ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Summary Report Surface Area Single point surface area at P/Po = 0.291848140: 5.2629 m²/g BET Surface Area: 5.4581 m²/g t-Plot External Surface Area: 6.2451 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å width: 4.507 m²/g BJH Desorption cumulative surface area of pores between 17.000 Å and 3000.000 Å width: 6.1352 m²/g Pore Volume Single point desorption total pore volume of pores less than 1022.447 Å width at P/Po = 0.980691103: 0.013741 cm³/g t-Plot micropore volume: -0.000386 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å width: 0.013130 cm³/g BJH Desorption cumulative volume of pores between 17.000 Å and 3000.000 Å width: 0.014001 cm³/g Pore Size Desorption average pore width (4V/A by BET): 100.7060 Å BJH Adsorption average pore width (4V/A): 116.535 Å BJH Desorption average pore width (4V/A): 91.281 Å Horvath-Kawazoe Maximum pore volume at P/Po = 0.010011879: 0.001251 cm³/g Median pore width: 7.335 Å ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Isotherm Tabular Report Quantity Relative Absolute Adsorbed Elapsed Saturation Pressure Pressure (cm³/g Time Pressure (P/Po) (mmHg) STP) (h:min) (mmHg) ----- 1.#QNAN0000 1.#QNAN0 1.#QNB 00:56 742.602661 0.000005315 0.003947 0.0128 01:47 1.#QNAN0 0.000003028 0.002249 0.0266 02:26 1.#QNAN0 0.000002553 0.001896 0.0404 03:05 1.#QNAN0 0.000002984 0.002217 0.0541 03:44 1.#QNAN0 0.000004228 0.003140 0.0675 04:23 1.#QNAN0 0.000006423 0.004771 0.0815 04:33 1.#QNAN0 0.000009486 0.007046 0.0955 04:43 1.#QNAN0 0.000013704 0.010179 0.1092 04:52 1.#QNAN0 0.000019092 0.014181 0.1227 05:01 1.#QNAN0 0.000025807 0.019169 0.1360 05:09 1.#QNAN0 0.000033911 0.025189 0.1489 05:17 1.#QNAN0 0.000044426 0.033000 0.1629 05:26 1.#QNAN0 0.000056495 0.041964 0.1764 05:34 1.#QNAN0 0.000069913 0.051932 0.1894 05:42 1.#QNAN0 0.000082363 0.061180 0.1996 05:51 1.#QNAN0 0.000095382 0.070852 0.2098 06:00 1.#QNAN0 0.000114564 0.085101 0.2229 06:08 1.#QNAN0 0.000130364 0.096838 0.2329 06:17 1.#QNAN0 0.000147920 0.109880 0.2428 06:25 1.#QNAN0 0.000166600 0.123758 0.2525 06:34 1.#QNAN0 0.000186319 0.138407 0.2622 06:42 1.#QNAN0 0.000207299 0.153993 0.2718 06:51 1.#QNAN0 0.000229665 0.170609 0.2812 06:59 1.#QNAN0 0.000253758 0.188508 0.2905 07:07 1.#QNAN0 0.000278572 0.206944 0.2998 07:16 1.#QNAN0 0.000304873 0.226484 0.3090 07:24 1.#QNAN0 0.000340502 0.252953 0.3209 07:31 1.#QNAN0 0.000378057 0.280855 0.3325 07:38 1.#QNAN0 0.000416886 0.309703 0.3438 07:46 1.#QNAN0 0.000456972 0.339485 0.3546 07:53 1.#QNAN0 0.000497242 0.369403 0.3650 08:00 1.#QNAN0 0.000538435 0.400009 0.3748 08:07 1.#QNAN0 0.000580865 0.431533 0.3845 08:14 1.#QNAN0 0.000623933 0.463533 0.3937 08:22 1.#QNAN0 0.000666468 0.495137 0.4024 08:29 1.#QNAN0 0.000709517 0.527122 0.4108 08:36 1.#QNAN0 0.000752883 0.559344 0.4188 08:43 1.#QNAN0 0.000796511 0.591761 0.4264 08:50 1.#QNAN0 0.000839010 0.623340 0.4337 08:58 1.#QNAN0 0.000881528 0.654933 0.4406 09:05 1.#QNAN0 0.000923552 0.686159 0.4473 09:12 1.#QNAN0 0.000965114 0.717042 0.4535 09:19 1.#QNAN0 0.001005638 0.747155 0.4594 09:26 1.#QNAN0 0.001045507 0.776782 0.4649 09:33 1.#QNAN0 0.001084558 0.805802 0.4702 09:41 1.#QNAN0 0.001122731 0.834169 0.4751 09:48 1.#QNAN0 0.001159458 0.861462 0.4798 09:55 1.#QNAN0 0.001195886 0.888534 0.4842 10:02 1.#QNAN0 0.001230583 0.914320 0.4884 10:09 1.#QNAN0 0.001264556 0.939568 0.4923 10:16 1.#QNAN0 0.001296858 0.963575 0.4960 10:23 1.#QNAN0 0.001328401 0.987018 0.4994 10:30 1.#QNAN0 0.001358960 1.009731 0.5026 10:37 1.#QNAN0 0.001387801 1.031167 0.5055 10:44 1.#QNAN0 0.001446770 1.074990 0.5121 10:52 1.#QNAN0 0.001507105 1.119829 0.5185 10:59 1.#QNAN0 0.001568550 1.165493 0.5249 11:07 1.#QNAN0 0.001630794 1.211752 0.5312 11:15 1.#QNAN0 0.001694629 1.259193 0.5373 11:22 1.#QNAN0 0.001759233 1.307207 0.5434 11:30 1.#QNAN0 0.001825401 1.356383 0.5494 11:37 1.#QNAN0 0.001892422 1.406194 0.5553 11:45 1.#QNAN0 0.001960790 1.457005 0.5611 11:52 1.#QNAN0 0.002030108 1.508526 0.5669 12:00 1.#QNAN0 0.002100724 1.561009 0.5725 12:07 1.#QNAN0 0.002172180 1.614117 0.5781 12:14 1.#QNAN0 0.002244357 1.667762 0.5836 12:21 1.#QNAN0 0.002336533 1.736269 0.5905 12:28 1.#QNAN0 0.002422451 1.800127 0.5967 12:35 1.#QNAN0 0.002499043 1.857056 0.6019 12:43 1.#QNAN0 0.002577668 1.915500 0.6069 12:52 1.#QNAN0 0.002656515 1.974105 0.6118 12:59 1.#QNAN0 0.002736416 2.033497 0.6167 13:07 1.#QNAN0 0.002817928 2.094086 0.6215 13:15 1.#QNAN0 0.002899530 2.154744 0.6262 13:23 1.#QNAN0 0.002982918 2.216727 0.6308 13:30 1.#QNAN0 0.003067348 2.279488 0.6353 13:38 1.#QNAN0 0.003151951 2.342376 0.6398 13:45 1.#QNAN0 0.003237984 2.406330 0.6442 13:53 1.#QNAN0 0.003325906 2.471689 0.6485 14:01 1.#QNAN0 0.003413134 2.536531 0.6527 14:08 1.#QNAN0 0.003502623 2.603054 0.6569 14:15 1.#QNAN0 0.003593184 2.670377 0.6609 14:23 1.#QNAN0 0.003683608 2.737599 0.6649 14:31 1.#QNAN0 0.003776485 2.806645 0.6688 14:39 1.#QNAN0 0.003869760 2.875986 0.6726 14:46 1.#QNAN0 0.003963470 2.945653 0.6764 14:54 1.#QNAN0 0.004057552 3.015595 0.6801 15:01 1.#QNAN0 0.004154169 3.087425 0.6836 15:09 1.#QNAN0 0.004251400 3.159709 0.6871 15:16 1.#QNAN0 0.004378980 3.254550 0.6920 15:23 1.#QNAN0 0.004478609 3.328622 0.6952 15:31 1.#QNAN0 0.004578968 3.403238 0.6984 15:39 1.#QNAN0 0.004679767 3.478182 0.7016 15:47 1.#QNAN0 0.004781978 3.554180 0.7046 15:56 1.#QNAN0 0.004885634 3.631250 0.7076 16:04 1.#QNAN0 0.004989578 3.708535 0.7105 16:12 1.#QNAN0 0.005093182 3.785568 0.7134 16:20 1.#QNAN0 0.005199667 3.864744 0.7161 16:28 1.#QNAN0 0.005305868 3.943706 0.7189 16:35 1.#QNAN0 0.005413460 4.023707 0.7215 16:43 1.#QNAN0 0.005521804 4.104269 0.7241 16:51 1.#QNAN0 0.005630319 4.184958 0.7266 16:59 1.#QNAN0 0.005739690 4.266285 0.7290 17:07 1.#QNAN0 0.005849534 4.347965 0.7315 17:15 1.#QNAN0 0.005961651 4.431336 0.7338 17:23 1.#QNAN0 0.006073149 4.514248 0.7361 17:31 1.#QNAN0 0.006185309 4.597653 0.7384 17:39 1.#QNAN0 0.006297113 4.680790 0.7405 17:46 1.#QNAN0 0.006410552 4.765149 0.7427 17:54 1.#QNAN0 0.006524464 4.849860 0.7447 18:02 1.#QNAN0 0.006639729 4.935574 0.7467 18:09 1.#QNAN0 0.006755766 5.021867 0.7486 18:17 1.#QNAN0 1.#QNAN0000 1.#QNAN0 1.#QNB 18:19 743.346741 0.007392127 5.495018 0.7621 18:27 1.#QNAN0 0.008035608 5.973442 0.7746 18:33 1.#QNAN0 0.008695166 6.463830 0.7865 18:39 1.#QNAN0 0.009344890 6.946939 0.7983 18:46 1.#QNAN0 0.010011879 7.442810 0.8089 18:48 1.#QNAN0 0.030288303 22.516422 0.9711 18:51 1.#QNAN0 0.056312836 41.863243 1.0833 18:52 1.#QNAN0 0.069919266 51.978455 1.1316 18:53 1.#QNAN0 0.090338715 67.158730 1.1935 18:55 1.#QNAN0 0.110435862 82.099350 1.2505 18:56 1.#QNAN0 0.130476959 96.998604 1.3037 18:58 1.#QNAN0 0.150600396 111.958946 1.3557 18:59 1.#QNAN0 0.170562061 126.799095 1.4062 19:00 1.#QNAN0 0.190734927 141.796326 1.4566 19:01 1.#QNAN0 0.211215533 157.022781 1.5069 19:03 1.#QNAN0 0.230770163 171.560577 1.5560 19:04 1.#QNAN0 0.250865264 186.500244 1.6047 19:05 1.#QNAN0 0.270866772 201.370880 1.6554 19:07 1.#QNAN0 0.291848140 216.969604 1.7072 19:08 1.#QNAN0 0.311206479 231.361786 1.7563 19:09 1.#QNAN0 0.331570386 246.502197 1.8089 19:11 1.#QNAN0 0.351421369 261.260803 1.8606 19:12 1.#QNAN0 0.371393210 276.109985 1.9120 19:14 1.#QNAN0 0.391600795 291.133881 1.9635 19:15 1.#QNAN0 0.412448116 306.634186 2.0175 19:17 1.#QNAN0 0.431640617 320.903595 2.0686 19:18 1.#QNAN0 0.452494948 336.409363 2.1220 19:20 1.#QNAN0 0.472617287 351.370239 2.1754 19:21 1.#QNAN0 0.493030953 366.548645 2.2294 19:23 1.#QNAN0 0.512859068 381.290955 2.2831 19:24 1.#QNAN0 0.533015848 396.278625 2.3387 19:26 1.#QNAN0 0.553034680 411.162903 2.3941 19:27 1.#QNAN0 0.573176273 426.138519 2.4514 19:28 1.#QNAN0 0.593276587 441.084564 2.5110 19:30 1.#QNAN0 0.613377140 456.029846 2.5727 19:31 1.#QNAN0 0.633379099 470.903015 2.6377 19:33 1.#QNAN0 0.653992426 486.230865 2.7078 19:35 1.#QNAN0 0.673588254 500.801178 2.7792 19:36 1.#QNAN0 0.693633815 515.707153 2.8573 19:38 1.#QNAN0 0.713820561 530.716980 2.9419 19:39 1.#QNAN0 0.733941291 545.677795 3.0352 19:40 1.#QNAN0 0.753898824 560.518677 3.1352 19:42 1.#QNAN0 0.774092049 575.533569 3.2464 19:43 1.#QNAN0 0.794062712 590.384460 3.3704 19:45 1.#QNAN0 0.814271623 605.411194 3.5120 19:46 1.#QNAN0 0.834305256 620.307678 3.6754 19:47 1.#QNAN0 0.854488470 635.316956 3.8644 19:49 1.#QNAN0 0.874257614 650.016968 4.0877 19:50 1.#QNAN0 0.894399777 664.995972 4.3790 19:52 1.#QNAN0 0.914657660 680.061157 4.7426 19:54 1.#QNAN0 0.934178104 694.578186 5.2153 19:56 1.#QNAN0 0.954008857 709.327759 5.9206 19:59 1.#QNAN0 0.973144531 723.560730 7.0502 20:02 1.#QNAN0 0.990593523 736.545044 9.2856 20:08 1.#QNAN0 0.980691103 729.185669 8.8838 20:10 1.#QNAN0 0.967695019 719.529358 7.9152 20:14 1.#QNAN0 0.948312890 705.122803 6.8727 20:17 1.#QNAN0 0.936281756 696.180298 6.3979 20:19 1.#QNAN0 1.#QNAN0000 1.#QNAN0 1.#QNB 20:21 743.562073 0.915504024 680.734070 5.7833 20:23 1.#QNAN0 0.895352776 665.750366 5.3357 20:26 1.#QNAN0 0.875236661 650.792786 4.9890 20:27 1.#QNAN0 0.855144924 635.853333 4.6994 20:29 1.#QNAN0 0.834669113 620.628296 4.4497 20:31 1.#QNAN0 0.814543968 605.664001 4.2305 20:32 1.#QNAN0 0.794218783 590.550964 4.0383 20:34 1.#QNAN0 0.774279888 575.725159 3.8711 20:36 1.#QNAN0 0.754081852 560.706665 3.7207 20:37 1.#QNAN0 0.734208544 545.929626 3.5889 20:39 1.#QNAN0 0.713978658 530.887451 3.4682 20:40 1.#QNAN0 0.694175368 516.162476 3.3600 20:42 1.#QNAN0 0.673691431 500.931396 3.2594 20:43 1.#QNAN0 0.653932384 486.239319 3.1691 20:45 1.#QNAN0 0.633505413 471.050598 3.0829 20:46 1.#QNAN0 0.613483326 456.162933 3.0040 20:48 1.#QNAN0 0.593296371 441.152679 2.9304 20:49 1.#QNAN0 0.573349966 426.321289 2.8585 20:50 1.#QNAN0 0.553105429 411.268219 2.7903 20:51 1.#QNAN0 0.532257240 395.766296 2.7219 20:53 1.#QNAN0 0.512928359 381.394073 2.6597 20:54 1.#QNAN0 0.492935575 366.528198 2.5865 20:56 1.#QNAN0 0.472978253 351.688690 2.4161 20:57 1.#QNAN0 0.451025818 335.365692 2.2230 20:59 1.#QNAN0 0.431063406 320.522400 2.1193 21:01 1.#QNAN0 0.412164896 306.470184 2.0475 21:02 1.#QNAN0 0.391729224 291.274994 1.9837 21:03 1.#QNAN0 0.371755690 276.423431 1.9269 21:05 1.#QNAN0 0.351439123 261.316803 1.8720 21:06 1.#QNAN0 0.331474639 246.471970 1.8201 21:07 1.#QNAN0 0.311195421 231.393112 1.7678 21:08 1.#QNAN0 0.291221702 216.541412 1.7180 21:10 1.#QNAN0 0.271155104 201.620651 1.6662 21:11 1.#QNAN0 0.250897659 186.557983 1.6175 21:12 1.#QNAN0 0.231182569 171.898590 1.5684 21:14 1.#QNAN0 0.210882399 156.804153 1.5194 21:15 1.#QNAN0 0.190971823 141.999405 1.4696 21:16 1.#QNAN0 0.170798751 126.999474 1.4195 21:18 1.#QNAN0 0.150752900 112.094139 1.3689 21:19 1.#QNAN0 0.130611339 97.117638 1.3170 21:21 1.#QNAN0 0.110578242 82.221786 1.2628 21:23 1.#QNAN0 0.090488270 67.283646 1.2052 21:25 1.#QNAN0 0.070412263 52.355888 1.1424 21:27 1.#QNAN0 0.050342695 37.432919 1.0701 21:29 1.#QNAN0 0.030357853 22.572948 0.9782 21:31 1.#QNAN0 0.009997201 7.433539 0.8062 21:36 1.#QNAN0 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Isotherm Linear Plot 000-598 rep of 597 cook sample 6cs-3 - Adsorption Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 5.3147e-006 0.012784 3.02841e-006 0.0265899 2.55327e-006 0.04042 2.98443e-006 0.0541125 4.22767e-006 0.0674654 6.42296e-006 0.0815294 9.48645e-006 0.0954553 1.3704e-005 0.109191 1.90916e-005 0.122729 2.58074e-005 0.135977 3.39114e-005 0.148912 4.44261e-005 0.162853 5.64949e-005 0.17636 6.99135e-005 0.189387 8.2363e-005 0.199625 9.53821e-005 0.209809 0.000114564 0.222943 0.000130364 0.232918 0.00014792 0.24275 0.0001666 0.252499 0.000186319 0.262173 0.000207299 0.271751 0.000229665 0.281212 0.000253758 0.290533 0.000278572 0.299803 0.000304873 0.308957 0.000340502 0.320852 0.000378057 0.332497 0.000416886 0.34377 0.000456972 0.354593 0.000497242 0.36497 0.000538435 0.374834 0.000580865 0.384489 0.000623933 0.393682 0.000666468 0.402364 0.000709517 0.410753 0.000752883 0.418817 0.000796511 0.426411 0.00083901 0.433703 0.000881528 0.440633 0.000923552 0.447263 0.000965114 0.45351 0.00100564 0.459354 0.00104551 0.464877 0.00108456 0.470196 0.00112273 0.475147 0.00115946 0.479778 0.00119589 0.484214 0.00123058 0.488439 0.00126456 0.492348 0.00129686 0.495976 0.0013284 0.499398 0.00135896 0.502626 0.0013878 0.505549 0.00144677 0.512103 0.00150711 0.518547 0.00156855 0.52492 0.00163079 0.531178 0.00169463 0.537337 0.00175923 0.543438 0.0018254 0.54942 0.00189242 0.555321 0.00196079 0.561149 0.00203011 0.566898 0.00210072 0.572544 0.00217218 0.578109 0.00224436 0.583592 0.00233653 0.590496 0.00242245 0.596726 0.00249904 0.601866 0.00257767 0.606865 0.00265651 0.611808 0.00273642 0.616702 0.00281793 0.621458 0.00289953 0.626161 0.00298292 0.630769 0.00306735 0.635318 0.00315195 0.639815 0.00323798 0.644192 0.00332591 0.64847 0.00341313 0.652739 0.00350262 0.656858 0.00359318 0.660919 0.00368361 0.664893 0.00377649 0.668755 0.00386976 0.672583 0.00396347 0.676371 0.00405755 0.680082 0.00415417 0.683617 0.0042514 0.687109 0.00437898 0.691999 0.00447861 0.695214 0.00457897 0.698425 0.00467977 0.70155 0.00478198 0.704625 0.00488563 0.707615 0.00498958 0.710495 0.00509318 0.713391 0.00519967 0.716149 0.00530587 0.718901 0.00541346 0.721529 0.0055218 0.724113 0.00563032 0.726645 0.00573969 0.729041 0.00584953 0.73151 0.00596165 0.733812 0.00607315 0.736133 0.00618531 0.738356 0.00629711 0.740524 0.00641055 0.742685 0.00652446 0.744708 0.00663973 0.746699 0.00675577 0.748643 0.00739213 0.762059 0.00803561 0.774625 0.00869517 0.786458 0.00934489 0.798339 0.0100119 0.808926 0.0302883 0.97113 0.0563128 1.08328 0.0699193 1.13162 0.0903387 1.19346 0.110436 1.25049 0.130477 1.3037 0.1506 1.35568 0.170562 1.40617 0.190735 1.45659 0.211216 1.50689 0.23077 1.55604 0.250865 1.60468 0.270867 1.65538 0.291848 1.70722 0.311206 1.75629 0.33157 1.80894 0.351421 1.86063 0.371393 1.91203 0.391601 1.96346 0.412448 2.01746 0.431641 2.06862 0.452495 2.122 0.472617 2.17538 0.493031 2.22941 0.512859 2.2831 0.533016 2.33865 0.553035 2.39413 0.573176 2.45137 0.593277 2.51099 0.613377 2.5727 0.633379 2.63766 0.653992 2.70778 0.673588 2.77919 0.693634 2.85729 0.713821 2.94187 0.733941 3.03524 0.753899 3.13521 0.774092 3.24643 0.794063 3.37042 0.814272 3.51202 0.834305 3.67545 0.854488 3.86439 0.874258 4.08771 0.8944 4.37896 0.914658 4.74258 0.934178 5.21534 0.954009 5.92056 0.973145 7.05016 0.990594 9.28557 000-598 rep of 597 cook sample 6cs-3 - Desorption Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 0.990594 9.28557 0.980691 8.88381 0.967695 7.91524 0.948313 6.87274 0.936282 6.3979 0.915504 5.78331 0.895353 5.33573 0.875237 4.98899 0.855145 4.69941 0.834669 4.44972 0.814544 4.23053 0.794219 4.03828 0.77428 3.87111 0.754082 3.72072 0.734209 3.5889 0.713979 3.46823 0.694175 3.36001 0.673691 3.2594 0.653932 3.16913 0.633505 3.0829 0.613483 3.00404 0.593296 2.93045 0.57335 2.85851 0.553105 2.7903 0.532257 2.72194 0.512928 2.65967 0.492936 2.58654 0.472978 2.41606 0.451026 2.22305 0.431063 2.11934 0.412165 2.0475 0.391729 1.98373 0.371756 1.92688 0.351439 1.87201 0.331475 1.82009 0.311195 1.76782 0.291222 1.71796 0.271155 1.66623 0.250898 1.61747 0.231183 1.56836 0.210882 1.51937 0.190972 1.46955 0.170799 1.41951 0.150753 1.36887 0.130611 1.317 0.110578 1.26281 0.0904883 1.20519 0.0704123 1.14243 0.0503427 1.07011 0.0303579 0.97822 0.0099972 0.806151 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Isotherm Log Plot 000-598 rep of 597 cook sample 6cs-3 - Adsorption Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 5.3147e-006 0.012784 3.02841e-006 0.0265899 2.55327e-006 0.04042 2.98443e-006 0.0541125 4.22767e-006 0.0674654 6.42296e-006 0.0815294 9.48645e-006 0.0954553 1.3704e-005 0.109191 1.90916e-005 0.122729 2.58074e-005 0.135977 3.39114e-005 0.148912 4.44261e-005 0.162853 5.64949e-005 0.17636 6.99135e-005 0.189387 8.2363e-005 0.199625 9.53821e-005 0.209809 0.000114564 0.222943 0.000130364 0.232918 0.00014792 0.24275 0.0001666 0.252499 0.000186319 0.262173 0.000207299 0.271751 0.000229665 0.281212 0.000253758 0.290533 0.000278572 0.299803 0.000304873 0.308957 0.000340502 0.320852 0.000378057 0.332497 0.000416886 0.34377 0.000456972 0.354593 0.000497242 0.36497 0.000538435 0.374834 0.000580865 0.384489 0.000623933 0.393682 0.000666468 0.402364 0.000709517 0.410753 0.000752883 0.418817 0.000796511 0.426411 0.00083901 0.433703 0.000881528 0.440633 0.000923552 0.447263 0.000965114 0.45351 0.00100564 0.459354 0.00104551 0.464877 0.00108456 0.470196 0.00112273 0.475147 0.00115946 0.479778 0.00119589 0.484214 0.00123058 0.488439 0.00126456 0.492348 0.00129686 0.495976 0.0013284 0.499398 0.00135896 0.502626 0.0013878 0.505549 0.00144677 0.512103 0.00150711 0.518547 0.00156855 0.52492 0.00163079 0.531178 0.00169463 0.537337 0.00175923 0.543438 0.0018254 0.54942 0.00189242 0.555321 0.00196079 0.561149 0.00203011 0.566898 0.00210072 0.572544 0.00217218 0.578109 0.00224436 0.583592 0.00233653 0.590496 0.00242245 0.596726 0.00249904 0.601866 0.00257767 0.606865 0.00265651 0.611808 0.00273642 0.616702 0.00281793 0.621458 0.00289953 0.626161 0.00298292 0.630769 0.00306735 0.635318 0.00315195 0.639815 0.00323798 0.644192 0.00332591 0.64847 0.00341313 0.652739 0.00350262 0.656858 0.00359318 0.660919 0.00368361 0.664893 0.00377649 0.668755 0.00386976 0.672583 0.00396347 0.676371 0.00405755 0.680082 0.00415417 0.683617 0.0042514 0.687109 0.00437898 0.691999 0.00447861 0.695214 0.00457897 0.698425 0.00467977 0.70155 0.00478198 0.704625 0.00488563 0.707615 0.00498958 0.710495 0.00509318 0.713391 0.00519967 0.716149 0.00530587 0.718901 0.00541346 0.721529 0.0055218 0.724113 0.00563032 0.726645 0.00573969 0.729041 0.00584953 0.73151 0.00596165 0.733812 0.00607315 0.736133 0.00618531 0.738356 0.00629711 0.740524 0.00641055 0.742685 0.00652446 0.744708 0.00663973 0.746699 0.00675577 0.748643 0.00739213 0.762059 0.00803561 0.774625 0.00869517 0.786458 0.00934489 0.798339 0.0100119 0.808926 0.0302883 0.97113 0.0563128 1.08328 0.0699193 1.13162 0.0903387 1.19346 0.110436 1.25049 0.130477 1.3037 0.1506 1.35568 0.170562 1.40617 0.190735 1.45659 0.211216 1.50689 0.23077 1.55604 0.250865 1.60468 0.270867 1.65538 0.291848 1.70722 0.311206 1.75629 0.33157 1.80894 0.351421 1.86063 0.371393 1.91203 0.391601 1.96346 0.412448 2.01746 0.431641 2.06862 0.452495 2.122 0.472617 2.17538 0.493031 2.22941 0.512859 2.2831 0.533016 2.33865 0.553035 2.39413 0.573176 2.45137 0.593277 2.51099 0.613377 2.5727 0.633379 2.63766 0.653992 2.70778 0.673588 2.77919 0.693634 2.85729 0.713821 2.94187 0.733941 3.03524 0.753899 3.13521 0.774092 3.24643 0.794063 3.37042 0.814272 3.51202 0.834305 3.67545 0.854488 3.86439 0.874258 4.08771 0.8944 4.37896 0.914658 4.74258 0.934178 5.21534 0.954009 5.92056 0.973145 7.05016 0.990594 9.28557 000-598 rep of 597 cook sample 6cs-3 - Desorption Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 0.990594 9.28557 0.980691 8.88381 0.967695 7.91524 0.948313 6.87274 0.936282 6.3979 0.915504 5.78331 0.895353 5.33573 0.875237 4.98899 0.855145 4.69941 0.834669 4.44972 0.814544 4.23053 0.794219 4.03828 0.77428 3.87111 0.754082 3.72072 0.734209 3.5889 0.713979 3.46823 0.694175 3.36001 0.673691 3.2594 0.653932 3.16913 0.633505 3.0829 0.613483 3.00404 0.593296 2.93045 0.57335 2.85851 0.553105 2.7903 0.532257 2.72194 0.512928 2.65967 0.492936 2.58654 0.472978 2.41606 0.451026 2.22305 0.431063 2.11934 0.412165 2.0475 0.391729 1.98373 0.371756 1.92688 0.351439 1.87201 0.331475 1.82009 0.311195 1.76782 0.291222 1.71796 0.271155 1.66623 0.250898 1.61747 0.231183 1.56836 0.210882 1.51937 0.190972 1.46955 0.170799 1.41951 0.150753 1.36887 0.130611 1.317 0.110578 1.26281 0.0904883 1.20519 0.0704123 1.14243 0.0503427 1.07011 0.0303579 0.97822 0.0099972 0.806151 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BET Surface Area Report BET Surface Area: 5.4581 ± 0.0137 m²/g Slope: 0.785658 ± 0.001972 g/cm³ STP Y-Intercept: 0.011915 ± 0.000368 g/cm³ STP C: 66.940021 Qm: 1.2538 cm³/g STP Correlation Coefficient: 0.9999653 Molecular Cross-Sectional Area: 0.1620 nm² Quantity Relative Adsorbed Pressure (cm³/g 1/[Q(Po/P (P/Po) STP) - 1)] --- 0.056312836 1.0833 0.055085 0.069919266 1.1316 0.066432 0.090338715 1.1935 0.083212 0.110435862 1.2505 0.099278 0.130476959 1.3037 0.115100 0.150600396 1.3557 0.130785 0.170562061 1.4062 0.146238 0.190734927 1.4566 0.161809 0.211215533 1.5069 0.177700 0.230770163 1.5560 0.192799 0.250865264 1.6047 0.208686 0.270866772 1.6554 0.224414 0.291848140 1.7072 0.241402 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BET Surface Area Plot 000-598 rep of 597 cook sample 6cs-3 Relative Pressure (P/Po) 1/[Q(Po/P - 1)] 0.0563128 0.0550855 0.0699193 0.066432 0.0903387 0.0832124 0.110436 0.0992776 0.130477 0.1151 0.1506 0.130785 0.170562 0.146238 0.190735 0.161809 0.211216 0.1777 0.23077 0.192799 0.250865 0.208686 0.270867 0.224414 0.291848 0.241402 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm t-Plot Report Micropore Volume: -0.000386 cm³/g Micropore Area: * External Surface Area: 6.2451 m²/g Slope: 0.403743 ± 0.007656 cm³/g·Å STP Y-Intercept: -0.249315 ± 0.023052 cm³/g STP Correlation Coefficient: 0.999461 Surface Area Correction Factor: 1.000 Density Conversion Factor: 0.0015468 Total Surface Area (BET): 5.4581 m²/g Thickness Range: 2.6000 Å to 3.5000 Å Thickness Equation: Harkins and Jura t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 Quantity Relative Statistical Adsorbed Pressure Thickness (cm³/g (P/Po) (Å) STP) --- 0.000005315 1.6234 0.0128 0.000003028 1.5873 0.0266 0.000002553 1.5768 0.0404 0.000002984 1.5864 0.0541 0.000004228 1.6084 0.0675 0.000006423 1.6361 0.0815 0.000009486 1.6633 0.0955 0.000013704 1.6902 0.1092 0.000019092 1.7156 0.1227 0.000025807 1.7397 0.1360 0.000033911 1.7625 0.1489 0.000044426 1.7859 0.1629 0.000056495 1.8075 0.1764 0.000069913 1.8274 0.1894 0.000082363 1.8431 0.1996 0.000095382 1.8575 0.2098 0.000114564 1.8760 0.2229 0.000130364 1.8894 0.2329 0.000147920 1.9028 0.2428 0.000166600 1.9156 0.2525 0.000186319 1.9280 0.2622 0.000207299 1.9399 0.2718 0.000229665 1.9517 0.2812 0.000253758 1.9633 0.2905 0.000278572 1.9743 0.2998 0.000304873 1.9852 0.3090 0.000340502 1.9987 0.3209 0.000378057 2.0118 0.3325 0.000416886 2.0243 0.3438 0.000456972 2.0362 0.3546 0.000497242 2.0474 0.3650 0.000538435 2.0581 0.3748 0.000580865 2.0684 0.3845 0.000623933 2.0783 0.3937 0.000666468 2.0876 0.4024 0.000709517 2.0965 0.4108 0.000752883 2.1050 0.4188 0.000796511 2.1132 0.4264 0.000839010 2.1209 0.4337 0.000881528 2.1282 0.4406 0.000923552 2.1352 0.4473 0.000965114 2.1419 0.4535 0.001005638 2.1482 0.4594 0.001045507 2.1542 0.4649 0.001084558 2.1599 0.4702 0.001122731 2.1654 0.4751 0.001159458 2.1704 0.4798 0.001195886 2.1754 0.4842 0.001230583 2.1800 0.4884 0.001264556 2.1844 0.4923 0.001296858 2.1884 0.4960 0.001328401 2.1924 0.4994 0.001358960 2.1961 0.5026 0.001387801 2.1996 0.5055 0.001446770 2.2065 0.5121 0.001507105 2.2133 0.5185 0.001568550 2.2201 0.5249 0.001630794 2.2267 0.5312 0.001694629 2.2333 0.5373 0.001759233 2.2398 0.5434 0.001825401 2.2463 0.5494 0.001892422 2.2526 0.5553 0.001960790 2.2590 0.5611 0.002030108 2.2652 0.5669 0.002100724 2.2714 0.5725 0.002172180 2.2775 0.5781 0.002244357 2.2835 0.5836 0.002336533 2.2910 0.5905 0.002422451 2.2978 0.5967 0.002499043 2.3037 0.6019 0.002577668 2.3096 0.6069 0.002656515 2.3153 0.6118 0.002736416 2.3211 0.6167 0.002817928 2.3268 0.6215 0.002899530 2.3324 0.6262 0.002982918 2.3380 0.6308 0.003067348 2.3435 0.6353 0.003151951 2.3490 0.6398 0.003237984 2.3544 0.6442 0.003325906 2.3599 0.6485 0.003413134 2.3652 0.6527 0.003502623 2.3705 0.6569 0.003593184 2.3758 0.6609 0.003683608 2.3810 0.6649 0.003776485 2.3862 0.6688 0.003869760 2.3914 0.6726 0.003963470 2.3965 0.6764 0.004057552 2.4015 0.6801 0.004154169 2.4066 0.6836 0.004251400 2.4116 0.6871 0.004378980 2.4181 0.6920 0.004478609 2.4230 0.6952 0.004578968 2.4279 0.6984 0.004679767 2.4328 0.7016 0.004781978 2.4376 0.7046 0.004885634 2.4425 0.7076 0.004989578 2.4473 0.7105 0.005093182 2.4519 0.7134 0.005199667 2.4567 0.7161 0.005305868 2.4614 0.7189 0.005413460 2.4660 0.7215 0.005521804 2.4706 0.7241 0.005630319 2.4752 0.7266 0.005739690 2.4797 0.7290 0.005849534 2.4842 0.7315 0.005961651 2.4888 0.7338 0.006073149 2.4932 0.7361 0.006185309 2.4976 0.7384 0.006297113 2.5020 0.7405 0.006410552 2.5063 0.7427 0.006524464 2.5106 0.7447 0.006639729 2.5150 0.7467 0.006755766 2.5192 0.7486 0.007392127 2.5419 0.7621 0.008035608 2.5634 0.7746 0.008695166 2.5843 0.7865 0.009344890 2.6038 0.7983 0.010011879 2.6229 0.8089 0.030288303 3.0017 0.9711 0.056312836 3.3016 1.0833 0.069919266 3.4296 1.1316 0.090338715 3.6023 1.1935 0.110435862 3.7575 1.2505 0.130476959 3.9028 1.3037 0.150600396 4.0423 1.3557 0.170562061 4.1763 1.4062 0.190734927 4.3087 1.4566 0.211215533 4.4412 1.5069 0.230770163 4.5667 1.5560 0.250865264 4.6954 1.6047 0.270866772 4.8237 1.6554 0.291848140 4.9592 1.7072 0.311206479 5.0855 1.7563 0.331570386 5.2200 1.8089 0.351421369 5.3533 1.8606 0.371393210 5.4900 1.9120 0.391600795 5.6314 1.9635 0.412448116 5.7809 2.0175 0.431640617 5.9223 2.0686 0.452494948 6.0805 2.1220 0.472617287 6.2383 2.1754 0.493030953 6.4040 2.2294 0.512859068 6.5711 2.2831 0.533015848 6.7477 2.3387 0.553034680 6.9307 2.3941 0.573176273 7.1233 2.4514 0.593276587 7.3249 2.5110 * The micropore area is not reported because either the micropore volume is negative or the calculated external surface area is larger than the total surface area. ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm t-Plot Harkins and Jura 000-598 rep of 597 cook sample 6cs-3 Thickness (Å) Quantity Adsorbed (cm³/g STP) 2.60384 0.798339 2.62294 0.808926 3.00166 0.97113 3.30164 1.08328 3.42961 1.13162 Not Fitted Points Thickness (Å) Quantity Adsorbed (cm³/g STP) 1.62339 0.012784 1.58728 0.0265899 1.57679 0.04042 1.58637 0.0541125 1.6084 0.0674654 1.63611 0.0815294 1.66329 0.0954553 1.6902 0.109191 1.71561 0.122729 1.73973 0.135977 1.76249 0.148912 1.7859 0.162853 1.80753 0.17636 1.82739 0.189387 1.84311 0.199625 1.85754 0.209809 1.87604 0.222943 1.88943 0.232918 1.90279 0.24275 1.91564 0.252499 1.92796 0.262173 1.93994 0.271751 1.95166 0.281212 1.96327 0.290533 1.97432 0.299803 1.98519 0.308957 1.99875 0.320852 2.01184 0.332497 2.02432 0.34377 2.03624 0.354593 2.0474 0.36497 2.05809 0.374834 2.06843 0.384489 2.07832 0.393682 2.08757 0.402364 2.09647 0.410753 2.105 0.418817 2.11321 0.426411 2.12086 0.433703 2.12822 0.440633 2.13522 0.447263 2.1419 0.45351 2.14821 0.459354 2.15421 0.464877 2.15993 0.470196 2.16536 0.475147 2.17045 0.479778 2.17537 0.484214 2.17996 0.488439 2.18435 0.492348 2.18844 0.495976 2.19236 0.499398 2.19609 0.502626 2.19955 0.505549 2.20646 0.512103 2.2133 0.518547 2.22006 0.52492 2.2267 0.531178 2.23331 0.537337 2.2398 0.543438 2.24627 0.54942 2.25264 0.555321 2.25896 0.561149 2.26521 0.566898 2.2714 0.572544 2.27751 0.578109 2.28353 0.583592 2.291 0.590496 2.29777 0.596726 2.30366 0.601866 2.30956 0.606865 2.31534 0.611808 2.32107 0.616702 2.32679 0.621458 2.33239 0.626161 2.33799 0.630769 2.34355 0.635318 2.349 0.639815 2.35444 0.644192 2.35989 0.64847 2.36519 0.652739 2.37052 0.656858 2.37581 0.660919 2.38101 0.664893 2.38624 0.668755 2.3914 0.672583 2.3965 0.676371 2.40152 0.680082 2.4066 0.683617 2.41162 0.687109 2.41808 0.691999 2.42304 0.695214 2.42794 0.698425 2.4328 0.70155 2.43764 0.704625 2.44247 0.707615 2.44725 0.710495 2.45194 0.713391 2.45669 0.716149 2.46135 0.718901 2.46601 0.721529 2.47064 0.724113 2.47521 0.726645 2.47975 0.729041 2.48425 0.73151 2.48878 0.733812 2.49322 0.736133 2.49764 0.738356 2.50198 0.740524 2.50633 0.742685 2.51065 0.744708 2.51496 0.746699 2.51925 0.748643 2.54189 0.762059 2.56344 0.774625 2.58432 0.786458 3.60225 1.19346 3.75748 1.25049 3.90281 1.3037 4.04229 1.35568 4.17628 1.40617 4.30871 1.45659 4.44121 1.50689 4.56673 1.55604 4.6954 1.60468 4.82373 1.65538 4.95921 1.70722 5.08545 1.75629 5.22 1.80894 5.35331 1.86063 5.49 1.91203 5.63135 1.96346 5.78087 2.01746 5.92228 2.06862 6.08053 2.122 6.23828 2.17538 6.404 2.22941 6.57105 2.2831 6.7477 2.33865 6.93071 2.39413 7.1233 2.45137 7.32492 2.51099 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Adsorption Pore Distribution Report Faas Correction Halsey t = 3.54 [ -5 / ln(P/Po) ] ^ 0.333 Width Range: 17.000 Å to 3000.000 Å Adsorbate Property Factor: 9.53000 Å Density Conversion Factor: 0.0015468 Fraction of Pores Open at Both Ends: 0.00 Incremental Cumulative Cumulative Average Pore Pore Incremental Pore Width Volume Volume Pore Area Area Pore Width Range (Å) (Å) (cm³/g) (cm³/g) (m²/g) (m²/g) ------ 2068.6 - 735.1 879.3 0.003750 0.003750 0.171 0.171 735.1 - 433.1 509.0 0.001897 0.005647 0.149 0.320 433.1 - 304.3 346.1 0.001194 0.006840 0.138 0.458 304.3 - 235.5 260.9 0.000805 0.007645 0.123 0.581 235.5 - 190.7 208.2 0.000622 0.008267 0.119 0.700 190.7 - 160.2 172.7 0.000502 0.008768 0.116 0.817 160.2 - 138.4 147.6 0.000383 0.009151 0.104 0.920 138.4 - 121.4 128.7 0.000324 0.009475 0.101 1.021 121.4 - 108.0 113.9 0.000281 0.009756 0.099 1.120 108.0 - 97.1 102.0 0.000243 0.009999 0.095 1.215 97.1 - 88.2 92.2 0.000212 0.010211 0.092 1.307 88.2 - 80.7 84.1 0.000190 0.010401 0.090 1.397 80.7 - 74.3 77.2 0.000170 0.010572 0.088 1.486 74.3 - 68.7 71.2 0.000159 0.010731 0.090 1.575 68.7 - 63.8 66.0 0.000143 0.010874 0.087 1.662 63.8 - 59.5 61.5 0.000132 0.011006 0.086 1.748 59.5 - 55.7 57.5 0.000120 0.011126 0.084 1.832 55.7 - 52.2 53.9 0.000117 0.011244 0.087 1.919 52.2 - 49.1 50.6 0.000109 0.011353 0.086 2.005 49.1 - 46.3 47.6 0.000103 0.011456 0.087 2.091 46.3 - 43.7 44.9 0.000100 0.011556 0.089 2.180 43.7 - 41.4 42.5 0.000095 0.011651 0.090 2.270 41.4 - 39.2 40.2 0.000093 0.011744 0.092 2.363 39.2 - 37.2 38.1 0.000094 0.011838 0.099 2.461 37.2 - 35.3 36.2 0.000091 0.011929 0.101 2.562 35.3 - 33.5 34.4 0.000092 0.012021 0.107 2.669 33.5 - 31.9 32.7 0.000092 0.012113 0.112 2.781 31.9 - 30.3 31.0 0.000090 0.012203 0.117 2.898 30.3 - 28.9 29.5 0.000089 0.012292 0.121 3.019 28.9 - 27.5 28.1 0.000093 0.012385 0.132 3.151 27.5 - 26.2 26.8 0.000088 0.012473 0.131 3.281 26.2 - 24.9 25.5 0.000088 0.012561 0.138 3.420 24.9 - 23.7 24.3 0.000089 0.012650 0.146 3.566 23.7 - 22.6 23.1 0.000089 0.012739 0.155 3.721 22.6 - 21.5 22.0 0.000081 0.012820 0.147 3.868 21.5 - 20.4 21.0 0.000083 0.012903 0.158 4.026 20.4 - 19.4 19.9 0.000081 0.012984 0.163 4.189 19.4 - 18.4 18.9 0.000072 0.013057 0.153 4.343 18.4 - 17.5 17.9 0.000074 0.013130 0.164 4.507 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Adsorption dV/dw Pore Volume Halsey : Faas Correction 000-598 rep of 597 cook sample 6cs-3 Pore Width (Å) Pore Volume (cm³/g·Å) 879.254 2.81198e-006 508.986 6.28038e-006 346.066 9.27057e-006 260.878 1.16922e-005 208.177 1.38723e-005 172.667 1.64712e-005 147.61 1.75419e-005 128.682 1.90172e-005 113.868 2.10989e-005 101.972 2.23014e-005 92.2402 2.38649e-005 84.0947 2.5038e-005 77.1862 2.66279e-005 71.2423 2.8554e-005 66.039 2.92112e-005 61.4751 3.07144e-005 57.4854 3.2122e-005 53.8534 3.32465e-005 50.5645 3.52568e-005 47.6195 3.64934e-005 44.9303 3.87076e-005 42.465 4.02844e-005 40.2019 4.27411e-005 38.1082 4.64641e-005 36.1756 4.92295e-005 34.36 5.14969e-005 32.6532 5.57367e-005 31.0322 5.65247e-005 29.548 6.42981e-005 28.1364 6.50643e-005 26.7714 6.67457e-005 25.5007 7.13158e-005 24.2987 7.58092e-005 23.1353 7.75581e-005 22.0352 7.70264e-005 20.9523 7.50339e-005 19.8952 7.97435e-005 18.8887 7.28013e-005 17.9196 7.78069e-005 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Adsorption dV/dw Pore Volume Halsey : Faas Correction 000-598 rep of 597 cook sample 6cs-3 Pore Width (Å) Pore Volume (cm³/g·Å) 879.254 2.81198e-006 508.986 6.28038e-006 346.066 9.27057e-006 260.878 1.16922e-005 208.177 1.38723e-005 172.667 1.64712e-005 147.61 1.75419e-005 128.682 1.90172e-005 113.868 2.10989e-005 101.972 2.23014e-005 92.2402 2.38649e-005 84.0947 2.5038e-005 77.1862 2.66279e-005 71.2423 2.8554e-005 66.039 2.92112e-005 61.4751 3.07144e-005 57.4854 3.2122e-005 53.8534 3.32465e-005 50.5645 3.52568e-005 47.6195 3.64934e-005 44.9303 3.87076e-005 42.465 4.02844e-005 40.2019 4.27411e-005 38.1082 4.64641e-005 36.1756 4.92295e-005 34.36 5.14969e-005 32.6532 5.57367e-005 31.0322 5.65247e-005 29.548 6.42981e-005 28.1364 6.50643e-005 26.7714 6.67457e-005 25.5007 7.13158e-005 24.2987 7.58092e-005 23.1353 7.75581e-005 22.0352 7.70264e-005 20.9523 7.50339e-005 19.8952 7.97435e-005 18.8887 7.28013e-005 17.9196 7.78069e-005 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Adsorption dV/dlog(w) Pore Volume Halsey : Faas Correction 000-598 rep of 597 cook sample 6cs-3 Pore Width (Å) dV/dlog(w) Pore Volume (cm³/g·Å) 879.254 0.0083453 508.986 0.00825478 346.066 0.00778943 260.878 0.00722678 208.177 0.00678105 172.667 0.00663705 147.61 0.00601956 128.682 0.00567855 113.868 0.00556573 101.972 0.00526312 92.2402 0.00508997 84.0947 0.00486607 77.1862 0.00474732 71.2423 0.00469717 66.039 0.00445306 61.4751 0.0043574 57.4854 0.00426012 53.8534 0.0041308 50.5645 0.00411198 47.6195 0.00400791 44.9303 0.00401061 42.465 0.00394465 40.2019 0.00396181 38.1082 0.00408243 36.1756 0.00410568 34.36 0.00407934 32.6532 0.00419558 31.0322 0.0040439 29.548 0.0043791 28.1364 0.00422029 26.7714 0.00411899 25.5007 0.00419201 24.2987 0.00424606 23.1353 0.0041363 22.0352 0.00391226 20.9523 0.00362456 19.8952 0.00365743 18.8887 0.00317032 17.9196 0.00321447 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Adsorption Cumulative Pore Area Halsey : Faas Correction 000-598 rep of 597 cook sample 6cs-3 Pore Width (Å) Pore Area (m²/g) 735.096 0.170593 433.067 0.319662 304.306 0.457635 235.492 0.581002 190.668 0.70048 160.213 0.816686 138.379 0.920474 121.355 1.02111 108.031 1.11986 97.148 1.21507 88.2496 1.30716 80.6719 1.3974 74.2714 1.48573 68.6855 1.57528 63.7855 1.66198 59.4899 1.74783 55.7455 1.83152 52.213 1.91875 49.1217 2.00497 46.2995 2.09148 43.7222 2.18029 41.3521 2.27023 39.1798 2.36261 37.1542 2.4614 35.3008 2.56229 33.52 2.66904 31.8767 2.78125 30.2777 2.89775 28.8895 3.01858 27.4623 3.1506 26.1505 3.28141 24.9159 3.41953 23.743 3.5659 22.5898 3.72053 21.5352 3.868 20.4322 4.026 19.4142 4.1892 18.4194 4.34257 17.4733 4.5069 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Adsorption dA/dw Pore Area Halsey : Faas Correction 000-598 rep of 597 cook sample 6cs-3 Pore Width (Å) Pore Area (m²/g·Å) 879.254 0.000127926 508.986 0.00049356 346.066 0.00107154 260.878 0.00179275 208.177 0.00266548 172.667 0.0038157 147.61 0.00475358 128.682 0.00591135 113.868 0.00741171 101.972 0.0087481 92.2402 0.010349 84.0947 0.0119094 77.1862 0.0137993 71.2423 0.016032 66.039 0.0176933 61.4751 0.0199849 57.4854 0.0223515 53.8534 0.0246941 50.5645 0.0278905 47.6195 0.0306542 44.9303 0.0344602 42.465 0.037946 40.2019 0.0425265 38.1082 0.0487707 36.1756 0.0544339 34.36 0.0599498 32.6532 0.0682772 31.0322 0.0728594 29.548 0.0870423 28.1364 0.0924984 26.7714 0.0997269 25.5007 0.111865 24.2987 0.124795 23.1353 0.134095 22.0352 0.139824 20.9523 0.143247 19.8952 0.160327 18.8887 0.154169 17.9196 0.17368 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Adsorption dA/dlog(w) Pore Area Halsey : Faas Correction 000-598 rep of 597 cook sample 6cs-3 Pore Width (Å) dA/dlog(w) Pore Area (m²/g·Å) 879.254 0.379654 508.986 0.648724 346.066 0.900341 260.878 1.10807 208.177 1.30294 172.667 1.53754 147.61 1.63121 128.682 1.76514 113.868 1.95516 101.972 2.06454 92.2402 2.20727 84.0947 2.31456 77.1862 2.46019 71.2423 2.63729 66.039 2.69723 61.4751 2.83523 57.4854 2.96432 53.8534 3.06818 50.5645 3.25286 47.6195 3.36661 44.9303 3.57052 42.465 3.71567 40.2019 3.94192 38.1082 4.28509 36.1756 4.53972 34.36 4.74894 32.6532 5.13956 31.0322 5.21251 29.548 5.92812 28.1364 5.99976 26.7714 6.15432 25.5007 6.57552 24.2987 6.98977 23.1353 7.1515 22.0352 7.10184 20.9523 6.91962 19.8952 7.3534 18.8887 6.71368 17.9196 7.1753 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Desorption Pore Distribution Report Faas Correction Halsey t = 3.54 [ -5 / ln(P/Po) ] ^ 0.333 Width Range: 17.000 Å to 3000.000 Å Adsorbate Property Factor: 9.53000 Å Density Conversion Factor: 0.0015468 Fraction of Pores Open at Both Ends: 0.00 Incremental Cumulative Cumulative Average Pore Pore Incremental Pore Width Volume Volume Pore Area Area Pore Width Range (Å) (Å) (cm³/g) (cm³/g) (m²/g) (m²/g) ------ 2070.3 - 1018.9 1219.5 0.000666 0.000666 0.022 0.022 1018.9 - 614.6 720.3 0.001643 0.002309 0.091 0.113 614.6 - 387.8 450.8 0.001804 0.004113 0.160 0.273 387.8 - 315.9 344.3 0.000828 0.004941 0.096 0.369 315.9 - 239.5 266.9 0.001086 0.006026 0.163 0.532 239.5 - 194.1 211.8 0.000798 0.006825 0.151 0.683 194.1 - 163.2 175.8 0.000622 0.007447 0.142 0.824 163.2 - 140.7 150.2 0.000524 0.007971 0.140 0.964 140.7 - 123.3 130.8 0.000455 0.008426 0.139 1.103 123.3 - 109.9 115.8 0.000404 0.008830 0.140 1.243 109.9 - 98.9 103.8 0.000355 0.009185 0.137 1.380 98.9 - 90.0 94.0 0.000310 0.009495 0.132 1.511 90.0 - 82.4 85.9 0.000279 0.009774 0.130 1.641 82.4 - 76.1 79.0 0.000244 0.010018 0.123 1.765 76.1 - 70.4 73.0 0.000223 0.010240 0.122 1.887 70.4 - 65.6 67.8 0.000199 0.010440 0.118 2.004 65.6 - 61.2 63.2 0.000184 0.010623 0.116 2.120 61.2 - 57.4 59.2 0.000165 0.010788 0.111 2.232 57.4 - 53.9 55.6 0.000156 0.010944 0.113 2.344 53.9 - 50.8 52.3 0.000142 0.011087 0.109 2.453 50.8 - 48.0 49.3 0.000131 0.011218 0.106 2.560 48.0 - 45.4 46.6 0.000131 0.011349 0.112 2.672 45.4 - 43.1 44.2 0.000122 0.011471 0.111 2.783 43.1 - 40.8 41.9 0.000124 0.011595 0.118 2.901 40.8 - 38.9 39.8 0.000114 0.011709 0.114 3.015 38.9 - 37.0 37.9 0.000145 0.011854 0.153 3.168 37.0 - 35.3 36.1 0.000431 0.012284 0.477 3.645 35.3 - 33.5 34.3 0.000491 0.012775 0.573 4.218 33.5 - 31.9 32.7 0.000230 0.013006 0.282 4.500 31.9 - 30.6 31.2 0.000138 0.013144 0.177 4.678 30.6 - 29.2 29.8 0.000107 0.013251 0.144 4.821 29.2 - 27.9 28.5 0.000089 0.013340 0.124 4.946 27.9 - 26.6 27.2 0.000081 0.013421 0.120 5.065 26.6 - 25.4 26.0 0.000074 0.013495 0.114 5.179 25.4 - 24.3 24.8 0.000074 0.013569 0.119 5.298 24.3 - 23.2 23.7 0.000067 0.013636 0.113 5.411 23.2 - 22.2 22.7 0.000073 0.013709 0.128 5.540 22.2 - 21.1 21.6 0.000060 0.013769 0.111 5.651 21.1 - 20.1 20.6 0.000063 0.013832 0.122 5.773 20.1 - 19.2 19.6 0.000057 0.013888 0.115 5.888 19.2 - 18.2 18.7 0.000059 0.013947 0.126 6.014 18.2 - 17.3 17.7 0.000054 0.014001 0.121 6.135 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Desorption Cumulative Pore Volume Halsey : Faas Correction BJH Desorption Cumulative Pore Volume Pore Width (Å) Pore Volume (cm³/g) 1018.92 0.000665852 614.636 0.00230886 387.784 0.00411312 315.907 0.00494084 239.529 0.00602645 194.098 0.0068247 163.175 0.00744691 140.715 0.00797126 123.331 0.00842637 109.898 0.00883022 98.9288 0.00918541 90.0309 0.00949524 82.44 0.00977401 76.0558 0.0100178 70.4312 0.0102403 65.6137 0.0104397 61.2154 0.0106234 57.4394 0.010788 53.9382 0.0109444 50.8421 0.0110867 48.0069 0.011218 45.4483 0.0113488 43.0648 0.0114713 40.8055 0.0115949 38.8656 0.0117087 36.9969 0.0118535 35.2552 0.0122841 33.4655 0.0127752 31.9395 0.0130057 30.5743 0.013144 29.1756 0.0132513 27.8782 0.0133398 26.6217 0.0134213 25.4422 0.0134952 24.294 0.0135691 23.2064 0.0136363 22.1518 0.0137089 21.1206 0.0137689 20.1443 0.0138318 19.162 0.0138883 18.2159 0.0139472 17.2688 0.0140007 BJH Desorption dV/dw Pore Volume Pore Width (Å) Pore Volume (cm³/g·Å) 1219.47 6.33292e-007 720.268 4.06398e-006 450.78 7.95348e-006 344.254 1.15158e-005 266.892 1.42136e-005 211.826 1.75706e-005 175.802 2.01209e-005 150.173 2.33465e-005 130.792 2.61785e-005 115.777 3.00651e-005 103.787 3.23809e-005 94.0217 3.482e-005 85.8684 3.67246e-005 78.9641 3.81869e-005 73.0043 3.95608e-005 67.8328 4.13946e-005 63.2444 4.17556e-005 59.1928 4.36004e-005 55.5652 4.46553e-005 52.2871 4.5967e-005 49.3326 4.63271e-005 46.6482 5.11072e-005 44.1836 5.13882e-005 41.8658 5.47359e-005 39.7816 5.86574e-005 37.8786 7.74738e-005 36.0779 0.0002472 34.3067 0.000274428 32.6614 0.000151036 31.2224 0.000101286 29.837 7.67099e-005 28.4927 6.82749e-005 27.2163 6.47939e-005 26.0009 6.27173e-005 24.8372 6.43749e-005 23.7211 6.17272e-005 22.6504 6.88872e-005 21.6075 5.81717e-005 20.6054 6.44114e-005 19.6244 5.75427e-005 18.6609 6.22665e-005 17.7127 5.64978e-005 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Desorption dV/dw Pore Volume Halsey : Faas Correction 000-598 rep of 597 cook sample 6cs-3 Pore Width (Å) Pore Volume (cm³/g·Å) 1219.47 6.33292e-007 720.268 4.06398e-006 450.78 7.95348e-006 344.254 1.15158e-005 266.892 1.42136e-005 211.826 1.75706e-005 175.802 2.01209e-005 150.173 2.33465e-005 130.792 2.61785e-005 115.777 3.00651e-005 103.787 3.23809e-005 94.0217 3.482e-005 85.8684 3.67246e-005 78.9641 3.81869e-005 73.0043 3.95608e-005 67.8328 4.13946e-005 63.2444 4.17556e-005 59.1928 4.36004e-005 55.5652 4.46553e-005 52.2871 4.5967e-005 49.3326 4.63271e-005 46.6482 5.11072e-005 44.1836 5.13882e-005 41.8658 5.47359e-005 39.7816 5.86574e-005 37.8786 7.74738e-005 36.0779 0.0002472 34.3067 0.000274428 32.6614 0.000151036 31.2224 0.000101286 29.837 7.67099e-005 28.4927 6.82749e-005 27.2163 6.47939e-005 26.0009 6.27173e-005 24.8372 6.43749e-005 23.7211 6.17272e-005 22.6504 6.88872e-005 21.6075 5.81717e-005 20.6054 6.44114e-005 19.6244 5.75427e-005 18.6609 6.22665e-005 17.7127 5.64978e-005 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Desorption dV/dlog(w) Pore Volume Halsey : Faas Correction 000-598 rep of 597 cook sample 6cs-3 Pore Width (Å) dV/dlog(w) Pore Volume (cm³/g·Å) 1219.47 0.00216256 720.268 0.00748446 450.78 0.00902004 344.254 0.00929706 266.892 0.00903162 211.826 0.00873962 175.802 0.00825555 150.173 0.00815329 130.792 0.00794661 115.777 0.00806397 103.787 0.00777788 94.0217 0.00756942 85.8684 0.00728748 78.9641 0.00696439 73.0043 0.00666863 67.8328 0.00648083 63.2444 0.0060946 59.1928 0.00595408 55.5652 0.00572419 52.2871 0.00554352 49.3326 0.00527077 46.6482 0.00549747 44.1836 0.00523542 41.8658 0.00528398 39.7816 0.00537927 37.8786 0.00676519 36.0779 0.0205589 34.3067 0.0217072 32.6614 0.011371 31.2224 0.00728853 29.837 0.00527588 28.4927 0.0044839 27.2163 0.00406479 26.0009 0.00375868 24.8372 0.00368551 23.7211 0.00337507 22.6504 0.00359668 21.6075 0.00289752 20.6054 0.00305949 19.6244 0.00260345 18.6609 0.00267894 17.7127 0.00230757 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Desorption Cumulative Pore Area Halsey : Faas Correction 000-598 rep of 597 cook sample 6cs-3 Pore Width (Å) Pore Area (m²/g) 1018.92 0.0218407 614.636 0.113085 387.784 0.273186 315.907 0.369361 239.529 0.532066 194.098 0.682803 163.175 0.824372 140.715 0.964038 123.331 1.10322 109.898 1.24275 98.9288 1.37964 90.0309 1.51145 82.44 1.64132 76.0558 1.76481 70.4312 1.88673 65.6137 2.00432 61.2154 2.12048 57.4394 2.23173 53.9382 2.34428 50.8421 2.45316 48.0069 2.55966 45.4483 2.67178 43.0648 2.78267 40.8055 2.90082 38.8656 3.01524 36.9969 3.16812 35.2552 3.64547 33.4655 4.21814 31.9395 4.5004 30.5743 4.67755 29.1756 4.82139 27.8782 4.94574 26.6217 5.0654 25.4422 5.1792 24.294 5.29825 23.2064 5.41145 22.1518 5.53974 21.1206 5.65079 20.1443 5.77286 19.162 5.88807 18.2159 6.01436 17.2688 6.1352 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Desorption dA/dw Pore Area Halsey : Faas Correction 000-598 rep of 597 cook sample 6cs-3 Pore Width (Å) Pore Area (m²/g·Å) 1219.47 2.07727e-005 720.268 0.000225693 450.78 0.000705752 344.254 0.00133806 266.892 0.00213025 211.826 0.00331793 175.802 0.00457808 150.173 0.00621859 130.792 0.00800614 115.777 0.0103872 103.787 0.0124798 94.0217 0.0148136 85.8684 0.0171074 78.9641 0.0193439 73.0043 0.0216759 67.8328 0.0244098 63.2444 0.0264091 59.1928 0.0294633 55.5652 0.0321463 52.2871 0.0351651 49.3326 0.0375631 46.6482 0.0438235 44.1836 0.0465224 41.8658 0.0522965 39.7816 0.0589794 37.8786 0.0818128 36.0779 0.274074 34.3067 0.31997 32.6614 0.184971 31.2224 0.12976 29.837 0.102839 28.4927 0.095849 27.2163 0.095228 26.0009 0.096485 24.8372 0.103675 23.7211 0.104088 22.6504 0.121653 21.6075 0.107688 20.6054 0.125038 19.6244 0.117288 18.6609 0.13347 17.7127 0.127587 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Desorption dA/dlog(w) Pore Area Halsey : Faas Correction 000-598 rep of 597 cook sample 6cs-3 Pore Width (Å) dA/dlog(w) Pore Area (m²/g·Å) 1219.47 0.0709345 720.268 0.415649 450.78 0.800394 344.254 1.08025 266.892 1.3536 211.826 1.65034 175.802 1.87837 150.173 2.17171 130.792 2.4303 115.777 2.78603 103.787 2.99764 94.0217 3.22029 85.8684 3.39472 78.9641 3.52787 73.0043 3.65383 67.8328 3.82165 63.2444 3.85464 59.1928 4.02351 55.5652 4.1207 52.2871 4.24083 49.3326 4.27366 46.6482 4.71398 44.1836 4.73969 41.8658 5.04849 39.7816 5.4088 37.8786 7.14408 36.0779 22.794 34.3067 25.3095 32.6614 13.9258 31.2224 9.33755 29.837 7.07293 28.4927 6.29482 27.2163 5.97406 26.0009 5.7824 24.8372 5.93547 23.7211 5.69125 22.6504 6.35163 21.6075 5.36393 20.6054 5.93919 19.6244 5.30654 18.6609 5.74236 17.7127 5.21111 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Horvath-Kawazoe Report Slit Pore Geometry (Original H-K) Maximum Pore Volume: 0.001251 cm³/g at Relative Pressure: 0.010011879 Median Pore Width: 7.335 Å Relative Pressure Range: 5.315e-06 to 1.001e-02 Diameter of Adsorptive Molecule: 3.000 Å Diameter of Adsorptive at Zero Interaction Energy: 2.574 Å Diameter of Sample Atom: 3.040 Å Diameter of Sample Atom at Zero Interaction Energy: 2.609 Å Interaction Parameter: 3.49e-43 erg·cm^4 Density Conversion Factor: 0.0015468 Quantity Cumulative Differential Absolute Relative Adsorbed Pore Pore Pore Pressure Pressure (cm³/g Width Volume Volume (mmHg) (P/Po) STP) (Å) (cm³/g) (cm³/g·Å) ------ 0.00395 0.000005315 0.01278 5.202 0.0000 0.0000 0.00225 0.000003028 0.02659 5.049 0.0000 -0.0001 0.00190 0.000002553 0.04042 5.005 0.0001 -0.0005 0.00222 0.000002984 0.05411 5.045 0.0001 0.0005 0.00314 0.000004228 0.06747 5.138 0.0001 0.0002 0.00477 0.000006423 0.08153 5.256 0.0001 0.0002 0.00705 0.000009486 0.09546 5.372 0.0001 0.0002 0.01018 0.000013704 0.10919 5.488 0.0002 0.0002 0.01418 0.000019092 0.12273 5.598 0.0002 0.0002 0.01917 0.000025807 0.13598 5.704 0.0002 0.0002 0.02519 0.000033911 0.14891 5.804 0.0002 0.0002 0.03300 0.000044426 0.16285 5.908 0.0003 0.0002 0.04196 0.000056495 0.17636 6.004 0.0003 0.0002 0.05193 0.000069913 0.18939 6.094 0.0003 0.0002 0.06118 0.000082363 0.19963 6.165 0.0003 0.0002 0.07085 0.000095382 0.20981 6.231 0.0003 0.0002 0.08510 0.000114564 0.22294 6.316 0.0003 0.0002 0.09684 0.000130364 0.23292 6.377 0.0004 0.0003 0.10988 0.000147920 0.24275 6.439 0.0004 0.0002 0.12376 0.000166600 0.25250 6.499 0.0004 0.0003 0.13841 0.000186319 0.26217 6.556 0.0004 0.0003 0.15399 0.000207299 0.27175 6.612 0.0004 0.0003 0.17061 0.000229665 0.28121 6.667 0.0004 0.0003 0.18851 0.000253758 0.29053 6.722 0.0004 0.0003 0.20694 0.000278572 0.29980 6.774 0.0005 0.0003 0.22648 0.000304873 0.30896 6.827 0.0005 0.0003 0.25295 0.000340502 0.32085 6.891 0.0005 0.0003 0.28085 0.000378057 0.33250 6.954 0.0005 0.0003 0.30970 0.000416886 0.34377 7.014 0.0005 0.0003 0.33948 0.000456972 0.35459 7.071 0.0005 0.0003 0.36940 0.000497242 0.36497 7.126 0.0006 0.0003 0.40001 0.000538435 0.37483 7.178 0.0006 0.0003 0.43153 0.000580865 0.38449 7.229 0.0006 0.0003 0.46353 0.000623933 0.39368 7.277 0.0006 0.0003 0.49514 0.000666468 0.40236 7.324 0.0006 0.0003 0.52712 0.000709517 0.41075 7.367 0.0006 0.0003 0.55934 0.000752883 0.41882 7.410 0.0006 0.0003 0.59176 0.000796511 0.42641 7.451 0.0007 0.0003 0.62334 0.000839010 0.43370 7.489 0.0007 0.0003 0.65493 0.000881528 0.44063 7.526 0.0007 0.0003 0.68616 0.000923552 0.44726 7.561 0.0007 0.0003 0.71704 0.000965114 0.45351 7.595 0.0007 0.0003 0.74716 0.001005638 0.45935 7.627 0.0007 0.0003 0.77678 0.001045507 0.46488 7.657 0.0007 0.0003 0.80580 0.001084558 0.47020 7.686 0.0007 0.0003 0.83417 0.001122731 0.47515 7.714 0.0007 0.0003 0.86146 0.001159458 0.47978 7.739 0.0007 0.0003 0.88853 0.001195886 0.48421 7.765 0.0007 0.0003 0.91432 0.001230583 0.48844 7.788 0.0008 0.0003 0.93957 0.001264556 0.49235 7.811 0.0008 0.0003 0.96358 0.001296858 0.49598 7.831 0.0008 0.0003 0.98702 0.001328401 0.49940 7.852 0.0008 0.0003 1.00973 0.001358960 0.50263 7.872 0.0008 0.0003 1.03117 0.001387801 0.50555 7.889 0.0008 0.0003 1.07499 0.001446770 0.51210 7.924 0.0008 0.0003 1.11983 0.001507105 0.51855 7.960 0.0008 0.0003 1.16549 0.001568550 0.52492 7.995 0.0008 0.0003 1.21175 0.001630794 0.53118 8.029 0.0008 0.0003 1.25919 0.001694629 0.53734 8.064 0.0008 0.0003 1.30721 0.001759233 0.54344 8.097 0.0008 0.0003 1.35638 0.001825401 0.54942 8.131 0.0008 0.0003 1.40619 0.001892422 0.55532 8.164 0.0009 0.0003 1.45701 0.001960790 0.56115 8.198 0.0009 0.0003 1.50853 0.002030108 0.56690 8.232 0.0009 0.0003 1.56101 0.002100724 0.57254 8.264 0.0009 0.0003 1.61412 0.002172180 0.57811 8.297 0.0009 0.0003 1.66776 0.002244357 0.58359 8.329 0.0009 0.0003 1.73627 0.002336533 0.59050 8.369 0.0009 0.0003 1.80013 0.002422451 0.59673 8.404 0.0009 0.0003 1.85706 0.002499043 0.60187 8.436 0.0009 0.0002 1.91550 0.002577668 0.60686 8.467 0.0009 0.0002 1.97411 0.002656515 0.61181 8.498 0.0009 0.0002 2.03350 0.002736416 0.61670 8.529 0.0010 0.0002 2.09409 0.002817928 0.62146 8.560 0.0010 0.0002 2.15474 0.002899530 0.62616 8.591 0.0010 0.0002 2.21673 0.002982918 0.63077 8.621 0.0010 0.0002 2.27949 0.003067348 0.63532 8.651 0.0010 0.0002 2.34238 0.003151951 0.63982 8.680 0.0010 0.0002 2.40633 0.003237984 0.64419 8.711 0.0010 0.0002 2.47169 0.003325906 0.64847 8.740 0.0010 0.0002 2.53653 0.003413134 0.65274 8.768 0.0010 0.0002 2.60305 0.003502623 0.65686 8.798 0.0010 0.0002 2.67038 0.003593184 0.66092 8.828 0.0010 0.0002 2.73760 0.003683608 0.66489 8.856 0.0010 0.0002 2.80665 0.003776485 0.66875 8.885 0.0010 0.0002 2.87599 0.003869760 0.67258 8.913 0.0010 0.0002 2.94565 0.003963470 0.67637 8.942 0.0010 0.0002 3.01559 0.004057552 0.68008 8.969 0.0011 0.0002 3.08742 0.004154169 0.68362 8.997 0.0011 0.0002 3.15971 0.004251400 0.68711 9.026 0.0011 0.0002 3.25455 0.004378980 0.69200 9.061 0.0011 0.0002 3.32862 0.004478609 0.69521 9.089 0.0011 0.0002 3.40324 0.004578968 0.69842 9.117 0.0011 0.0002 3.47818 0.004679767 0.70155 9.143 0.0011 0.0002 3.55418 0.004781978 0.70462 9.171 0.0011 0.0002 3.63125 0.004885634 0.70761 9.198 0.0011 0.0002 3.70853 0.004989578 0.71050 9.225 0.0011 0.0002 3.78557 0.005093182 0.71339 9.250 0.0011 0.0002 3.86474 0.005199667 0.71615 9.278 0.0011 0.0002 3.94371 0.005305868 0.71890 9.305 0.0011 0.0002 4.02371 0.005413460 0.72153 9.330 0.0011 0.0002 4.10427 0.005521804 0.72411 9.357 0.0011 0.0001 4.18496 0.005630319 0.72664 9.382 0.0011 0.0002 4.26628 0.005739690 0.72904 9.409 0.0011 0.0001 4.34797 0.005849534 0.73151 9.434 0.0011 0.0002 4.43134 0.005961651 0.73381 9.462 0.0011 0.0001 4.51425 0.006073149 0.73613 9.487 0.0011 0.0001 4.59765 0.006185309 0.73836 9.512 0.0011 0.0001 4.68079 0.006297113 0.74052 9.537 0.0011 0.0001 4.76515 0.006410552 0.74269 9.562 0.0011 0.0001 4.84986 0.006524464 0.74471 9.587 0.0012 0.0001 4.93557 0.006639729 0.74670 9.612 0.0012 0.0001 5.02187 0.006755766 0.74864 9.636 0.0012 0.0001 5.49502 0.007392127 0.76206 9.768 0.0012 0.0002 5.97344 0.008035608 0.77463 9.895 0.0012 0.0002 6.46383 0.008695166 0.78646 10.018 0.0012 0.0001 6.94694 0.009344890 0.79834 10.134 0.0012 0.0002 7.44281 0.010011879 0.80893 10.249 0.0013 0.0001 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Horvath-Kawazoe Cumulative Pore Volume Plot Slit Pore Geometry (Original H-K) 000-598 rep of 597 cook sample 6cs-3 Pore Width (Å) Pore Volume (cm³/g) 5.20188 1.97743e-005 5.04941 4.11292e-005 5.00492 6.25217e-005 5.04514 8.37013e-005 5.1382 0.000104356 5.25597 0.00012611 5.37211 0.00014765 5.4882 0.000168896 5.5983 0.000189837 5.70377 0.000210329 5.80432 0.000230337 5.9078 0.0002519 6.00444 0.000272793 6.09398 0.000292944 6.16522 0.00030878 6.23058 0.000324533 6.31587 0.000344848 6.37668 0.000360277 6.43883 0.000375486 6.49855 0.000390566 6.55578 0.00040553 6.6124 0.000420344 6.66741 0.000434979 6.72178 0.000449397 6.77449 0.000463735 6.82651 0.000477894 6.89064 0.000496294 6.95419 0.000514307 7.01416 0.000531743 7.07147 0.000548484 7.12607 0.000564535 7.17792 0.000579794 7.22901 0.000594728 7.27727 0.000608947 7.3237 0.000622376 7.36723 0.000635353 7.4099 0.000647827 7.45065 0.000659572 7.48947 0.000670852 7.52632 0.000681571 7.56119 0.000691827 7.59511 0.000701489 7.62702 0.000710529 7.65688 0.000719071 7.68577 0.0007273 7.71365 0.000734957 7.73946 0.000742121 7.76533 0.000748982 7.78802 0.000755518 7.81076 0.000761564 7.83138 0.000767175 7.85203 0.000772469 7.87164 0.000777461 7.8891 0.000781983 7.92407 0.000792121 7.96025 0.000802088 7.99545 0.000811946 8.02856 0.000821626 8.06398 0.000831153 8.09729 0.00084059 8.1307 0.000849843 8.16422 0.000858971 8.19783 0.000867985 8.23154 0.000876877 8.26423 0.000885611 8.29701 0.000894219 8.32876 0.000902701 8.36855 0.000913379 8.40391 0.000923015 8.43596 0.000930966 8.46694 0.000938699 8.49801 0.000946344 8.52916 0.000953914 8.5604 0.000961271 8.59056 0.000968546 8.6208 0.000975674 8.65112 0.000982711 8.68035 0.000989667 8.71082 0.000996436 8.74019 0.00100305 8.76847 0.00100966 8.79799 0.00101603 8.82758 0.00102231 8.85607 0.00102846 8.88462 0.00103443 8.91324 0.00104035 8.94192 0.00104621 8.96948 0.00105195 8.9971 0.00105742 9.02599 0.00106282 9.06098 0.00107038 9.08882 0.00107536 9.11671 0.00108032 9.14346 0.00108516 9.17148 0.00108991 9.19834 0.00109454 9.22527 0.00109899 9.2498 0.00110347 9.27807 0.00110774 9.30517 0.001112 9.32986 0.00111606 9.35707 0.00112006 9.38186 0.00112397 9.40919 0.00112768 9.43409 0.0011315 9.46153 0.00113506 9.48654 0.00113865 9.51159 0.00114209 9.53669 0.00114544 9.56185 0.00114879 9.58705 0.00115191 9.6123 0.00115499 9.63634 0.001158 9.76818 0.00117875 9.89498 0.00119819 10.0179 0.00121649 10.1341 0.00123487 10.2487 0.00125125 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Horvath-Kawazoe Differential Pore Volume Plot Slit Pore Geometry (Original H-K) 000-598 rep of 597 cook sample 6cs-3 Pore Width (Å) dV/dw (cm³/g·Å) 5.20188 3.80138e-006 5.04941 -0.000140055 5.00492 -0.00048082 5.04514 0.000526532 5.1382 0.000221946 5.25597 0.000184724 5.37211 0.000185466 5.4882 0.000183018 5.5983 0.000190197 5.70377 0.000194287 5.80432 0.000198974 5.9078 0.000208389 6.00444 0.000216202 6.09398 0.000225051 6.16522 0.000222274 6.23058 0.000241025 6.31587 0.000238192 6.37668 0.000253714 6.43883 0.000244704 6.49855 0.000252531 6.55578 0.000261462 6.6124 0.000261663 6.66741 0.000265995 6.72178 0.000265224 6.77449 0.000272 6.82651 0.000272208 6.89064 0.000286906 6.95419 0.000283415 7.01416 0.000290771 7.07147 0.000292124 7.12607 0.000293963 7.17792 0.000294304 7.22901 0.000292309 7.27727 0.000294608 7.3237 0.000289247 7.36723 0.000298131 7.4099 0.000292333 7.45065 0.0002882 7.48947 0.000290592 7.52632 0.000290874 7.56119 0.00029411 7.59511 0.000284835 7.62702 0.000283315 7.65688 0.000286023 7.68577 0.0002849 7.71365 0.000274584 7.73946 0.000277559 7.76533 0.000265233 7.78802 0.000288008 7.81076 0.000265919 7.83138 0.000272174 7.85203 0.000256275 7.87164 0.000254641 7.8891 0.000258981 7.92407 0.00028988 7.96025 0.00027548 7.99545 0.000280047 8.02856 0.00029238 8.06398 0.000268999 8.09729 0.00028329 8.1307 0.000276918 8.16422 0.000272376 8.19783 0.000268177 8.23154 0.000263771 8.26423 0.00026719 8.29701 0.000262567 8.32876 0.000267196 8.36855 0.000268363 8.40391 0.000272476 8.43596 0.000248114 8.46694 0.000249574 8.49801 0.000246083 8.52916 0.000243007 8.5604 0.000235497 8.59056 0.000241223 8.6208 0.000235698 8.65112 0.000232105 8.68035 0.000237996 8.71082 0.00022214 8.74019 0.00022525 8.76847 0.000233589 8.79799 0.00021582 8.82758 0.000212231 8.85607 0.000215813 8.88462 0.000209229 8.91324 0.000206884 8.94192 0.000204271 8.96948 0.000208312 8.9971 0.00019792 9.02599 0.000186962 9.06098 0.000216174 9.08882 0.000178669 9.11671 0.000178036 9.14346 0.000180788 9.17148 0.000169712 9.19834 0.000172152 9.22527 0.000165463 9.2498 0.000182587 9.27807 0.00015093 9.30517 0.00015708 9.32986 0.00016465 9.35707 0.000146842 9.38186 0.000157978 9.40919 0.000135634 9.43409 0.000153407 9.46153 0.000129723 9.48654 0.000143584 9.51159 0.000137275 9.53669 0.000133577 9.56185 0.00013291 9.58705 0.000124136 9.6123 0.000121964 9.63634 0.000125036 9.76818 0.000157416 9.89498 0.000153285 10.0179 0.000148947 10.1341 0.000158137 10.2487 0.000142883 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Porosity Distribution by Original Density Functional Theory Model: N2 @ 77K on Carbon, Slit Pores Method: Non-negative Regularization; No Smoothing Standard Deviation of Fit: 0.03257, cm³/g STP Volume in Pores < 5.00 Å : 0.00003 cm³/g Total Volume in Pores <= 1366.77 Å : 0.00870 cm³/g Area in Pores > 1366.77 Å : 1.692 m²/g Total Area in Pores >= 5.00 Å : 3.376 m²/g Pore Size Table Cumulative Incremental Cumulative Pore Width Volume Volume Area Incremental (Å) (cm³/g) (cm³/g) (m²/g) Area (m²/g) ----- 5.00 0.00000 0.00000 0.000 0.000 5.36 0.00000 0.00000 0.000 0.000 5.90 0.00000 0.00000 0.000 0.000 6.43 0.00000 0.00000 0.000 0.000 6.79 0.00000 0.00000 0.000 0.000 7.33 0.00000 0.00000 0.000 0.000 8.04 0.00000 0.00000 0.000 0.000 8.58 0.00000 0.00000 0.000 0.000 9.29 0.00000 0.00000 0.000 0.000 10.01 0.00000 0.00000 0.000 0.000 10.90 0.00000 0.00000 0.000 0.000 11.79 0.00000 0.00000 0.000 0.000 12.69 0.00000 0.00000 0.006 0.006 13.58 0.00025 0.00024 0.363 0.357 14.83 0.00034 0.00010 0.491 0.128 15.91 0.00034 0.00000 0.491 0.000 17.16 0.00034 0.00000 0.491 0.000 18.59 0.00034 0.00000 0.491 0.000 20.02 0.00034 0.00000 0.491 0.000 21.62 0.00034 0.00000 0.491 0.000 23.41 0.00034 0.00000 0.491 0.000 25.20 0.00034 0.00000 0.491 0.000 27.34 0.00045 0.00011 0.569 0.078 29.49 0.00055 0.00011 0.642 0.072 31.81 0.00067 0.00011 0.712 0.070 34.31 0.00077 0.00011 0.774 0.062 36.99 0.00084 0.00007 0.812 0.039 40.03 0.00092 0.00008 0.851 0.039 43.25 0.00101 0.00009 0.893 0.041 46.64 0.00111 0.00010 0.936 0.044 50.40 0.00122 0.00010 0.977 0.040 54.33 0.00132 0.00010 1.014 0.037 58.80 0.00141 0.00009 1.046 0.032 63.44 0.00151 0.00009 1.076 0.030 68.45 0.00161 0.00011 1.107 0.031 73.99 0.00171 0.00010 1.134 0.027 79.88 0.00182 0.00011 1.162 0.028 86.32 0.00198 0.00015 1.198 0.036 93.11 0.00214 0.00016 1.233 0.035 100.61 0.00228 0.00014 1.260 0.027 108.66 0.00241 0.00013 1.284 0.025 117.23 0.00255 0.00014 1.308 0.023 126.53 0.00269 0.00015 1.331 0.023 136.71 0.00286 0.00017 1.355 0.024 147.61 0.00305 0.00019 1.381 0.026 159.41 0.00324 0.00019 1.405 0.024 172.10 0.00343 0.00019 1.427 0.022 185.86 0.00361 0.00018 1.447 0.020 200.69 0.00381 0.00019 1.466 0.019 216.60 0.00401 0.00020 1.485 0.019 233.93 0.00421 0.00020 1.502 0.017 252.52 0.00444 0.00023 1.520 0.018 272.71 0.00469 0.00024 1.538 0.018 294.51 0.00486 0.00017 1.550 0.012 317.92 0.00501 0.00015 1.559 0.009 343.30 0.00515 0.00014 1.568 0.008 370.64 0.00527 0.00012 1.574 0.007 400.31 0.00544 0.00017 1.583 0.008 432.30 0.00562 0.00018 1.591 0.008 466.79 0.00586 0.00024 1.601 0.010 503.96 0.00624 0.00039 1.616 0.015 544.17 0.00666 0.00042 1.632 0.015 587.60 0.00695 0.00028 1.641 0.010 634.42 0.00720 0.00025 1.649 0.008 684.99 0.00750 0.00030 1.658 0.009 739.68 0.00771 0.00021 1.664 0.006 798.65 0.00789 0.00018 1.668 0.005 862.45 0.00810 0.00021 1.673 0.005 931.26 0.00827 0.00017 1.677 0.004 1005.60 0.00837 0.00011 1.679 0.002 1085.66 0.00846 0.00009 1.681 0.002 1172.33 0.00857 0.00011 1.682 0.002 1265.80 0.00863 0.00006 1.683 0.001 1366.77 0.00866 0.00003 1.684 0.000 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Porosity Distribution by Original Density Functional Theory Model: N2 @ 77K on Carbon, Slit Pores Method: Non-negative Regularization; No Smoothing Standard Deviation of Fit: 0.03257, cm³/g STP Isotherm Table Fitted Experimental Quantity Absolute Quantity Adsorbed Residual Relative Adsorbed (cm³/g (cm³/g Relative Pressure (cm³/g STP) STP) STP) Residual ----- 0.000008995 0.0937 0.0314 0.0624 0.665224 0.000015520 0.1141 0.0394 0.0747 0.654880 0.000026102 0.1365 0.0527 0.0838 0.613837 0.000042841 0.1609 0.0752 0.0858 0.532948 0.000068697 0.1883 0.1133 0.0750 0.398266 0.000107744 0.2184 0.1764 0.0420 0.192299 0.000165451 0.2519 0.2637 -0.0118 -0.046770 0.000249000 0.2887 0.3510 -0.0622 -0.215541 0.000367617 0.3293 0.4221 -0.0928 -0.281733 0.000532902 0.3735 0.4782 -0.1047 -0.280267 0.000759152 0.4199 0.5234 -0.1035 -0.246443 0.001063641 0.4674 0.5608 -0.0935 -0.199966 0.001466847 0.5143 0.5926 -0.0783 -0.152345 0.001992604 0.5638 0.6202 -0.0564 -0.100073 0.002668156 0.6125 0.6447 -0.0322 -0.052585 0.003524104 0.6578 0.6670 -0.0091 -0.013871 0.004594232 0.6989 0.6875 0.0114 0.016261 0.005915212 0.7329 0.7076 0.0252 0.034440 0.007526182 0.7647 0.7272 0.0376 0.049153 0.009468212 0.8005 0.8045 -0.0039 -0.004933 0.011783670 0.8306 0.8262 0.0044 0.005251 0.014515520 0.8605 0.8463 0.0142 0.016556 0.017706521 0.8907 0.8904 0.0003 0.000360 0.021398440 0.9199 0.9102 0.0097 0.010496 0.025631230 0.9471 0.9302 0.0169 0.017880 0.030442240 0.9718 0.9509 0.0210 0.021593 0.035865448 0.9969 0.9729 0.0240 0.024104 0.041930798 1.0244 0.9968 0.0276 0.026903 0.048663601 1.0534 1.0233 0.0301 0.028554 0.056084011 1.0824 1.0529 0.0295 0.027265 0.064206667 1.1123 1.0862 0.0260 0.023400 0.073040441 1.1414 1.1232 0.0181 0.015889 0.082588248 1.1706 1.1632 0.0074 0.006335 0.092847057 1.2007 1.2045 -0.0038 -0.003196 0.103808001 1.2322 1.2455 -0.0133 -0.010828 0.115456402 1.2640 1.2847 -0.0207 -0.016341 0.127772301 1.2966 1.3215 -0.0248 -0.019139 0.140730694 1.3303 1.3558 -0.0255 -0.019174 0.154301897 1.3651 1.3880 -0.0229 -0.016809 0.168452203 1.4009 1.4185 -0.0176 -0.012562 0.183144197 1.4377 1.4475 -0.0098 -0.006838 0.198337302 1.4753 1.4756 -0.0003 -0.000179 0.213988706 1.5138 1.5030 0.0108 0.007121 0.230053306 1.5543 1.5650 -0.0108 -0.006940 0.246484801 1.5939 1.5919 0.0020 0.001267 0.263235897 1.6361 1.6191 0.0170 0.010389 0.280259013 1.6786 1.6823 -0.0037 -0.002198 0.297506303 1.7214 1.7105 0.0109 0.006339 0.314930797 1.7659 1.7785 -0.0126 -0.007154 0.332486212 1.8113 1.8089 0.0025 0.001356 0.350127310 1.8573 1.8407 0.0165 0.008908 0.367810607 1.9028 1.9115 -0.0087 -0.004547 0.385494202 1.9479 1.9459 0.0020 0.001040 0.403138310 1.9932 1.9813 0.0119 0.005982 0.420704991 2.0394 2.0424 -0.0030 -0.001475 0.438158900 2.0854 2.0778 0.0076 0.003646 0.455466807 2.1299 2.1408 -0.0109 -0.005115 0.472598106 2.1753 2.1741 0.0012 0.000563 0.489524394 2.2201 2.2064 0.0137 0.006189 0.506219923 2.2649 2.2708 -0.0059 -0.002607 0.522661209 2.3101 2.3009 0.0092 0.003966 0.538827300 2.3547 2.3691 -0.0144 -0.006126 0.554699600 2.3988 2.3979 0.0009 0.000379 0.570261598 2.4430 2.4264 0.0166 0.006780 0.585499227 2.4877 2.4946 -0.0069 -0.002789 0.600400090 2.5326 2.5232 0.0093 0.003685 0.614954293 2.5777 2.5930 -0.0154 -0.005960 0.629153311 2.6237 2.6227 0.0010 0.000393 0.642990828 2.6699 2.6532 0.0167 0.006252 0.656461716 2.7165 2.7233 -0.0068 -0.002516 0.669562697 2.7641 2.7555 0.0086 0.003128 0.682291925 2.8125 2.8279 -0.0155 -0.005495 0.694648683 2.8614 2.8610 0.0004 0.000136 0.706633508 2.9109 2.8940 0.0168 0.005782 0.718248010 2.9616 2.9712 -0.0096 -0.003239 0.729494929 3.0139 3.0029 0.0110 0.003651 0.740377605 3.0667 3.0776 -0.0109 -0.003559 0.750900388 3.1197 3.1076 0.0121 0.003888 0.761068285 3.1733 3.1857 -0.0125 -0.003924 0.770887017 3.2280 3.2145 0.0135 0.004192 0.780362606 3.2837 3.3124 -0.0287 -0.008733 0.789501607 3.3409 3.3406 0.0003 0.000102 0.798311174 3.3985 3.3691 0.0295 0.008671 0.806798697 3.4574 3.4723 -0.0149 -0.004300 0.814971626 3.5173 3.5016 0.0157 0.004461 0.822837889 3.5790 3.5948 -0.0158 -0.004419 0.830405474 3.6421 3.6255 0.0165 0.004541 0.837682605 3.7050 3.7209 -0.0159 -0.004292 0.844677329 3.7693 3.7528 0.0165 0.004387 0.851397991 3.8340 3.8502 -0.0162 -0.004227 0.857852995 3.8986 3.8818 0.0168 0.004301 0.864050388 3.9661 3.9855 -0.0193 -0.004871 0.869998574 4.0356 4.0158 0.0198 0.004914 0.875705481 4.1060 4.1283 -0.0223 -0.005426 0.881179392 4.1799 4.1572 0.0227 0.005438 0.886428118 4.2564 4.2806 -0.0241 -0.005672 0.891459525 4.3332 4.3086 0.0245 0.005665 0.896281302 4.4089 4.4334 -0.0245 -0.005563 0.900900900 4.4866 4.4617 0.0249 0.005547 0.905325770 4.5657 4.5903 -0.0246 -0.005393 0.909563184 4.6447 4.6198 0.0249 0.005371 0.913620114 4.7225 4.7459 -0.0235 -0.004969 0.917503417 4.8007 4.7770 0.0238 0.004948 0.921219707 4.8841 4.9112 -0.0270 -0.005533 0.924775481 4.9703 4.9430 0.0273 0.005490 0.928177178 5.0570 5.0840 -0.0270 -0.005339 0.931430817 5.1424 5.1151 0.0272 0.005296 0.934542298 5.2251 5.2536 -0.0284 -0.005443 0.937517405 5.3119 5.2832 0.0286 0.005393 0.940361619 5.4046 5.4381 -0.0335 -0.006191 0.943080306 5.5004 5.4668 0.0336 0.006117 0.945678592 5.5969 5.6300 -0.0331 -0.005914 0.948161721 5.6921 5.6588 0.0333 0.005844 0.950534225 5.7847 5.7846 0.0001 0.000017 0.952800930 5.8735 5.8992 -0.0258 -0.004386 0.954966187 5.9565 5.9306 0.0259 0.004346 0.957034409 6.0281 6.0444 -0.0163 -0.002701 0.959009588 6.0941 6.0777 0.0164 0.002689 0.960896015 6.1606 6.1798 -0.0192 -0.003120 0.962697208 6.2325 6.2131 0.0193 0.003099 0.964416981 6.3130 6.3428 -0.0298 -0.004722 0.966058910 6.4045 6.3746 0.0299 0.004670 0.967626274 6.5085 6.5085 0.0001 0.000008 0.969122529 6.6260 6.6760 -0.0500 -0.007549 0.970550597 6.7570 6.7069 0.0501 0.007417 0.971913695 6.9016 6.9641 -0.0626 -0.009064 0.973214507 7.0591 6.9965 0.0627 0.008876 0.974455774 7.2181 7.2764 -0.0583 -0.008073 0.975640416 7.3699 7.3116 0.0584 0.007918 0.976770699 7.5147 7.5147 0.0000 0.000003 0.977849126 7.6529 7.7006 -0.0478 -0.006241 0.978878021 7.7847 7.7369 0.0478 0.006143 0.979859591 7.9104 7.9531 -0.0427 -0.005396 0.980795979 8.0304 7.9877 0.0427 0.005321 0.981689274 8.1448 8.1448 0.0000 0.000001 0.982541502 8.2540 8.2887 -0.0347 -0.004201 0.983354270 8.3581 8.3234 0.0347 0.004153 0.984129488 8.4575 8.4859 -0.0284 -0.003360 0.984869003 8.5522 8.5237 0.0284 0.003326 0.985574186 8.6425 8.6652 -0.0226 -0.002618 0.986246824 8.7287 8.7061 0.0226 0.002594 0.986888289 8.8109 8.8109 0.0000 0.000000 0.987500012 8.8893 8.9070 -0.0178 -0.001998 0.988083303 8.9640 8.9462 0.0178 0.001983 0.988639593 9.0352 9.0498 -0.0145 -0.001608 0.989170074 9.1032 9.0887 0.0145 0.001597 0.989675879 9.1680 9.1680 0.0000 0.000000 0.990158200 9.2298 9.2298 0.0000 0.000000 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Cumulative Surface Area vs. Pore Width Cumulative Surface Area Pore Width (Angstroms) Cumulative Surface Area (m²/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 0.0058729 13.5819 0.362693 14.8329 0.49105 15.9052 0.49105 17.1561 0.49105 18.5858 0.49105 20.0155 0.49105 21.6239 0.49105 23.411 0.49105 25.198 0.49105 27.3426 0.569367 29.4871 0.641508 31.8103 0.711797 34.3122 0.7738 36.9929 0.81244 40.0309 0.851386 43.2477 0.892826 46.6432 0.936449 50.3961 0.976777 54.3277 1.01418 58.7954 1.0464 63.4419 1.07634 68.4458 1.10715 73.9858 1.13448 79.8832 1.16211 86.3167 1.19776 93.1077 1.23265 100.613 1.25959 108.655 1.28441 117.233 1.30756 126.526 1.33097 136.713 1.35537 147.614 1.3809 159.409 1.40465 172.097 1.42707 185.858 1.44676 200.691 1.46606 216.596 1.4849 233.931 1.50199 252.517 1.52024 272.711 1.53816 294.513 1.54993 317.924 1.55939 343.301 1.56776 370.644 1.57427 400.309 1.58273 432.298 1.59098 466.789 1.60107 503.961 1.61643 544.171 1.63176 587.597 1.6414 634.419 1.64934 684.994 1.65821 739.679 1.66378 798.653 1.66836 862.452 1.67322 931.255 1.67683 1005.6 1.67897 1085.66 1.68061 1172.33 1.68242 1265.8 1.68341 1366.77 1.68388 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Incremental Surface Area vs. Pore Width Incremental Surface Area Pore Width (Angstroms) Incremental Surface Area (m²/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 0.0058729 13.5819 0.356821 14.8329 0.128357 15.9052 0 17.1561 0 18.5858 0 20.0155 0 21.6239 0 23.411 0 25.198 0 27.3426 0.0783162 29.4871 0.072141 31.8103 0.0702893 34.3122 0.0620033 36.9929 0.0386394 40.0309 0.0389463 43.2477 0.0414402 46.6432 0.0436233 50.3961 0.0403279 54.3277 0.0374067 58.7954 0.0322159 63.4419 0.029937 68.4458 0.0308139 73.9858 0.0273289 79.8832 0.0276349 86.3167 0.0356432 93.1077 0.0348923 100.613 0.0269423 108.655 0.0248135 117.233 0.0231531 126.526 0.0234104 136.713 0.0244024 147.614 0.0255315 159.409 0.0237477 172.097 0.0224139 185.858 0.0196996 200.691 0.0192908 216.596 0.0188466 233.931 0.0170858 252.517 0.0182568 272.711 0.0179199 294.513 0.0117627 317.924 0.00946043 343.301 0.00837705 370.644 0.00650418 400.309 0.00846381 432.298 0.00824697 466.789 0.0100891 503.961 0.0153566 544.171 0.0153393 587.597 0.00963537 634.419 0.00794228 684.994 0.00887012 739.679 0.00556621 798.653 0.00457799 862.452 0.00485888 931.255 0.00361013 1005.6 0.0021424 1085.66 0.00164276 1172.33 0.00180791 1265.8 0.000995332 1366.77 0.000462432 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Differential Surface Area vs. Pore Width Differential Surface Area Pore Width (Angstroms) Differential Surface Area (m²/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 0.191707 13.5819 10.5226 14.8329 3.74347 15.9052 0 17.1561 0 18.5858 0 20.0155 0 21.6239 0 23.411 0 25.198 0 27.3426 2.29448 29.4871 2.19512 31.8103 2.13589 34.3122 1.89178 36.9929 1.15433 40.0309 1.1481 43.2477 1.24834 46.6432 1.31329 50.3961 1.21776 54.3277 1.11751 58.7954 0.956603 63.4419 0.907144 68.4458 0.922958 73.9858 0.814467 79.8832 0.82558 86.3167 1.07149 93.1077 1.04843 100.613 0.803459 108.655 0.747447 117.233 0.700233 126.526 0.701355 136.713 0.72901 147.614 0.765522 159.409 0.71265 172.097 0.672399 185.858 0.59022 200.691 0.580442 216.596 0.566305 233.931 0.512781 252.517 0.54813 272.711 0.536404 294.513 0.353122 317.924 0.284224 343.301 0.251439 370.644 0.194968 400.309 0.253305 432.298 0.247192 466.789 0.302915 503.961 0.461062 544.171 0.46007 587.597 0.289172 634.419 0.238482 684.994 0.266102 739.679 0.166974 798.653 0.137288 862.452 0.14567 931.255 0.108267 1005.6 0.0643121 1085.66 0.0493123 1172.33 0.0542338 1265.8 0.0298701 1366.77 0.0138741 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Cumulative Pore Volume vs. Pore Width Cumulative Pore Volume Pore Width (Angstroms) Cumulative Pore Volume (cm³/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 3.72588e-006 13.5819 0.000246041 14.8329 0.000341237 15.9052 0.000341237 17.1561 0.000341237 18.5858 0.000341237 20.0155 0.000341237 21.6239 0.000341237 23.411 0.000341237 25.198 0.000341237 27.3426 0.000448305 29.4871 0.000554666 31.8103 0.000666463 34.3122 0.000772836 36.9929 0.000844305 40.0309 0.000922258 43.2477 0.00101187 46.6432 0.0011136 50.3961 0.00121522 54.3277 0.00131683 58.7954 0.00141154 63.4419 0.0015065 68.4458 0.00161196 73.9858 0.00171306 79.8832 0.00182343 86.3167 0.00197726 93.1077 0.0021397 100.613 0.00227524 108.655 0.00241005 117.233 0.00254576 126.526 0.00269386 136.713 0.00286067 147.614 0.00304911 159.409 0.00323839 172.097 0.00343126 185.858 0.00361433 200.691 0.0038079 216.596 0.004012 233.931 0.00421185 252.517 0.00444236 272.711 0.0046867 294.513 0.00485992 317.924 0.0050103 343.301 0.0051541 370.644 0.00527463 400.309 0.00544404 432.298 0.0056223 466.789 0.00585777 503.961 0.00624473 544.171 0.00666209 587.597 0.00694517 634.419 0.00719711 684.994 0.00750091 739.679 0.00770677 798.653 0.00788958 862.452 0.00809911 931.255 0.00826721 1005.6 0.00837493 1085.66 0.0084641 1172.33 0.00857007 1265.8 0.00863307 1366.77 0.00866467 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Incremental Pore Volume vs. Pore Width Incremental Pore Volume Pore Width (Angstroms) Incremental Pore Volume (cm³/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 3.72588e-006 13.5819 0.000242316 14.8329 9.51952e-005 15.9052 0 17.1561 0 18.5858 0 20.0155 0 21.6239 0 23.411 0 25.198 0 27.3426 0.000107068 29.4871 0.000106361 31.8103 0.000111796 34.3122 0.000106374 36.9929 7.14691e-005 40.0309 7.79528e-005 43.2477 8.96096e-005 46.6432 0.000101736 50.3961 0.000101619 54.3277 0.000101611 58.7954 9.47074e-005 63.4419 9.49632e-005 68.4458 0.000105454 73.9858 0.000101098 79.8832 0.000110378 86.3167 0.00015383 93.1077 0.000162437 100.613 0.000135538 108.655 0.000134806 117.233 0.000135716 126.526 0.000148102 136.713 0.000166806 147.614 0.00018844 159.409 0.00018928 172.097 0.000192869 185.858 0.000183066 200.691 0.000193574 216.596 0.000204105 233.931 0.000199844 252.517 0.000230507 272.711 0.000244348 294.513 0.000173214 317.924 0.000150385 343.301 0.000143792 370.644 0.000120537 400.309 0.000169407 432.298 0.000178258 466.789 0.000235474 503.961 0.000386956 544.171 0.000417361 587.597 0.000283086 634.419 0.000251937 684.994 0.000303799 739.679 0.00020586 798.653 0.000182811 862.452 0.000209527 931.255 0.000168098 1005.6 0.00010772 1085.66 8.91742e-005 1172.33 0.000105974 1265.8 6.29946e-005 1366.77 3.1602e-005 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Differential Pore Volume vs. Pore Width Differential Pore Volume Pore Width (Angstroms) Differential Pore Volume (cm³/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 0.000121622 13.5819 0.00714587 14.8329 0.00277632 15.9052 0 17.1561 0 18.5858 0 20.0155 0 21.6239 0 23.411 0 25.198 0 27.3426 0.00313685 29.4871 0.00323638 31.8103 0.00339717 34.3122 0.00324556 36.9929 0.0021351 40.0309 0.00229797 43.2477 0.00269939 46.6432 0.00306279 50.3961 0.00306851 54.3277 0.00303557 58.7954 0.0028122 63.4419 0.00287755 68.4458 0.00315863 73.9858 0.00301295 79.8832 0.0032975 86.3167 0.00462437 93.1077 0.00488083 100.613 0.00404194 108.655 0.00406071 117.233 0.00410454 126.526 0.004437 136.713 0.00498325 147.614 0.00565009 159.409 0.00568014 172.097 0.0057859 185.858 0.00548485 200.691 0.00582447 216.596 0.00613297 233.931 0.00599777 252.517 0.00692059 272.711 0.00731416 294.513 0.00519996 317.924 0.00451809 343.301 0.00431597 370.644 0.00361317 400.309 0.00507001 432.298 0.00534304 466.789 0.00706988 503.961 0.0116179 544.171 0.0125178 587.597 0.00849583 634.419 0.00756487 684.994 0.00911391 739.679 0.00617536 798.653 0.00548226 862.452 0.00628167 931.255 0.00504119 1005.6 0.00323361 1085.66 0.00267682 1172.33 0.00317901 1265.8 0.00189048 1366.77 0.000948135 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Standard Deviation of Fit: 0.03257, cm³/g STP Goodness of Fit Input Data Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 5.3147e-006 0.012784 3.02841e-006 0.0265899 2.55327e-006 0.04042 2.98443e-006 0.0541125 4.22767e-006 0.0674654 6.42296e-006 0.0815294 9.48645e-006 0.0954553 1.3704e-005 0.109191 1.90916e-005 0.122729 2.58074e-005 0.135977 3.39114e-005 0.148912 4.44261e-005 0.162853 5.64949e-005 0.17636 6.99135e-005 0.189387 8.2363e-005 0.199625 9.53821e-005 0.209809 0.000114564 0.222943 0.000130364 0.232918 0.00014792 0.24275 0.0001666 0.252499 0.000186319 0.262173 0.000207299 0.271751 0.000229665 0.281212 0.000253758 0.290533 0.000278572 0.299803 0.000304873 0.308957 0.000340502 0.320852 0.000378057 0.332497 0.000416886 0.34377 0.000456972 0.354593 0.000497242 0.36497 0.000538435 0.374834 0.000580865 0.384489 0.000623933 0.393682 0.000666468 0.402364 0.000709517 0.410753 0.000752883 0.418817 0.000796511 0.426411 0.00083901 0.433703 0.000881528 0.440633 0.000923552 0.447263 0.000965114 0.45351 0.00100564 0.459354 0.00104551 0.464877 0.00108456 0.470196 0.00112273 0.475147 0.00115946 0.479778 0.00119589 0.484214 0.00123058 0.488439 0.00126456 0.492348 0.00129686 0.495976 0.0013284 0.499398 0.00135896 0.502626 0.0013878 0.505549 0.00144677 0.512103 0.00150711 0.518547 0.00156855 0.52492 0.00163079 0.531178 0.00169463 0.537337 0.00175923 0.543438 0.0018254 0.54942 0.00189242 0.555321 0.00196079 0.561149 0.00203011 0.566898 0.00210072 0.572544 0.00217218 0.578109 0.00224436 0.583592 0.00233653 0.590496 0.00242245 0.596726 0.00249904 0.601866 0.00257767 0.606865 0.00265651 0.611808 0.00273642 0.616702 0.00281793 0.621458 0.00289953 0.626161 0.00298292 0.630769 0.00306735 0.635318 0.00315195 0.639815 0.00323798 0.644192 0.00332591 0.64847 0.00341313 0.652739 0.00350262 0.656858 0.00359318 0.660919 0.00368361 0.664893 0.00377649 0.668755 0.00386976 0.672583 0.00396347 0.676371 0.00405755 0.680082 0.00415417 0.683617 0.0042514 0.687109 0.00437898 0.691999 0.00447861 0.695214 0.00457897 0.698425 0.00467977 0.70155 0.00478198 0.704625 0.00488563 0.707615 0.00498958 0.710495 0.00509318 0.713391 0.00519967 0.716149 0.00530587 0.718901 0.00541346 0.721529 0.0055218 0.724113 0.00563032 0.726645 0.00573969 0.729041 0.00584953 0.73151 0.00596165 0.733812 0.00607315 0.736133 0.00618531 0.738356 0.00629711 0.740524 0.00641055 0.742685 0.00652446 0.744708 0.00663973 0.746699 0.00675577 0.748643 0.00739213 0.762059 0.00803561 0.774625 0.00869517 0.786458 0.00934489 0.798339 0.0100119 0.808926 0.0302883 0.97113 0.0563128 1.08328 0.0699193 1.13162 0.0903387 1.19346 0.110436 1.25049 0.130477 1.3037 0.1506 1.35568 0.170562 1.40617 0.190735 1.45659 0.211216 1.50689 0.23077 1.55604 0.250865 1.60468 0.270867 1.65538 0.291848 1.70722 0.311206 1.75629 0.33157 1.80894 0.351421 1.86063 0.371393 1.91203 0.391601 1.96346 0.412448 2.01746 0.431641 2.06862 0.452495 2.122 0.472617 2.17538 0.493031 2.22941 0.512859 2.2831 0.533016 2.33865 0.553035 2.39413 0.573176 2.45137 0.593277 2.51099 0.613377 2.5727 0.633379 2.63766 0.653992 2.70778 0.673588 2.77919 0.693634 2.85729 0.713821 2.94187 0.733941 3.03524 0.753899 3.13521 0.774092 3.24643 0.794063 3.37042 0.814272 3.51202 0.834305 3.67545 0.854488 3.86439 0.874258 4.08771 0.8944 4.37896 0.914658 4.74258 0.934178 5.21534 0.954009 5.92056 0.973145 7.05016 0.990594 9.28557 Model Fit Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 8.99464e-006 0.0313833 1.552e-005 0.0393695 2.61021e-005 0.0527048 4.28409e-005 0.0751593 6.86973e-005 0.113325 0.000107744 0.17644 0.000165451 0.263699 0.000249 0.350956 0.000367617 0.422135 0.000532902 0.478235 0.000759152 0.523408 0.00106364 0.560822 0.00146685 0.59261 0.0019926 0.620233 0.00266816 0.644743 0.0035241 0.666951 0.00459423 0.687542 0.00591521 0.707624 0.00752618 0.727151 0.00946821 0.804493 0.0117837 0.826239 0.0145155 0.846299 0.0177065 0.890363 0.0213984 0.910216 0.0256312 0.930166 0.0304422 0.950858 0.0358654 0.972873 0.0419308 0.996806 0.0486636 1.02329 0.056084 1.05293 0.0642067 1.08623 0.0730404 1.12323 0.0825882 1.16318 0.0928471 1.20454 0.103808 1.24549 0.115456 1.28467 0.127772 1.32146 0.140731 1.35583 0.154302 1.38804 0.168452 1.41847 0.183144 1.44752 0.198337 1.47558 0.213989 1.50301 0.230053 1.56504 0.246485 1.59192 0.263236 1.61908 0.280259 1.68226 0.297506 1.71052 0.314931 1.77852 0.332486 1.80886 0.350127 1.84073 0.367811 1.9115 0.385494 1.94588 0.403138 1.98128 0.420705 2.04243 0.438159 2.07776 0.455467 2.14077 0.472598 2.17411 0.489524 2.20638 0.50622 2.27083 0.522661 2.30091 0.538827 2.36915 0.5547 2.39785 0.570262 2.4264 0.585499 2.4946 0.6004 2.52323 0.614954 2.59304 0.629153 2.62266 0.642991 2.65321 0.656462 2.7233 0.669563 2.75548 0.682292 2.82794 0.694649 2.86098 0.706634 2.89402 0.718248 2.9712 0.729495 3.00293 0.740378 3.07758 0.7509 3.10761 0.761068 3.18574 0.770887 3.2145 0.780363 3.31236 0.789502 3.34059 0.798311 3.36908 0.806799 3.4723 0.814972 3.50158 0.822838 3.59484 0.830405 3.62554 0.837683 3.72095 0.844677 3.75277 0.851398 3.85018 0.857853 3.88184 0.86405 3.98546 0.869999 4.0158 0.875705 4.12828 0.881179 4.15717 0.886428 4.28055 0.89146 4.30864 0.896281 4.43344 0.900901 4.46172 0.905326 4.59032 0.909563 4.61976 0.91362 4.74593 0.917503 4.77695 0.92122 4.91117 0.924775 4.94304 0.928177 5.084 0.931431 5.11513 0.934542 5.25357 0.937517 5.28322 0.940362 5.43808 0.94308 5.46677 0.945679 5.62997 0.948162 5.65885 0.950534 5.78458 0.952801 5.89922 0.954966 5.93062 0.957034 6.04439 0.95901 6.07768 0.960896 6.17985 0.962697 6.21314 0.964417 6.34276 0.966059 6.37458 0.967626 6.50849 0.969123 6.67598 0.970551 6.70689 0.971914 6.96412 0.973215 6.99647 0.974456 7.27641 0.97564 7.31155 0.976771 7.51469 0.977849 7.70063 0.978878 7.73686 0.97986 7.95311 0.980796 7.98766 0.981689 8.14482 0.982542 8.28869 0.983354 8.32343 0.984129 8.48587 0.984869 8.52375 0.985574 8.66516 0.986247 8.70606 0.986888 8.81088 0.9875 8.90702 0.988083 8.9462 0.98864 9.04977 0.98917 9.08867 0.989676 9.16801 0.990158 9.2298 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-598 rep of 597 cook sample 6cs-3 Operator: saw jms Submitter: File: C:\...\DOCUME~1\000-598.SMP Started: 8/23/2017 2:05:59PM Analysis Adsorptive: N2 Completed: 8/24/2017 11:56:13AM Analysis Bath Temp.: -195.988 °C Report Time: 8/24/2017 11:56:13AM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4495 cm³ Measured Cold Free Space: 48.2861 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Standard Deviation of Fit: 0.03257, cm³/g STP Goodness of Fit Input Data Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 5.3147e-006 0.012784 3.02841e-006 0.0265899 2.55327e-006 0.04042 2.98443e-006 0.0541125 4.22767e-006 0.0674654 6.42296e-006 0.0815294 9.48645e-006 0.0954553 1.3704e-005 0.109191 1.90916e-005 0.122729 2.58074e-005 0.135977 3.39114e-005 0.148912 4.44261e-005 0.162853 5.64949e-005 0.17636 6.99135e-005 0.189387 8.2363e-005 0.199625 9.53821e-005 0.209809 0.000114564 0.222943 0.000130364 0.232918 0.00014792 0.24275 0.0001666 0.252499 0.000186319 0.262173 0.000207299 0.271751 0.000229665 0.281212 0.000253758 0.290533 0.000278572 0.299803 0.000304873 0.308957 0.000340502 0.320852 0.000378057 0.332497 0.000416886 0.34377 0.000456972 0.354593 0.000497242 0.36497 0.000538435 0.374834 0.000580865 0.384489 0.000623933 0.393682 0.000666468 0.402364 0.000709517 0.410753 0.000752883 0.418817 0.000796511 0.426411 0.00083901 0.433703 0.000881528 0.440633 0.000923552 0.447263 0.000965114 0.45351 0.00100564 0.459354 0.00104551 0.464877 0.00108456 0.470196 0.00112273 0.475147 0.00115946 0.479778 0.00119589 0.484214 0.00123058 0.488439 0.00126456 0.492348 0.00129686 0.495976 0.0013284 0.499398 0.00135896 0.502626 0.0013878 0.505549 0.00144677 0.512103 0.00150711 0.518547 0.00156855 0.52492 0.00163079 0.531178 0.00169463 0.537337 0.00175923 0.543438 0.0018254 0.54942 0.00189242 0.555321 0.00196079 0.561149 0.00203011 0.566898 0.00210072 0.572544 0.00217218 0.578109 0.00224436 0.583592 0.00233653 0.590496 0.00242245 0.596726 0.00249904 0.601866 0.00257767 0.606865 0.00265651 0.611808 0.00273642 0.616702 0.00281793 0.621458 0.00289953 0.626161 0.00298292 0.630769 0.00306735 0.635318 0.00315195 0.639815 0.00323798 0.644192 0.00332591 0.64847 0.00341313 0.652739 0.00350262 0.656858 0.00359318 0.660919 0.00368361 0.664893 0.00377649 0.668755 0.00386976 0.672583 0.00396347 0.676371 0.00405755 0.680082 0.00415417 0.683617 0.0042514 0.687109 0.00437898 0.691999 0.00447861 0.695214 0.00457897 0.698425 0.00467977 0.70155 0.00478198 0.704625 0.00488563 0.707615 0.00498958 0.710495 0.00509318 0.713391 0.00519967 0.716149 0.00530587 0.718901 0.00541346 0.721529 0.0055218 0.724113 0.00563032 0.726645 0.00573969 0.729041 0.00584953 0.73151 0.00596165 0.733812 0.00607315 0.736133 0.00618531 0.738356 0.00629711 0.740524 0.00641055 0.742685 0.00652446 0.744708 0.00663973 0.746699 0.00675577 0.748643 0.00739213 0.762059 0.00803561 0.774625 0.00869517 0.786458 0.00934489 0.798339 0.0100119 0.808926 0.0302883 0.97113 0.0563128 1.08328 0.0699193 1.13162 0.0903387 1.19346 0.110436 1.25049 0.130477 1.3037 0.1506 1.35568 0.170562 1.40617 0.190735 1.45659 0.211216 1.50689 0.23077 1.55604 0.250865 1.60468 0.270867 1.65538 0.291848 1.70722 0.311206 1.75629 0.33157 1.80894 0.351421 1.86063 0.371393 1.91203 0.391601 1.96346 0.412448 2.01746 0.431641 2.06862 0.452495 2.122 0.472617 2.17538 0.493031 2.22941 0.512859 2.2831 0.533016 2.33865 0.553035 2.39413 0.573176 2.45137 0.593277 2.51099 0.613377 2.5727 0.633379 2.63766 0.653992 2.70778 0.673588 2.77919 0.693634 2.85729 0.713821 2.94187 0.733941 3.03524 0.753899 3.13521 0.774092 3.24643 0.794063 3.37042 0.814272 3.51202 0.834305 3.67545 0.854488 3.86439 0.874258 4.08771 0.8944 4.37896 0.914658 4.74258 0.934178 5.21534 0.954009 5.92056 0.973145 7.05016 0.990594 9.28557 Model Fit Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 8.99464e-006 0.0313833 1.552e-005 0.0393695 2.61021e-005 0.0527048 4.28409e-005 0.0751593 6.86973e-005 0.113325 0.000107744 0.17644 0.000165451 0.263699 0.000249 0.350956 0.000367617 0.422135 0.000532902 0.478235 0.000759152 0.523408 0.00106364 0.560822 0.00146685 0.59261 0.0019926 0.620233 0.00266816 0.644743 0.0035241 0.666951 0.00459423 0.687542 0.00591521 0.707624 0.00752618 0.727151 0.00946821 0.804493 0.0117837 0.826239 0.0145155 0.846299 0.0177065 0.890363 0.0213984 0.910216 0.0256312 0.930166 0.0304422 0.950858 0.0358654 0.972873 0.0419308 0.996806 0.0486636 1.02329 0.056084 1.05293 0.0642067 1.08623 0.0730404 1.12323 0.0825882 1.16318 0.0928471 1.20454 0.103808 1.24549 0.115456 1.28467 0.127772 1.32146 0.140731 1.35583 0.154302 1.38804 0.168452 1.41847 0.183144 1.44752 0.198337 1.47558 0.213989 1.50301 0.230053 1.56504 0.246485 1.59192 0.263236 1.61908 0.280259 1.68226 0.297506 1.71052 0.314931 1.77852 0.332486 1.80886 0.350127 1.84073 0.367811 1.9115 0.385494 1.94588 0.403138 1.98128 0.420705 2.04243 0.438159 2.07776 0.455467 2.14077 0.472598 2.17411 0.489524 2.20638 0.50622 2.27083 0.522661 2.30091 0.538827 2.36915 0.5547 2.39785 0.570262 2.4264 0.585499 2.4946 0.6004 2.52323 0.614954 2.59304 0.629153 2.62266 0.642991 2.65321 0.656462 2.7233 0.669563 2.75548 0.682292 2.82794 0.694649 2.86098 0.706634 2.89402 0.718248 2.9712 0.729495 3.00293 0.740378 3.07758 0.7509 3.10761 0.761068 3.18574 0.770887 3.2145 0.780363 3.31236 0.789502 3.34059 0.798311 3.36908 0.806799 3.4723 0.814972 3.50158 0.822838 3.59484 0.830405 3.62554 0.837683 3.72095 0.844677 3.75277 0.851398 3.85018 0.857853 3.88184 0.86405 3.98546 0.869999 4.0158 0.875705 4.12828 0.881179 4.15717 0.886428 4.28055 0.89146 4.30864 0.896281 4.43344 0.900901 4.46172 0.905326 4.59032 0.909563 4.61976 0.91362 4.74593 0.917503 4.77695 0.92122 4.91117 0.924775 4.94304 0.928177 5.084 0.931431 5.11513 0.934542 5.25357 0.937517 5.28322 0.940362 5.43808 0.94308 5.46677 0.945679 5.62997 0.948162 5.65885 0.950534 5.78458 0.952801 5.89922 0.954966 5.93062 0.957034 6.04439 0.95901 6.07768 0.960896 6.17985 0.962697 6.21314 0.964417 6.34276 0.966059 6.37458 0.967626 6.50849 0.969123 6.67598 0.970551 6.70689 0.971914 6.96412 0.973215 6.99647 0.974456 7.27641 0.97564 7.31155 0.976771 7.51469 0.977849 7.70063 0.978878 7.73686 0.97986 7.95311 0.980796 7.98766 0.981689 8.14482 0.982542 8.28869 0.983354 8.32343 0.984129 8.48587 0.984869 8.52375 0.985574 8.66516 0.986247 8.70606 0.986888 8.81088 0.9875 8.90702 0.988083 8.9462 0.98864 9.04977 0.98917 9.08867 0.989676 9.16801 0.990158 9.2298