp.: -196.035 °C Report Time: 8/22/2017 11:36:14AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4317 cm³ Measured Cold Free Space: 48.2577 cm³ Equilibration Interval: 30 s Low Pressure Dose: None Automatic Degas: Yes Comments: tube 15 ann cook 6 CS-3 core sed for BET Standard Deviation of Fit: 0.00951, cm³/g STP Goodness of Fit Input Data Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 0.0110618 1.16742 0.0324757 1.34058 0.0563795 1.44859 0.0699273 1.50104 0.0904189 1.56778 0.110449 1.62698 0.130522 1.68221 0.150653 1.73616 0.171237 1.7894 0.19078 1.83834 0.210867 1.88806 0.231046 1.93801 0.251064 1.98736 0.271327 2.03683 0.291259 2.08588 0.312215 2.13796 0.351084 2.23474 0.371385 2.28806 0.391566 2.33934 0.412738 2.39385 Model Fit Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 0.0117837 1.17604 0.0145155 1.19934 0.0177065 1.24165 0.0213984 1.26433 0.0256312 1.2871 0.0304422 1.33182 0.0358654 1.35578 0.0419308 1.38421 0.0486636 1.41083 0.056084 1.4397 0.0642067 1.47127 0.0730404 1.5056 0.0825882 1.54203 0.0928471 1.57925 0.103808 1.61578 0.115456 1.65057 0.127772 1.68321 0.140731 1.71372 0.154302 1.75011 0.168452 1.77713 0.183144 1.83259 0.198337 1.85729 0.213989 1.88138 0.230053 1.95265 0.246485 1.97599 0.263236 1.99949 0.280259 2.06784 0.297506 2.09198 0.314931 2.16232 0.332486 2.18791 0.350127 2.21469 0.367811 2.29526 0.385494 2.32353 0.403138 2.35247