ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Summary Report Surface Area Single point surface area at P/Po = 0.291237599: 4.9115 m²/g BET Surface Area: 5.0390 m²/g t-Plot External Surface Area: 5.7881 m²/g BJH Adsorption cumulative surface area of pores between 17.000 Å and 3000.000 Å width: 3.827 m²/g BJH Desorption cumulative surface area of pores between 17.000 Å and 3000.000 Å width: 5.4269 m²/g Pore Volume Single point desorption total pore volume of pores less than 996.312 Å width at P/Po = 0.980174201: 0.012881 cm³/g t-Plot micropore volume: -0.000255 cm³/g BJH Adsorption cumulative volume of pores between 17.000 Å and 3000.000 Å width: 0.012218 cm³/g BJH Desorption cumulative volume of pores between 17.000 Å and 3000.000 Å width: 0.013161 cm³/g Pore Size Desorption average pore width (4V/A by BET): 102.2522 Å BJH Adsorption average pore width (4V/A): 127.711 Å BJH Desorption average pore width (4V/A): 97.007 Å Horvath-Kawazoe Maximum pore volume at P/Po = 0.010034034: 0.001261 cm³/g Median pore width: 7.344 Å ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Isotherm Tabular Report Quantity Relative Absolute Adsorbed Elapsed Saturation Pressure Pressure (cm³/g Time Pressure (P/Po) (mmHg) STP) (h:min) (mmHg) ----- 1.#QNAN0000 1.#QNAN0 1.#QNB 00:53 741.363525 0.000004903 0.003635 0.0128 01:46 1.#QNAN0 0.000003011 0.002232 0.0266 02:25 1.#QNAN0 0.000002641 0.001958 0.0403 03:04 1.#QNAN0 0.000003048 0.002259 0.0540 03:43 1.#QNAN0 0.000004157 0.003082 0.0673 04:23 1.#QNAN0 0.000006216 0.004609 0.0801 05:03 1.#QNAN0 0.000009341 0.006926 0.0939 05:12 1.#QNAN0 0.000013594 0.010079 0.1077 05:22 1.#QNAN0 0.000018982 0.014074 0.1211 05:31 1.#QNAN0 0.000025669 0.019033 0.1343 05:39 1.#QNAN0 0.000033697 0.024985 0.1472 05:48 1.#QNAN0 0.000044118 0.032713 0.1611 05:56 1.#QNAN0 0.000056024 0.041541 0.1746 06:04 1.#QNAN0 0.000069370 0.051436 0.1876 06:13 1.#QNAN0 0.000081408 0.060363 0.1979 06:22 1.#QNAN0 0.000094676 0.070201 0.2080 06:31 1.#QNAN0 0.000113249 0.083973 0.2212 06:39 1.#QNAN0 0.000129123 0.095744 0.2311 06:47 1.#QNAN0 0.000146155 0.108374 0.2410 06:56 1.#QNAN0 0.000164359 0.121872 0.2508 07:04 1.#QNAN0 0.000183754 0.136254 0.2605 07:13 1.#QNAN0 0.000204548 0.151674 0.2701 07:21 1.#QNAN0 0.000226497 0.167950 0.2796 07:29 1.#QNAN0 0.000249630 0.185104 0.2890 07:38 1.#QNAN0 0.000274116 0.203261 0.2983 07:46 1.#QNAN0 0.000307637 0.228118 0.3104 07:53 1.#QNAN0 0.000335002 0.248411 0.3195 08:01 1.#QNAN0 0.000371234 0.275279 0.3311 08:09 1.#QNAN0 0.000409217 0.303445 0.3424 08:16 1.#QNAN0 0.000448445 0.332535 0.3533 08:23 1.#QNAN0 0.000488458 0.362208 0.3637 08:30 1.#QNAN0 0.000530314 0.393247 0.3740 08:37 1.#QNAN0 0.000571812 0.424020 0.3836 08:45 1.#QNAN0 0.000614215 0.455465 0.3930 08:52 1.#QNAN0 0.000656358 0.486718 0.4018 08:59 1.#QNAN0 0.000698660 0.518088 0.4103 09:06 1.#QNAN0 0.000741051 0.549525 0.4183 09:13 1.#QNAN0 0.000783677 0.581137 0.4261 09:21 1.#QNAN0 0.000825368 0.612055 0.4334 09:28 1.#QNAN0 0.000867380 0.643212 0.4404 09:35 1.#QNAN0 0.000908944 0.674036 0.4470 09:42 1.#QNAN0 0.000950026 0.704503 0.4534 09:49 1.#QNAN0 0.000990220 0.734312 0.4594 09:57 1.#QNAN0 0.001029298 0.763294 0.4650 10:04 1.#QNAN0 0.001068424 0.792311 0.4705 10:11 1.#QNAN0 0.001106367 0.820452 0.4756 10:18 1.#QNAN0 0.001143778 0.848197 0.4804 10:25 1.#QNAN0 0.001180401 0.875359 0.4851 10:32 1.#QNAN0 0.001214305 0.900505 0.4893 10:39 1.#QNAN0 0.001247664 0.925246 0.4933 10:46 1.#QNAN0 0.001279922 0.949172 0.4971 10:53 1.#QNAN0 0.001311247 0.972405 0.5007 11:00 1.#QNAN0 0.001341735 0.995018 0.5040 11:07 1.#QNAN0 0.001371674 1.017224 0.5072 11:14 1.#QNAN0 0.001429868 1.060385 0.5139 11:22 1.#QNAN0 0.001489244 1.104422 0.5204 11:30 1.#QNAN0 0.001549919 1.149423 0.5268 11:38 1.#QNAN0 0.001611478 1.195080 0.5332 11:45 1.#QNAN0 0.001674122 1.241542 0.5394 11:53 1.#QNAN0 0.001738447 1.289250 0.5456 12:00 1.#QNAN0 0.001803295 1.337348 0.5517 12:08 1.#QNAN0 0.001869299 1.386302 0.5576 12:15 1.#QNAN0 0.001936359 1.436041 0.5635 12:23 1.#QNAN0 0.002004951 1.486915 0.5693 12:30 1.#QNAN0 0.002074318 1.538365 0.5750 12:38 1.#QNAN0 0.002144685 1.590556 0.5807 12:45 1.#QNAN0 0.002216467 1.643798 0.5862 12:52 1.#QNAN0 0.002309351 1.712689 0.5933 12:59 1.#QNAN0 0.002396952 1.777663 0.5998 13:06 1.#QNAN0 0.002479098 1.838592 0.6055 13:14 1.#QNAN0 0.002556425 1.895948 0.6106 13:22 1.#QNAN0 0.002634718 1.954022 0.6157 13:30 1.#QNAN0 0.002714321 2.013067 0.6206 13:38 1.#QNAN0 0.002794796 2.072759 0.6254 13:46 1.#QNAN0 0.002876291 2.133208 0.6302 13:54 1.#QNAN0 0.002958814 2.194420 0.6349 14:02 1.#QNAN0 0.003042173 2.256253 0.6395 14:10 1.#QNAN0 0.003126472 2.318784 0.6440 14:18 1.#QNAN0 0.003211760 2.382048 0.6485 14:26 1.#QNAN0 0.003297938 2.445971 0.6528 14:33 1.#QNAN0 0.003384867 2.510454 0.6571 14:41 1.#QNAN0 0.003472748 2.575642 0.6614 14:49 1.#QNAN0 0.003562239 2.642026 0.6654 14:57 1.#QNAN0 0.003653193 2.709495 0.6694 15:05 1.#QNAN0 0.003744220 2.777020 0.6735 15:13 1.#QNAN0 0.003836968 2.845819 0.6774 15:20 1.#QNAN0 0.003929950 2.914793 0.6812 15:27 1.#QNAN0 0.004023930 2.984508 0.6850 15:35 1.#QNAN0 0.004118395 3.054582 0.6887 15:42 1.#QNAN0 0.004213678 3.125263 0.6923 15:49 1.#QNAN0 0.004309948 3.196680 0.6958 15:57 1.#QNAN0 0.004429812 3.285594 0.7003 16:04 1.#QNAN0 0.004528843 3.359059 0.7036 16:12 1.#QNAN0 0.004629121 3.433451 0.7068 16:21 1.#QNAN0 0.004730040 3.508317 0.7101 16:29 1.#QNAN0 0.004830993 3.583207 0.7132 16:36 1.#QNAN0 0.004933874 3.659530 0.7162 16:44 1.#QNAN0 0.005037339 3.736287 0.7192 16:52 1.#QNAN0 0.005141032 3.813213 0.7221 17:00 1.#QNAN0 0.005246457 3.891424 0.7249 17:08 1.#QNAN0 0.005351773 3.969556 0.7277 17:16 1.#QNAN0 0.005458358 4.048628 0.7304 17:24 1.#QNAN0 0.005565897 4.128410 0.7330 17:32 1.#QNAN0 0.005673494 4.208235 0.7356 17:40 1.#QNAN0 0.005781658 4.288481 0.7381 17:48 1.#QNAN0 0.005890321 4.369096 0.7406 17:55 1.#QNAN0 0.006000369 4.450741 0.7430 18:03 1.#QNAN0 0.006111549 4.533226 0.7453 18:11 1.#QNAN0 0.006222637 4.615644 0.7475 18:19 1.#QNAN0 0.006334192 4.698406 0.7498 18:26 1.#QNAN0 0.006447032 4.782125 0.7520 18:34 1.#QNAN0 0.006561523 4.867068 0.7541 18:42 1.#QNAN0 0.006675892 4.951922 0.7561 18:50 1.#QNAN0 0.006789834 5.036458 0.7581 18:57 1.#QNAN0 1.#QNAN0000 1.#QNAN0 1.#QNB 18:59 741.765259 0.007413145 5.499022 0.7717 19:07 1.#QNAN0 0.008037847 5.962593 0.7850 19:13 1.#QNAN0 0.008694188 6.449690 0.7957 19:20 1.#QNAN0 0.009358324 6.942571 0.8057 19:26 1.#QNAN0 0.010034034 7.443924 0.8150 19:28 1.#QNAN0 0.030272247 22.458317 0.9685 19:31 1.#QNAN0 0.049538176 36.751637 1.0475 19:33 1.#QNAN0 0.069699806 51.709496 1.1109 19:34 1.#QNAN0 0.089965135 66.744431 1.1661 19:35 1.#QNAN0 0.110440706 81.935875 1.2154 19:37 1.#QNAN0 0.130478594 96.802429 1.2607 19:38 1.#QNAN0 0.150574055 111.711838 1.3042 19:39 1.#QNAN0 0.171178067 126.999290 1.3481 19:41 1.#QNAN0 0.190652951 141.448639 1.3878 19:42 1.#QNAN0 0.210766953 156.372299 1.4281 19:43 1.#QNAN0 0.231572127 171.808899 1.4692 19:44 1.#QNAN0 0.251655693 186.711151 1.5108 19:46 1.#QNAN0 0.271042459 201.095749 1.5503 19:47 1.#QNAN0 0.291237599 216.080246 1.5919 19:48 1.#QNAN0 0.311266600 230.942719 1.6337 19:50 1.#QNAN0 0.332289467 246.541702 1.6783 19:51 1.#QNAN0 0.351269233 260.626190 1.7189 19:53 1.#QNAN0 0.372247703 276.193909 1.7646 19:55 1.#QNAN0 0.391447999 290.441193 1.8056 19:56 1.#QNAN0 0.412538485 306.092529 1.8506 19:58 1.#QNAN0 0.431564747 320.211029 1.8928 19:59 1.#QNAN0 0.452944515 336.077515 1.9385 20:01 1.#QNAN0 0.472790370 350.806152 1.9803 20:03 1.#QNAN0 0.492909559 365.736145 2.0249 20:04 1.#QNAN0 0.512888502 380.564026 2.0691 20:06 1.#QNAN0 0.533404736 395.790863 2.1150 20:08 1.#QNAN0 0.553174063 410.461823 2.1610 20:09 1.#QNAN0 0.572990203 425.169678 2.2083 20:11 1.#QNAN0 0.593124766 440.112000 2.2584 20:12 1.#QNAN0 0.613265848 455.061462 2.3117 20:14 1.#QNAN0 0.633172089 469.834717 2.3668 20:15 1.#QNAN0 0.653431030 484.872131 2.4275 20:17 1.#QNAN0 0.673582815 499.827942 2.4904 20:18 1.#QNAN0 0.693316649 514.473755 2.5579 20:19 1.#QNAN0 0.713681807 529.590698 2.6342 20:21 1.#QNAN0 0.733686187 544.437622 2.7166 20:22 1.#QNAN0 0.753710237 559.301941 2.8075 20:24 1.#QNAN0 0.773973969 574.341675 2.9090 20:25 1.#QNAN0 0.794024071 589.223022 3.0242 20:26 1.#QNAN0 0.814072088 604.105835 3.1549 20:28 1.#QNAN0 0.834055900 618.941284 3.3081 20:30 1.#QNAN0 0.854229817 633.918091 3.4873 20:32 1.#QNAN0 0.874047181 648.627502 3.7014 20:33 1.#QNAN0 0.894174044 663.569885 3.9733 20:35 1.#QNAN0 0.914213673 678.447815 4.3253 20:37 1.#QNAN0 0.934099127 693.214905 4.7943 20:40 1.#QNAN0 0.953754811 707.808533 5.4673 20:42 1.#QNAN0 0.972771312 721.934937 6.5662 20:46 1.#QNAN0 0.990498203 735.108276 8.7226 20:51 1.#QNAN0 0.980174201 727.453125 8.3276 20:53 1.#QNAN0 0.966804313 717.544067 7.3946 20:57 1.#QNAN0 0.947477326 703.209961 6.3917 21:00 1.#QNAN0 1.#QNAN0000 1.#QNAN0 1.#QNB 21:02 742.198914 0.935819901 694.564514 5.9368 21:04 1.#QNAN0 0.915172604 679.240112 5.3536 21:07 1.#QNAN0 0.895611145 664.721619 4.9356 21:09 1.#QNAN0 0.874980788 649.409790 4.5926 21:11 1.#QNAN0 0.854981753 634.566528 4.3149 21:12 1.#QNAN0 0.834856980 619.629944 4.0760 21:14 1.#QNAN0 0.814533033 604.545532 3.8691 21:16 1.#QNAN0 0.794335646 589.555054 3.6900 21:17 1.#QNAN0 0.774348454 574.720581 3.5291 21:19 1.#QNAN0 0.754099916 559.692139 3.3880 21:21 1.#QNAN0 0.734042906 544.805847 3.2645 21:22 1.#QNAN0 0.714018131 529.943481 3.1541 21:23 1.#QNAN0 0.693828557 514.958801 3.0537 21:25 1.#QNAN0 0.673734623 500.045105 2.9645 21:26 1.#QNAN0 0.653663755 485.148529 2.8821 21:28 1.#QNAN0 0.633553497 470.222717 2.8070 21:30 1.#QNAN0 0.613436372 455.291809 2.7378 21:31 1.#QNAN0 0.593218303 440.285980 2.6723 21:33 1.#QNAN0 0.573282878 425.489929 2.6114 21:34 1.#QNAN0 0.553014275 410.446594 2.5520 21:35 1.#QNAN0 0.532994312 395.587799 2.4962 21:37 1.#QNAN0 0.512995729 380.744873 2.4396 21:39 1.#QNAN0 0.493322965 366.143768 2.3701 21:40 1.#QNAN0 0.473822689 351.670685 2.2144 21:43 1.#QNAN0 0.452069857 335.525757 2.0291 21:45 1.#QNAN0 0.431277044 320.093353 1.9273 21:46 1.#QNAN0 0.412177214 305.917480 1.8643 21:48 1.#QNAN0 0.392018355 290.955597 1.8102 21:49 1.#QNAN0 0.371522699 275.743744 1.7614 21:50 1.#QNAN0 0.351378437 260.792694 1.7172 21:52 1.#QNAN0 0.331423193 245.981934 1.6745 21:53 1.#QNAN0 0.311331664 231.070023 1.6327 21:54 1.#QNAN0 0.291147949 216.089691 1.5916 21:55 1.#QNAN0 0.271174263 201.265244 1.5515 21:57 1.#QNAN0 0.251062422 186.338257 1.5119 21:58 1.#QNAN0 0.231033927 171.473129 1.4726 21:59 1.#QNAN0 0.211016944 156.616547 1.4337 22:01 1.#QNAN0 0.190781400 141.597748 1.3946 22:02 1.#QNAN0 0.170779631 126.752457 1.3553 22:04 1.#QNAN0 0.150721675 111.865463 1.3140 22:05 1.#QNAN0 0.130624256 96.949181 1.2720 22:07 1.#QNAN0 0.110565631 82.061691 1.2286 22:09 1.#QNAN0 0.090495864 67.165932 1.1813 22:11 1.#QNAN0 0.070403785 52.253613 1.1281 22:13 1.#QNAN0 0.050341953 37.363743 1.0659 22:15 1.#QNAN0 0.030292467 22.483036 0.9819 22:17 1.#QNAN0 0.009926799 7.367659 0.8186 22:22 1.#QNAN0 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Isotherm Linear Plot 000-597 cook sample 6cs-3 - Adsorption Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 4.90273e-006 0.0128345 3.01067e-006 0.0265556 2.64145e-006 0.0403348 3.0475e-006 0.0539532 4.15677e-006 0.0672834 6.21601e-006 0.0800843 9.34144e-006 0.0939413 1.35937e-005 0.107652 1.89817e-005 0.121115 2.56692e-005 0.134309 3.36969e-005 0.147192 4.41181e-005 0.161107 5.60239e-005 0.174593 6.93696e-005 0.187617 8.14081e-005 0.197877 9.46756e-005 0.208045 0.000113249 0.221161 0.000129123 0.231138 0.000146155 0.241013 0.000164359 0.250804 0.000183754 0.260495 0.000204548 0.270076 0.000226497 0.279572 0.00024963 0.288977 0.000274116 0.298282 0.000307637 0.310444 0.000335002 0.319524 0.000371234 0.331054 0.000409217 0.342374 0.000448445 0.353266 0.000488458 0.363721 0.000530314 0.37401 0.000571812 0.383648 0.000614215 0.39297 0.000656358 0.401807 0.00069866 0.41027 0.000741051 0.418325 0.000783677 0.426094 0.000825368 0.433379 0.00086738 0.440358 0.000908944 0.447036 0.000950026 0.453383 0.00099022 0.459376 0.0010293 0.465021 0.00106842 0.470459 0.00110637 0.475578 0.00114378 0.480438 0.0011804 0.485057 0.00121431 0.489288 0.00124766 0.493332 0.00127992 0.497098 0.00131125 0.500665 0.00134173 0.504026 0.00137167 0.507239 0.00142987 0.513854 0.00148924 0.52039 0.00154992 0.526825 0.00161148 0.533177 0.00167412 0.539417 0.00173845 0.545561 0.0018033 0.55165 0.0018693 0.557644 0.00193636 0.563526 0.00200495 0.569321 0.00207432 0.575039 0.00214468 0.580656 0.00221647 0.586187 0.00230935 0.59332 0.00239695 0.59978 0.0024791 0.605541 0.00255642 0.610637 0.00263472 0.615661 0.00271432 0.620603 0.0027948 0.625439 0.00287629 0.630206 0.00295881 0.634891 0.00304217 0.639493 0.00312647 0.643997 0.00321176 0.648474 0.00329794 0.652847 0.00338487 0.657121 0.00347275 0.661353 0.00356224 0.665441 0.00365319 0.66943 0.00374422 0.673481 0.00383697 0.677381 0.00392995 0.681201 0.00402393 0.684993 0.0041184 0.688668 0.00421368 0.692298 0.00430995 0.695792 0.00442981 0.700256 0.00452884 0.703599 0.00462912 0.706846 0.00473004 0.710056 0.00483099 0.713173 0.00493387 0.716177 0.00503734 0.719216 0.00514103 0.722118 0.00524646 0.724922 0.00535177 0.727691 0.00545836 0.730375 0.0055659 0.733049 0.00567349 0.735615 0.00578166 0.738126 0.00589032 0.740589 0.00600037 0.743019 0.00611155 0.745295 0.00622264 0.747547 0.00633419 0.749771 0.00644703 0.751995 0.00656152 0.754056 0.00667589 0.756148 0.00678983 0.758136 0.00741314 0.771722 0.00803785 0.785017 0.00869419 0.795671 0.00935832 0.805674 0.010034 0.815038 0.0302722 0.968469 0.0495382 1.04746 0.0696998 1.1109 0.0899651 1.16608 0.110441 1.21539 0.130479 1.26066 0.150574 1.30424 0.171178 1.34814 0.190653 1.38784 0.210767 1.42808 0.231572 1.46924 0.251656 1.51075 0.271042 1.55028 0.291238 1.59187 0.311267 1.63368 0.332289 1.67828 0.351269 1.71887 0.372248 1.76462 0.391448 1.8056 0.412538 1.85064 0.431565 1.89276 0.452945 1.93847 0.47279 1.98032 0.49291 2.02493 0.512889 2.06905 0.533405 2.11503 0.553174 2.16104 0.57299 2.20832 0.593125 2.25841 0.613266 2.31174 0.633172 2.36679 0.653431 2.42753 0.673583 2.4904 0.693317 2.55787 0.713682 2.63423 0.733686 2.71656 0.75371 2.80747 0.773974 2.909 0.794024 3.02424 0.814072 3.15487 0.834056 3.30807 0.85423 3.48729 0.874047 3.70139 0.894174 3.97332 0.914214 4.3253 0.934099 4.79426 0.953755 5.46727 0.972771 6.56621 0.990498 8.7226 000-597 cook sample 6cs-3 - Desorption Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 0.990498 8.7226 0.980174 8.32763 0.966804 7.39461 0.947477 6.39174 0.93582 5.93685 0.915173 5.35359 0.895611 4.9356 0.874981 4.59256 0.854982 4.31486 0.834857 4.07599 0.814533 3.86912 0.794336 3.68997 0.774348 3.52911 0.7541 3.388 0.734043 3.26449 0.714018 3.15413 0.693829 3.05368 0.673735 2.96449 0.653664 2.88206 0.633553 2.80695 0.613436 2.73779 0.593218 2.67233 0.573283 2.61141 0.553014 2.552 0.532994 2.4962 0.512996 2.43955 0.493323 2.37012 0.473823 2.21442 0.45207 2.02909 0.431277 1.92732 0.412177 1.86434 0.392018 1.8102 0.371523 1.76143 0.351378 1.71721 0.331423 1.67454 0.311332 1.63271 0.291148 1.5916 0.271174 1.5515 0.251062 1.51189 0.231034 1.47258 0.211017 1.43367 0.190781 1.39456 0.17078 1.35531 0.150722 1.31402 0.130624 1.27203 0.110566 1.22857 0.0904959 1.18128 0.0704038 1.12812 0.050342 1.06593 0.0302925 0.981894 0.0099268 0.818587 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Isotherm Log Plot 000-597 cook sample 6cs-3 - Adsorption Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 4.90273e-006 0.0128345 3.01067e-006 0.0265556 2.64145e-006 0.0403348 3.0475e-006 0.0539532 4.15677e-006 0.0672834 6.21601e-006 0.0800843 9.34144e-006 0.0939413 1.35937e-005 0.107652 1.89817e-005 0.121115 2.56692e-005 0.134309 3.36969e-005 0.147192 4.41181e-005 0.161107 5.60239e-005 0.174593 6.93696e-005 0.187617 8.14081e-005 0.197877 9.46756e-005 0.208045 0.000113249 0.221161 0.000129123 0.231138 0.000146155 0.241013 0.000164359 0.250804 0.000183754 0.260495 0.000204548 0.270076 0.000226497 0.279572 0.00024963 0.288977 0.000274116 0.298282 0.000307637 0.310444 0.000335002 0.319524 0.000371234 0.331054 0.000409217 0.342374 0.000448445 0.353266 0.000488458 0.363721 0.000530314 0.37401 0.000571812 0.383648 0.000614215 0.39297 0.000656358 0.401807 0.00069866 0.41027 0.000741051 0.418325 0.000783677 0.426094 0.000825368 0.433379 0.00086738 0.440358 0.000908944 0.447036 0.000950026 0.453383 0.00099022 0.459376 0.0010293 0.465021 0.00106842 0.470459 0.00110637 0.475578 0.00114378 0.480438 0.0011804 0.485057 0.00121431 0.489288 0.00124766 0.493332 0.00127992 0.497098 0.00131125 0.500665 0.00134173 0.504026 0.00137167 0.507239 0.00142987 0.513854 0.00148924 0.52039 0.00154992 0.526825 0.00161148 0.533177 0.00167412 0.539417 0.00173845 0.545561 0.0018033 0.55165 0.0018693 0.557644 0.00193636 0.563526 0.00200495 0.569321 0.00207432 0.575039 0.00214468 0.580656 0.00221647 0.586187 0.00230935 0.59332 0.00239695 0.59978 0.0024791 0.605541 0.00255642 0.610637 0.00263472 0.615661 0.00271432 0.620603 0.0027948 0.625439 0.00287629 0.630206 0.00295881 0.634891 0.00304217 0.639493 0.00312647 0.643997 0.00321176 0.648474 0.00329794 0.652847 0.00338487 0.657121 0.00347275 0.661353 0.00356224 0.665441 0.00365319 0.66943 0.00374422 0.673481 0.00383697 0.677381 0.00392995 0.681201 0.00402393 0.684993 0.0041184 0.688668 0.00421368 0.692298 0.00430995 0.695792 0.00442981 0.700256 0.00452884 0.703599 0.00462912 0.706846 0.00473004 0.710056 0.00483099 0.713173 0.00493387 0.716177 0.00503734 0.719216 0.00514103 0.722118 0.00524646 0.724922 0.00535177 0.727691 0.00545836 0.730375 0.0055659 0.733049 0.00567349 0.735615 0.00578166 0.738126 0.00589032 0.740589 0.00600037 0.743019 0.00611155 0.745295 0.00622264 0.747547 0.00633419 0.749771 0.00644703 0.751995 0.00656152 0.754056 0.00667589 0.756148 0.00678983 0.758136 0.00741314 0.771722 0.00803785 0.785017 0.00869419 0.795671 0.00935832 0.805674 0.010034 0.815038 0.0302722 0.968469 0.0495382 1.04746 0.0696998 1.1109 0.0899651 1.16608 0.110441 1.21539 0.130479 1.26066 0.150574 1.30424 0.171178 1.34814 0.190653 1.38784 0.210767 1.42808 0.231572 1.46924 0.251656 1.51075 0.271042 1.55028 0.291238 1.59187 0.311267 1.63368 0.332289 1.67828 0.351269 1.71887 0.372248 1.76462 0.391448 1.8056 0.412538 1.85064 0.431565 1.89276 0.452945 1.93847 0.47279 1.98032 0.49291 2.02493 0.512889 2.06905 0.533405 2.11503 0.553174 2.16104 0.57299 2.20832 0.593125 2.25841 0.613266 2.31174 0.633172 2.36679 0.653431 2.42753 0.673583 2.4904 0.693317 2.55787 0.713682 2.63423 0.733686 2.71656 0.75371 2.80747 0.773974 2.909 0.794024 3.02424 0.814072 3.15487 0.834056 3.30807 0.85423 3.48729 0.874047 3.70139 0.894174 3.97332 0.914214 4.3253 0.934099 4.79426 0.953755 5.46727 0.972771 6.56621 0.990498 8.7226 000-597 cook sample 6cs-3 - Desorption Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 0.990498 8.7226 0.980174 8.32763 0.966804 7.39461 0.947477 6.39174 0.93582 5.93685 0.915173 5.35359 0.895611 4.9356 0.874981 4.59256 0.854982 4.31486 0.834857 4.07599 0.814533 3.86912 0.794336 3.68997 0.774348 3.52911 0.7541 3.388 0.734043 3.26449 0.714018 3.15413 0.693829 3.05368 0.673735 2.96449 0.653664 2.88206 0.633553 2.80695 0.613436 2.73779 0.593218 2.67233 0.573283 2.61141 0.553014 2.552 0.532994 2.4962 0.512996 2.43955 0.493323 2.37012 0.473823 2.21442 0.45207 2.02909 0.431277 1.92732 0.412177 1.86434 0.392018 1.8102 0.371523 1.76143 0.351378 1.71721 0.331423 1.67454 0.311332 1.63271 0.291148 1.5916 0.271174 1.5515 0.251062 1.51189 0.231034 1.47258 0.211017 1.43367 0.190781 1.39456 0.17078 1.35531 0.150722 1.31402 0.130624 1.27203 0.110566 1.22857 0.0904959 1.18128 0.0704038 1.12812 0.050342 1.06593 0.0302925 0.981894 0.0099268 0.818587 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BET Surface Area Report BET Surface Area: 5.0390 ± 0.0145 m²/g Slope: 0.856683 ± 0.002451 g/cm³ STP Y-Intercept: 0.007221 ± 0.000457 g/cm³ STP C: 119.635124 Qm: 1.1575 cm³/g STP Correlation Coefficient: 0.9999550 Molecular Cross-Sectional Area: 0.1620 nm² Quantity Relative Adsorbed Pressure (cm³/g 1/[Q(Po/P (P/Po) STP) - 1)] --- 0.049538176 1.0475 0.049759 0.069699806 1.1109 0.067443 0.089965135 1.1661 0.084779 0.110440706 1.2154 0.102150 0.130478594 1.2607 0.119031 0.150574055 1.3042 0.135915 0.171178067 1.3481 0.153197 0.190652951 1.3878 0.169735 0.210766953 1.4281 0.187001 0.231572127 1.4692 0.205111 0.251655693 1.5108 0.222593 0.271042459 1.5503 0.239842 0.291237599 1.5919 0.258131 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BET Surface Area Plot 000-597 cook sample 6cs-3 Relative Pressure (P/Po) 1/[Q(Po/P - 1)] 0.0495382 0.0497585 0.0696998 0.0674427 0.0899651 0.084779 0.110441 0.10215 0.130479 0.119031 0.150574 0.135915 0.171178 0.153197 0.190653 0.169735 0.210767 0.187001 0.231572 0.205111 0.251656 0.222593 0.271042 0.239842 0.291238 0.258131 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm t-Plot Report Micropore Volume: -0.000255 cm³/g Micropore Area: * External Surface Area: 5.7881 m²/g Slope: 0.374200 ± 0.010553 cm³/g·Å STP Y-Intercept: -0.164798 ± 0.031613 cm³/g STP Correlation Coefficient: 0.998809 Surface Area Correction Factor: 1.000 Density Conversion Factor: 0.0015468 Total Surface Area (BET): 5.0390 m²/g Thickness Range: 2.6000 Å to 3.5000 Å Thickness Equation: Harkins and Jura t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 Quantity Relative Statistical Adsorbed Pressure Thickness (cm³/g (P/Po) (Å) STP) --- 0.000004903 1.6181 0.0128 0.000003011 1.5869 0.0266 0.000002641 1.5789 0.0403 0.000003048 1.5877 0.0540 0.000004157 1.6073 0.0673 0.000006216 1.6339 0.0801 0.000009341 1.6622 0.0939 0.000013594 1.6896 0.1077 0.000018982 1.7152 0.1211 0.000025669 1.7393 0.1343 0.000033697 1.7619 0.1472 0.000044118 1.7853 0.1611 0.000056024 1.8068 0.1746 0.000069370 1.8266 0.1876 0.000081408 1.8420 0.1979 0.000094676 1.8568 0.2080 0.000113249 1.8749 0.2212 0.000129123 1.8884 0.2311 0.000146155 1.9015 0.2410 0.000164359 1.9142 0.2508 0.000183754 1.9264 0.2605 0.000204548 1.9384 0.2701 0.000226497 1.9501 0.2796 0.000249630 1.9613 0.2890 0.000274116 1.9724 0.2983 0.000307637 1.9863 0.3104 0.000335002 1.9967 0.3195 0.000371234 2.0095 0.3311 0.000409217 2.0219 0.3424 0.000448445 2.0338 0.3533 0.000488458 2.0450 0.3637 0.000530314 2.0560 0.3740 0.000571812 2.0663 0.3836 0.000614215 2.0761 0.3930 0.000656358 2.0854 0.4018 0.000698660 2.0943 0.4103 0.000741051 2.1027 0.4183 0.000783677 2.1108 0.4261 0.000825368 2.1184 0.4334 0.000867380 2.1258 0.4404 0.000908944 2.1328 0.4470 0.000950026 2.1395 0.4534 0.000990220 2.1458 0.4594 0.001029298 2.1518 0.4650 0.001068424 2.1576 0.4705 0.001106367 2.1630 0.4756 0.001143778 2.1683 0.4804 0.001180401 2.1733 0.4851 0.001214305 2.1778 0.4893 0.001247664 2.1822 0.4933 0.001279922 2.1863 0.4971 0.001311247 2.1902 0.5007 0.001341735 2.1940 0.5040 0.001371674 2.1976 0.5072 0.001429868 2.2045 0.5139 0.001489244 2.2113 0.5204 0.001549919 2.2180 0.5268 0.001611478 2.2247 0.5332 0.001674122 2.2312 0.5394 0.001738447 2.2377 0.5456 0.001803295 2.2441 0.5517 0.001869299 2.2505 0.5576 0.001936359 2.2567 0.5635 0.002004951 2.2630 0.5693 0.002074318 2.2691 0.5750 0.002144685 2.2752 0.5807 0.002216467 2.2812 0.5862 0.002309351 2.2888 0.5933 0.002396952 2.2958 0.5998 0.002479098 2.3021 0.6055 0.002556425 2.3080 0.6106 0.002634718 2.3138 0.6157 0.002714321 2.3195 0.6206 0.002794796 2.3252 0.6254 0.002876291 2.3308 0.6302 0.002958814 2.3364 0.6349 0.003042173 2.3419 0.6395 0.003126472 2.3474 0.6440 0.003211760 2.3528 0.6485 0.003297938 2.3582 0.6528 0.003384867 2.3635 0.6571 0.003472748 2.3688 0.6614 0.003562239 2.3740 0.6654 0.003653193 2.3793 0.6694 0.003744220 2.3844 0.6735 0.003836968 2.3896 0.6774 0.003929950 2.3947 0.6812 0.004023930 2.3997 0.6850 0.004118395 2.4047 0.6887 0.004213678 2.4097 0.6923 0.004309948 2.4146 0.6958 0.004429812 2.4206 0.7003 0.004528843 2.4255 0.7036 0.004629121 2.4304 0.7068 0.004730040 2.4352 0.7101 0.004830993 2.4399 0.7132 0.004933874 2.4447 0.7162 0.005037339 2.4494 0.7192 0.005141032 2.4541 0.7221 0.005246457 2.4588 0.7249 0.005351773 2.4633 0.7277 0.005458358 2.4679 0.7304 0.005565897 2.4725 0.7330 0.005673494 2.4770 0.7356 0.005781658 2.4815 0.7381 0.005890321 2.4859 0.7406 0.006000369 2.4903 0.7430 0.006111549 2.4947 0.7453 0.006222637 2.4991 0.7475 0.006334192 2.5034 0.7498 0.006447032 2.5077 0.7520 0.006561523 2.5120 0.7541 0.006675892 2.5163 0.7561 0.006789834 2.5205 0.7581 0.007413145 2.5426 0.7717 0.008037847 2.5635 0.7850 0.008694188 2.5843 0.7957 0.009358324 2.6042 0.8057 0.010034034 2.6236 0.8150 0.030272247 3.0014 0.9685 0.049538176 3.2323 1.0475 0.069699806 3.4276 1.1109 0.089965135 3.5992 1.1661 0.110440706 3.7575 1.2154 0.130478594 3.9028 1.2607 0.150574055 4.0421 1.3042 0.171178067 4.1804 1.3481 0.190652951 4.3082 1.3878 0.210766953 4.4383 1.4281 0.231572127 4.5719 1.4692 0.251655693 4.7005 1.5108 0.271042459 4.8249 1.5503 0.291237599 4.9553 1.5919 0.311266600 5.0858 1.6337 0.332289467 5.2248 1.6783 0.351269233 5.3523 1.7189 0.372247703 5.4959 1.7646 0.391447999 5.6303 1.8056 0.412538485 5.7815 1.8506 0.431564747 5.9217 1.8928 0.452944515 6.0840 1.9385 0.472790370 6.2397 1.9803 0.492909559 6.4030 2.0249 0.512888502 6.5713 2.0691 0.533404736 6.7512 2.1150 0.553174063 6.9320 2.1610 0.572990203 7.1215 2.2083 0.593124766 7.3234 2.2584 * The micropore area is not reported because either the micropore volume is negative or the calculated external surface area is larger than the total surface area. ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm t-Plot Harkins and Jura 000-597 cook sample 6cs-3 Thickness (Å) Quantity Adsorbed (cm³/g STP) 2.60423 0.805674 2.62356 0.815038 3.00144 0.968469 3.23228 1.04746 3.42764 1.1109 Not Fitted Points Thickness (Å) Quantity Adsorbed (cm³/g STP) 1.61806 0.0128345 1.58691 0.0265556 1.57886 0.0403348 1.58767 0.0539532 1.60731 0.0672834 1.63389 0.0800843 1.66219 0.0939413 1.68959 0.107652 1.71515 0.121115 1.73929 0.134309 1.76195 0.147192 1.78528 0.161107 1.80677 0.174593 1.82665 0.187617 1.84198 0.197877 1.8568 0.208045 1.87486 0.221161 1.88843 0.231138 1.90151 0.241013 1.91416 0.250804 1.92642 0.260495 1.93843 0.270076 1.95006 0.279572 1.96135 0.288977 1.9724 0.298282 1.98629 0.310444 1.99673 0.319524 2.00955 0.331054 2.02193 0.342374 2.03378 0.353266 2.04503 0.363721 2.05603 0.37401 2.06627 0.383648 2.07614 0.39297 2.08542 0.401807 2.09426 0.41027 2.10271 0.418325 2.11083 0.426094 2.11844 0.433379 2.1258 0.440358 2.13282 0.447036 2.13951 0.453383 2.14583 0.459376 2.15179 0.465021 2.15759 0.470459 2.16305 0.475578 2.16829 0.480438 2.17329 0.485057 2.17782 0.489288 2.18218 0.493332 2.18631 0.497098 2.19024 0.500665 2.194 0.504026 2.19762 0.507239 2.2045 0.513854 2.2113 0.52039 2.21803 0.526825 2.22466 0.533177 2.2312 0.539417 2.23773 0.545561 2.24413 0.55165 2.25046 0.557644 2.25672 0.563526 2.26296 0.569321 2.2691 0.575039 2.27518 0.580656 2.28122 0.586187 2.28882 0.59332 2.29578 0.59978 2.30214 0.605541 2.30798 0.610637 2.31375 0.615661 2.3195 0.620603 2.32518 0.625439 2.33081 0.630206 2.33639 0.634891 2.34191 0.639493 2.34737 0.643997 2.3528 0.648474 2.35817 0.652847 2.36348 0.657121 2.36875 0.661353 2.37402 0.665441 2.37927 0.66943 2.38443 0.673481 2.3896 0.677381 2.39469 0.681201 2.39974 0.684993 2.40473 0.688668 2.40968 0.692298 2.4146 0.695792 2.42062 0.700256 2.4255 0.703599 2.43037 0.706846 2.43519 0.710056 2.43994 0.713173 2.4447 0.716177 2.44942 0.719216 2.45408 0.722118 2.45875 0.724922 2.46335 0.727691 2.46794 0.730375 2.4725 0.733049 2.47701 0.735615 2.48147 0.738126 2.4859 0.740589 2.49033 0.743019 2.49474 0.745295 2.49909 0.747547 2.50341 0.749771 2.50772 0.751995 2.51204 0.754056 2.5163 0.756148 2.5205 0.758136 2.54261 0.771722 2.56351 0.785017 2.58429 0.795671 3.59925 1.16608 3.75751 1.21539 3.90282 1.26066 4.04211 1.30424 4.18036 1.34814 4.30817 1.38784 4.43833 1.42808 4.57187 1.46924 4.70046 1.51075 4.82486 1.55028 4.95525 1.59187 5.08585 1.63368 5.22479 1.67828 5.35228 1.71887 5.49591 1.76462 5.63027 1.8056 5.78153 1.85064 5.92171 1.89276 6.08399 1.93847 6.23967 1.98032 6.403 2.02493 6.57131 2.06905 6.75118 2.11503 6.93201 2.16104 7.12148 2.20832 7.32336 2.25841 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Adsorption Pore Distribution Report Faas Correction Halsey t = 3.54 [ -5 / ln(P/Po) ] ^ 0.333 Width Range: 17.000 Å to 3000.000 Å Adsorbate Property Factor: 9.53000 Å Density Conversion Factor: 0.0015468 Fraction of Pores Open at Both Ends: 0.00 Incremental Cumulative Cumulative Average Pore Pore Incremental Pore Width Volume Volume Pore Area Area Pore Width Range (Å) (Å) (cm³/g) (cm³/g) (m²/g) (m²/g) ------ 2048.1 - 725.2 867.2 0.003620 0.003620 0.167 0.167 725.2 - 430.7 505.7 0.001847 0.005467 0.146 0.313 430.7 - 303.9 345.3 0.001139 0.006606 0.132 0.445 303.9 - 234.3 259.8 0.000799 0.007404 0.123 0.568 234.3 - 190.3 207.5 0.000603 0.008007 0.116 0.684 190.3 - 159.9 172.3 0.000466 0.008473 0.108 0.792 159.9 - 138.1 147.3 0.000367 0.008839 0.100 0.892 138.1 - 121.2 128.5 0.000306 0.009145 0.095 0.987 121.2 - 107.9 113.7 0.000262 0.009408 0.092 1.079 107.9 - 97.1 101.9 0.000222 0.009630 0.087 1.166 97.1 - 88.2 92.2 0.000196 0.009825 0.085 1.251 88.2 - 80.6 84.0 0.000171 0.009996 0.081 1.333 80.6 - 74.2 77.1 0.000153 0.010149 0.079 1.412 74.2 - 68.6 71.2 0.000137 0.010286 0.077 1.489 68.6 - 63.7 66.0 0.000127 0.010413 0.077 1.566 63.7 - 59.5 61.4 0.000111 0.010523 0.072 1.638 59.5 - 55.6 57.4 0.000102 0.010625 0.071 1.709 55.6 - 52.2 53.8 0.000099 0.010725 0.074 1.783 52.2 - 49.1 50.5 0.000089 0.010813 0.070 1.853 49.1 - 46.3 47.6 0.000086 0.010899 0.072 1.925 46.3 - 43.7 44.9 0.000080 0.010979 0.071 1.996 43.7 - 41.4 42.5 0.000075 0.011054 0.071 2.067 41.4 - 39.2 40.2 0.000073 0.011127 0.073 2.139 39.2 - 37.2 38.1 0.000073 0.011200 0.077 2.216 37.2 - 35.3 36.2 0.000071 0.011271 0.078 2.294 35.3 - 33.5 34.4 0.000073 0.011343 0.084 2.379 33.5 - 31.9 32.7 0.000067 0.011410 0.082 2.460 31.9 - 30.3 31.0 0.000074 0.011484 0.096 2.556 30.3 - 28.9 29.5 0.000071 0.011555 0.096 2.651 28.9 - 27.4 28.1 0.000074 0.011629 0.105 2.756 27.4 - 26.2 26.8 0.000067 0.011696 0.101 2.857 26.2 - 24.9 25.5 0.000076 0.011772 0.120 2.977 24.9 - 23.8 24.3 0.000067 0.011839 0.110 3.087 23.8 - 22.6 23.2 0.000072 0.011911 0.125 3.212 22.6 - 21.5 22.0 0.000066 0.011978 0.120 3.332 21.5 - 20.4 20.9 0.000064 0.012042 0.122 3.454 20.4 - 19.5 19.9 0.000059 0.012101 0.119 3.573 19.5 - 18.5 18.9 0.000061 0.012162 0.130 3.703 18.5 - 17.4 17.9 0.000056 0.012218 0.124 3.827 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Adsorption dV/dw Pore Volume Halsey : Faas Correction 000-597 cook sample 6cs-3 Pore Width (Å) Pore Volume (cm³/g·Å) 867.216 2.73622e-006 505.666 6.27289e-006 345.305 8.98095e-006 259.847 1.14662e-005 207.523 1.36873e-005 172.347 1.53694e-005 147.35 1.68048e-005 128.47 1.80466e-005 113.72 1.97745e-005 101.911 2.05964e-005 92.2005 2.19032e-005 84.0332 2.24757e-005 77.1115 2.38007e-005 71.1866 2.47875e-005 65.979 2.56603e-005 61.4408 2.62289e-005 57.4238 2.64915e-005 53.7875 2.86296e-005 50.5377 2.87998e-005 47.5979 3.03872e-005 44.9055 3.09048e-005 42.4608 3.21921e-005 40.2286 3.41726e-005 38.1248 3.53697e-005 36.1678 3.77806e-005 34.3603 4.13326e-005 32.6765 4.10502e-005 31.0419 4.52776e-005 29.546 5.12666e-005 28.1306 5.12268e-005 26.7938 5.40718e-005 25.5168 5.89197e-005 24.3146 5.93632e-005 23.1527 6.07007e-005 22.0156 6.06822e-005 20.9399 6.03637e-005 19.9183 5.98714e-005 18.9252 6.16279e-005 17.922 5.52651e-005 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Adsorption dV/dw Pore Volume Halsey : Faas Correction 000-597 cook sample 6cs-3 Pore Width (Å) Pore Volume (cm³/g·Å) 867.216 2.73622e-006 505.666 6.27289e-006 345.305 8.98095e-006 259.847 1.14662e-005 207.523 1.36873e-005 172.347 1.53694e-005 147.35 1.68048e-005 128.47 1.80466e-005 113.72 1.97745e-005 101.911 2.05964e-005 92.2005 2.19032e-005 84.0332 2.24757e-005 77.1115 2.38007e-005 71.1866 2.47875e-005 65.979 2.56603e-005 61.4408 2.62289e-005 57.4238 2.64915e-005 53.7875 2.86296e-005 50.5377 2.87998e-005 47.5979 3.03872e-005 44.9055 3.09048e-005 42.4608 3.21921e-005 40.2286 3.41726e-005 38.1248 3.53697e-005 36.1678 3.77806e-005 34.3603 4.13326e-005 32.6765 4.10502e-005 31.0419 4.52776e-005 29.546 5.12666e-005 28.1306 5.12268e-005 26.7938 5.40718e-005 25.5168 5.89197e-005 24.3146 5.93632e-005 23.1527 6.07007e-005 22.0156 6.06822e-005 20.9399 6.03637e-005 19.9183 5.98714e-005 18.9252 6.16279e-005 17.922 5.52651e-005 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Adsorption dV/dlog(w) Pore Volume Halsey : Faas Correction 000-597 cook sample 6cs-3 Pore Width (Å) dV/dlog(w) Pore Volume (cm³/g·Å) 867.216 0.00802785 505.666 0.00816404 345.305 0.00752024 259.847 0.00706528 207.523 0.00666595 172.347 0.0061812 147.35 0.00575656 128.47 0.00537967 113.72 0.00520936 101.911 0.0048574 92.2005 0.00466971 84.0332 0.004365 77.1115 0.00423923 71.1866 0.00407425 65.979 0.00390835 61.4408 0.00371872 57.4238 0.00351001 53.7875 0.00355255 50.5377 0.00335707 47.5979 0.0033358 44.9055 0.00320039 42.4608 0.0031518 40.2286 0.00316957 38.1248 0.00310915 36.1678 0.00315023 34.3603 0.00327408 32.6765 0.00309216 31.0419 0.00324047 29.546 0.00349127 28.1306 0.00332215 26.7938 0.00333929 25.5168 0.00346593 24.3146 0.00332678 23.1527 0.00323995 22.0156 0.00307961 20.9399 0.0029139 19.9183 0.00274898 18.9252 0.00268892 17.922 0.00228387 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Adsorption Cumulative Pore Area Halsey : Faas Correction 000-597 cook sample 6cs-3 Pore Width (Å) Pore Area (m²/g) 725.178 0.166963 430.725 0.313073 303.944 0.44497 234.283 0.567925 190.26 0.684068 159.942 0.792214 138.129 0.891724 121.167 0.987034 107.909 1.07925 97.1262 1.16642 88.1985 1.25125 80.6038 1.3325 74.1926 1.41166 68.6466 1.4889 63.7104 1.56569 59.4858 1.63783 55.6411 1.70878 52.1764 1.78255 49.1024 1.85262 46.2762 1.92479 43.6964 1.99581 41.3648 2.06652 39.2174 2.13948 37.154 2.21605 35.2869 2.29407 33.5317 2.37853 31.9093 2.46005 30.269 2.55575 28.8928 2.65127 27.4491 2.75643 26.2017 2.85712 24.9037 2.97701 23.7816 3.08659 22.5902 3.21154 21.4995 3.33178 20.4383 3.45416 19.4509 3.57287 18.4557 3.70251 17.4488 3.8267 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Adsorption dA/dw Pore Area Halsey : Faas Correction 000-597 cook sample 6cs-3 Pore Width (Å) Pore Area (m²/g·Å) 867.216 0.000126207 505.666 0.000496208 345.305 0.00104035 259.847 0.00176507 207.523 0.00263823 172.347 0.00356707 147.35 0.00456189 128.47 0.00561893 113.72 0.0069555 101.911 0.00808407 92.2005 0.00950241 84.0332 0.0106985 77.1115 0.0123461 71.1866 0.0139282 65.979 0.0155567 61.4408 0.0170759 57.4238 0.0184533 53.7875 0.0212909 50.5377 0.0227947 47.5979 0.0255366 44.9055 0.0275287 42.4608 0.0303265 40.2286 0.0339784 38.1248 0.0371094 36.1678 0.0417836 34.3603 0.0481167 32.6765 0.0502504 31.0419 0.0583439 29.546 0.0694058 28.1306 0.0728414 26.7938 0.0807228 25.5168 0.0923622 24.3146 0.0976587 23.1527 0.10487 22.0156 0.110253 20.9399 0.115309 19.9183 0.120234 18.9252 0.130256 17.922 0.123346 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Adsorption dA/dlog(w) Pore Area Halsey : Faas Correction 000-597 cook sample 6cs-3 Pore Width (Å) dA/dlog(w) Pore Area (m²/g·Å) 867.216 0.370282 505.666 0.645805 345.305 0.871142 259.847 1.08761 207.523 1.28486 172.347 1.43459 147.35 1.5627 128.47 1.675 113.72 1.83235 101.911 1.90653 92.2005 2.02589 84.0332 2.07775 77.1115 2.19901 71.1866 2.28934 65.979 2.36945 61.4408 2.42101 57.4238 2.44498 53.7875 2.64192 50.5377 2.65708 47.5979 2.80332 44.9055 2.85077 42.4608 2.96914 40.2286 3.15156 38.1248 3.26208 36.1678 3.48401 34.3603 3.81147 32.6765 3.78517 31.0419 4.1756 29.546 4.72656 28.1306 4.7239 26.7938 4.98517 25.5168 5.43317 24.3146 5.47291 23.1527 5.59753 22.0156 5.59532 20.9399 5.56622 19.9183 5.52053 18.9252 5.68326 17.922 5.09735 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Desorption Pore Distribution Report Faas Correction Halsey t = 3.54 [ -5 / ln(P/Po) ] ^ 0.333 Width Range: 17.000 Å to 3000.000 Å Adsorbate Property Factor: 9.53000 Å Density Conversion Factor: 0.0015468 Fraction of Pores Open at Both Ends: 0.00 Incremental Cumulative Cumulative Average Pore Pore Incremental Pore Width Volume Volume Pore Area Area Pore Width Range (Å) (Å) (cm³/g) (cm³/g) (m²/g) (m²/g) ------ 2050.3 - 993.3 1189.6 0.000656 0.000656 0.022 0.022 993.3 - 599.0 701.9 0.001587 0.002243 0.090 0.113 599.0 - 382.3 443.4 0.001743 0.003986 0.157 0.270 382.3 - 314.2 341.3 0.000797 0.004783 0.093 0.363 314.2 - 239.1 266.2 0.001034 0.005817 0.155 0.518 239.1 - 195.1 212.4 0.000749 0.006566 0.141 0.659 195.1 - 163.4 176.3 0.000619 0.007185 0.141 0.800 163.4 - 141.1 150.5 0.000506 0.007691 0.135 0.935 141.1 - 124.0 131.4 0.000439 0.008131 0.134 1.068 124.0 - 110.4 116.4 0.000383 0.008513 0.132 1.200 110.4 - 99.5 104.4 0.000333 0.008846 0.128 1.327 99.5 - 90.6 94.6 0.000301 0.009147 0.127 1.455 90.6 - 83.0 86.4 0.000263 0.009411 0.122 1.577 83.0 - 76.5 79.5 0.000230 0.009640 0.116 1.692 76.5 - 71.0 73.5 0.000205 0.009845 0.111 1.804 71.0 - 66.1 68.3 0.000185 0.010030 0.109 1.912 66.1 - 61.8 63.8 0.000163 0.010193 0.102 2.014 61.8 - 57.9 59.7 0.000150 0.010343 0.101 2.115 57.9 - 54.5 56.1 0.000135 0.010478 0.096 2.211 54.5 - 51.4 52.8 0.000123 0.010601 0.093 2.304 51.4 - 48.5 49.9 0.000116 0.010718 0.093 2.398 48.5 - 46.0 47.2 0.000108 0.010825 0.091 2.489 46.0 - 43.6 44.7 0.000105 0.010931 0.094 2.583 43.6 - 41.4 42.4 0.000099 0.011029 0.093 2.676 41.4 - 39.4 40.4 0.000103 0.011133 0.103 2.779 39.4 - 37.6 38.4 0.000144 0.011277 0.150 2.929 37.6 - 35.9 36.7 0.000406 0.011683 0.442 3.371 35.9 - 34.1 34.9 0.000490 0.012173 0.561 3.933 34.1 - 32.5 33.2 0.000235 0.012407 0.283 4.215 32.5 - 31.1 31.8 0.000120 0.012527 0.151 4.366 31.1 - 29.7 30.4 0.000088 0.012616 0.116 4.483 29.7 - 28.4 29.0 0.000070 0.012686 0.097 4.579 28.4 - 27.2 27.7 0.000058 0.012744 0.083 4.663 27.2 - 26.0 26.5 0.000054 0.012798 0.081 4.744 26.0 - 24.8 25.4 0.000051 0.012849 0.080 4.824 24.8 - 23.7 24.3 0.000048 0.012897 0.079 4.903 23.7 - 22.7 23.2 0.000045 0.012942 0.078 4.981 22.7 - 21.7 22.1 0.000042 0.012984 0.076 5.057 21.7 - 20.7 21.1 0.000040 0.013024 0.076 5.133 20.7 - 19.7 20.2 0.000037 0.013061 0.073 5.206 19.7 - 18.7 19.2 0.000034 0.013094 0.070 5.276 18.7 - 17.8 18.2 0.000032 0.013126 0.070 5.346 17.8 - 16.9 17.3 0.000035 0.013161 0.081 5.427 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Desorption Cumulative Pore Volume Halsey : Faas Correction BJH Desorption Cumulative Pore Volume Pore Width (Å) Pore Volume (cm³/g) 993.321 0.000655915 598.993 0.00224334 382.275 0.00398591 314.215 0.00478289 239.146 0.00581683 195.107 0.00656561 163.38 0.00718485 141.093 0.00769125 124.006 0.00813063 110.427 0.0085132 99.5211 0.008846 90.5941 0.00914746 82.9814 0.00941079 76.5416 0.00964048 70.9767 0.00984501 66.0698 0.0100304 61.7594 0.0101931 57.9261 0.0103431 54.4813 0.0104782 51.3704 0.0106013 48.5317 0.0107176 45.9753 0.0108254 43.5898 0.0109308 41.4175 0.0110294 39.4074 0.0111328 37.5671 0.0112771 35.8618 0.0116827 34.0831 0.0121727 32.4906 0.0124074 31.1104 0.0125275 29.7301 0.0126157 28.3987 0.012686 27.1533 0.0127437 25.9745 0.0127977 24.8367 0.0128486 23.7377 0.0128967 22.688 0.0129419 21.6641 0.0129839 20.6723 0.013024 19.7037 0.0130607 18.7421 0.0130944 17.8031 0.0131263 16.866 0.0131612 BJH Desorption dV/dw Pore Volume Pore Width (Å) Pore Volume (cm³/g·Å) 1189.61 6.20528e-007 701.88 4.02565e-006 443.432 8.04074e-006 341.349 1.17099e-005 266.155 1.37731e-005 212.431 1.70027e-005 176.262 1.95179e-005 150.488 2.27223e-005 131.361 2.57139e-005 116.362 2.81732e-005 104.354 3.05164e-005 94.5967 3.37694e-005 86.4188 3.45903e-005 79.4728 3.56673e-005 73.5249 3.67541e-005 68.3264 3.77819e-005 63.751 3.77405e-005 59.704 3.91455e-005 56.0839 3.92153e-005 52.8218 3.95758e-005 49.8589 4.09629e-005 47.1742 4.21687e-005 44.7094 4.41816e-005 42.4396 4.5371e-005 40.3546 5.14587e-005 38.4362 7.83983e-005 36.6684 0.000237862 34.9196 0.000275434 33.2422 0.000147433 31.7653 8.69897e-005 30.3833 6.39095e-005 29.0284 5.28096e-005 27.7429 4.631e-005 26.5328 4.58197e-005 25.3753 4.4729e-005 24.2575 4.37379e-005 23.1845 4.30735e-005 22.1477 4.10118e-005 21.1403 4.04506e-005 20.16 3.7946e-005 19.1939 3.49632e-005 18.2435 3.39763e-005 17.3039 3.72756e-005 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Desorption dV/dw Pore Volume Halsey : Faas Correction 000-597 cook sample 6cs-3 Pore Width (Å) Pore Volume (cm³/g·Å) 1189.61 6.20528e-007 701.88 4.02565e-006 443.432 8.04074e-006 341.349 1.17099e-005 266.155 1.37731e-005 212.431 1.70027e-005 176.262 1.95179e-005 150.488 2.27223e-005 131.361 2.57139e-005 116.362 2.81732e-005 104.354 3.05164e-005 94.5967 3.37694e-005 86.4188 3.45903e-005 79.4728 3.56673e-005 73.5249 3.67541e-005 68.3264 3.77819e-005 63.751 3.77405e-005 59.704 3.91455e-005 56.0839 3.92153e-005 52.8218 3.95758e-005 49.8589 4.09629e-005 47.1742 4.21687e-005 44.7094 4.41816e-005 42.4396 4.5371e-005 40.3546 5.14587e-005 38.4362 7.83983e-005 36.6684 0.000237862 34.9196 0.000275434 33.2422 0.000147433 31.7653 8.69897e-005 30.3833 6.39095e-005 29.0284 5.28096e-005 27.7429 4.631e-005 26.5328 4.58197e-005 25.3753 4.4729e-005 24.2575 4.37379e-005 23.1845 4.30735e-005 22.1477 4.10118e-005 21.1403 4.04506e-005 20.16 3.7946e-005 19.1939 3.49632e-005 18.2435 3.39763e-005 17.3039 3.72756e-005 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Desorption dV/dlog(w) Pore Volume Halsey : Faas Correction 000-597 cook sample 6cs-3 Pore Width (Å) dV/dlog(w) Pore Volume (cm³/g·Å) 1189.61 0.002084 701.88 0.00722649 443.432 0.00893418 341.349 0.00935974 266.155 0.00872047 212.431 0.0084713 176.262 0.0080344 150.488 0.00795076 131.361 0.00783719 116.362 0.00759545 104.354 0.00736953 94.5967 0.00738596 86.4188 0.00690795 79.4728 0.00654701 73.5249 0.00623923 68.3264 0.0059587 63.751 0.00555212 59.704 0.00539213 56.0839 0.0050734 52.8218 0.00482156 49.8589 0.00471014 47.1742 0.00458705 44.7094 0.00455473 42.4396 0.00443942 40.3546 0.00478741 38.4362 0.00694635 36.6684 0.0201048 34.9196 0.0221751 33.2422 0.0112979 31.7653 0.00636868 30.3833 0.00447578 29.0284 0.00353357 27.7429 0.00296134 26.5328 0.00280213 25.3753 0.00261615 24.2575 0.00244556 23.1845 0.00230187 22.1477 0.00209378 21.1403 0.00197127 20.16 0.00176357 19.1939 0.00154723 18.2435 0.00142921 17.3039 0.00148746 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Desorption Cumulative Pore Area Halsey : Faas Correction 000-597 cook sample 6cs-3 Pore Width (Å) Pore Area (m²/g) 993.321 0.0220547 598.993 0.112522 382.275 0.269711 314.215 0.363103 239.146 0.518492 195.107 0.659485 163.38 0.800012 141.093 0.934614 124.006 1.06841 110.427 1.19992 99.5211 1.32748 90.5941 1.45496 82.9814 1.57684 76.5416 1.69245 70.9767 1.80372 66.0698 1.91225 61.7594 2.01432 57.9261 2.11486 54.4813 2.2112 51.3704 2.30443 48.5317 2.39772 45.9753 2.48913 43.5898 2.58342 41.4175 2.67632 39.4074 2.77885 37.5671 2.92899 35.8618 3.37147 34.0831 3.93268 32.4906 4.21519 31.1104 4.36639 29.7301 4.48252 28.3987 4.5794 27.1533 4.66256 25.9745 4.74399 24.8367 4.82421 23.7377 4.90347 22.688 4.98148 21.6641 5.05732 20.6723 5.13323 19.7037 5.20615 18.7421 5.27622 17.8031 5.34617 16.866 5.42692 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Desorption dA/dw Pore Area Halsey : Faas Correction 000-597 cook sample 6cs-3 Pore Width (Å) Pore Area (m²/g·Å) 1189.61 2.08649e-005 701.88 0.000229421 443.432 0.000725319 341.349 0.00137218 266.155 0.00206994 212.431 0.00320155 176.262 0.00442929 150.488 0.00603962 131.361 0.00783003 116.362 0.0096847 104.354 0.0116972 94.5967 0.0142793 86.4188 0.0160105 79.4728 0.0179519 73.5249 0.0199954 68.3264 0.0221185 63.751 0.0236799 59.704 0.0262264 56.0839 0.027969 52.8218 0.0299693 49.8589 0.0328631 47.1742 0.0357557 44.7094 0.0395278 42.4396 0.0427629 40.3546 0.0510066 38.4362 0.081588 36.6684 0.259474 34.9196 0.315506 33.2422 0.177404 31.7653 0.109541 30.3833 0.0841377 29.0284 0.0727697 27.7429 0.0667703 26.5328 0.0690763 25.3753 0.070508 24.2575 0.0721226 23.1845 0.0743144 22.1477 0.0740695 21.1403 0.0765376 20.16 0.0752896 19.1939 0.0728631 18.2435 0.0744953 17.3039 0.0861671 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm BJH Desorption dA/dlog(w) Pore Area Halsey : Faas Correction 000-597 cook sample 6cs-3 Pore Width (Å) dA/dlog(w) Pore Area (m²/g·Å) 1189.61 0.0700733 701.88 0.411836 443.432 0.805912 341.349 1.09679 266.155 1.31059 212.431 1.59511 176.262 1.82328 150.488 2.11333 131.361 2.38647 116.362 2.61098 104.354 2.82481 94.5967 3.12314 86.4188 3.19743 79.4728 3.29522 73.5249 3.39435 68.3264 3.48837 63.751 3.48363 59.704 3.61258 56.0839 3.61844 52.8218 3.6512 49.8589 3.77878 47.1742 3.88946 44.7094 4.07497 42.4396 4.18422 40.3546 4.74534 38.4362 7.22897 36.6684 21.9315 34.9196 25.4013 33.2422 13.5947 31.7653 8.01967 30.3833 5.89242 29.0284 4.86913 27.7429 4.26968 26.5328 4.2244 25.3753 4.12393 24.2575 4.03265 23.1845 3.9714 22.1477 3.78148 21.1403 3.72988 20.16 3.49914 19.1939 3.22442 18.2435 3.13364 17.3039 3.43845 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Horvath-Kawazoe Report Slit Pore Geometry (Original H-K) Maximum Pore Volume: 0.001261 cm³/g at Relative Pressure: 0.010034034 Median Pore Width: 7.344 Å Relative Pressure Range: 4.903e-06 to 1.003e-02 Diameter of Adsorptive Molecule: 3.000 Å Diameter of Adsorptive at Zero Interaction Energy: 2.574 Å Diameter of Sample Atom: 3.040 Å Diameter of Sample Atom at Zero Interaction Energy: 2.609 Å Interaction Parameter: 3.49e-43 erg·cm^4 Density Conversion Factor: 0.0015468 Quantity Cumulative Differential Absolute Relative Adsorbed Pore Pore Pore Pressure Pressure (cm³/g Width Volume Volume (mmHg) (P/Po) STP) (Å) (cm³/g) (cm³/g·Å) ------ 0.00363 0.000004903 0.01283 5.180 0.0000 0.0000 0.00223 0.000003011 0.02656 5.048 0.0000 -0.0002 0.00196 0.000002641 0.04033 5.014 0.0001 -0.0006 0.00226 0.000003048 0.05395 5.051 0.0001 0.0006 0.00308 0.000004157 0.06728 5.135 0.0001 0.0002 0.00461 0.000006216 0.08008 5.247 0.0001 0.0002 0.00693 0.000009341 0.09394 5.368 0.0001 0.0002 0.01008 0.000013594 0.10765 5.486 0.0002 0.0002 0.01407 0.000018982 0.12111 5.597 0.0002 0.0002 0.01903 0.000025669 0.13431 5.703 0.0002 0.0002 0.02499 0.000033697 0.14719 5.802 0.0002 0.0002 0.03271 0.000044118 0.16111 5.906 0.0002 0.0002 0.04154 0.000056024 0.17459 6.002 0.0003 0.0002 0.05144 0.000069370 0.18762 6.092 0.0003 0.0002 0.06036 0.000081408 0.19788 6.161 0.0003 0.0002 0.07020 0.000094676 0.20804 6.229 0.0003 0.0002 0.08397 0.000113249 0.22116 6.311 0.0003 0.0002 0.09574 0.000129123 0.23114 6.374 0.0004 0.0002 0.10837 0.000146155 0.24101 6.434 0.0004 0.0003 0.12187 0.000164359 0.25080 6.493 0.0004 0.0003 0.13625 0.000183754 0.26049 6.550 0.0004 0.0003 0.15167 0.000204548 0.27008 6.605 0.0004 0.0003 0.16795 0.000226497 0.27957 6.660 0.0004 0.0003 0.18510 0.000249630 0.28898 6.714 0.0004 0.0003 0.20326 0.000274116 0.29828 6.766 0.0005 0.0003 0.22812 0.000307637 0.31044 6.832 0.0005 0.0003 0.24841 0.000335002 0.31952 6.883 0.0005 0.0003 0.27528 0.000371234 0.33105 6.944 0.0005 0.0003 0.30345 0.000409217 0.34237 7.003 0.0005 0.0003 0.33254 0.000448445 0.35327 7.061 0.0005 0.0003 0.36221 0.000488458 0.36372 7.116 0.0006 0.0003 0.39325 0.000530314 0.37401 7.170 0.0006 0.0003 0.42402 0.000571812 0.38365 7.220 0.0006 0.0003 0.45547 0.000614215 0.39297 7.268 0.0006 0.0003 0.48672 0.000656358 0.40181 7.314 0.0006 0.0003 0.51809 0.000698660 0.41027 7.358 0.0006 0.0003 0.54953 0.000741051 0.41832 7.399 0.0006 0.0003 0.58114 0.000783677 0.42609 7.440 0.0007 0.0003 0.61205 0.000825368 0.43338 7.478 0.0007 0.0003 0.64321 0.000867380 0.44036 7.515 0.0007 0.0003 0.67404 0.000908944 0.44704 7.550 0.0007 0.0003 0.70450 0.000950026 0.45338 7.584 0.0007 0.0003 0.73431 0.000990220 0.45938 7.616 0.0007 0.0003 0.76329 0.001029298 0.46502 7.646 0.0007 0.0003 0.79231 0.001068424 0.47046 7.675 0.0007 0.0003 0.82045 0.001106367 0.47558 7.703 0.0007 0.0003 0.84820 0.001143778 0.48044 7.730 0.0007 0.0003 0.87536 0.001180401 0.48506 7.755 0.0008 0.0003 0.90050 0.001214305 0.48929 7.778 0.0008 0.0003 0.92525 0.001247664 0.49333 7.800 0.0008 0.0003 0.94917 0.001279922 0.49710 7.821 0.0008 0.0003 0.97240 0.001311247 0.50066 7.842 0.0008 0.0003 0.99502 0.001341735 0.50403 7.862 0.0008 0.0003 1.01722 0.001371674 0.50724 7.880 0.0008 0.0003 1.06038 0.001429868 0.51385 7.915 0.0008 0.0003 1.10442 0.001489244 0.52039 7.951 0.0008 0.0003 1.14942 0.001549919 0.52682 7.985 0.0008 0.0003 1.19508 0.001611478 0.53318 8.021 0.0008 0.0003 1.24154 0.001674122 0.53942 8.054 0.0008 0.0003 1.28925 0.001738447 0.54556 8.087 0.0008 0.0003 1.33735 0.001803295 0.55165 8.122 0.0009 0.0003 1.38630 0.001869299 0.55764 8.155 0.0009 0.0003 1.43604 0.001936359 0.56353 8.188 0.0009 0.0003 1.48691 0.002004951 0.56932 8.221 0.0009 0.0003 1.53836 0.002074318 0.57504 8.253 0.0009 0.0003 1.59056 0.002144685 0.58066 8.286 0.0009 0.0003 1.64380 0.002216467 0.58619 8.317 0.0009 0.0003 1.71269 0.002309351 0.59332 8.358 0.0009 0.0003 1.77766 0.002396952 0.59978 8.395 0.0009 0.0003 1.83859 0.002479098 0.60554 8.429 0.0009 0.0003 1.89595 0.002556425 0.61064 8.460 0.0009 0.0003 1.95402 0.002634718 0.61566 8.491 0.0010 0.0003 2.01307 0.002714321 0.62060 8.522 0.0010 0.0002 2.07276 0.002794796 0.62544 8.553 0.0010 0.0002 2.13321 0.002876291 0.63021 8.583 0.0010 0.0002 2.19442 0.002958814 0.63489 8.614 0.0010 0.0002 2.25625 0.003042173 0.63949 8.644 0.0010 0.0002 2.31878 0.003126472 0.64400 8.673 0.0010 0.0002 2.38205 0.003211760 0.64847 8.702 0.0010 0.0002 2.44597 0.003297938 0.65285 8.732 0.0010 0.0002 2.51045 0.003384867 0.65712 8.761 0.0010 0.0002 2.57564 0.003472748 0.66135 8.790 0.0010 0.0002 2.64203 0.003562239 0.66544 8.819 0.0010 0.0002 2.70950 0.003653193 0.66943 8.848 0.0010 0.0002 2.77702 0.003744220 0.67348 8.876 0.0010 0.0002 2.84582 0.003836968 0.67738 8.905 0.0010 0.0002 2.91479 0.003929950 0.68120 8.933 0.0011 0.0002 2.98451 0.004023930 0.68499 8.961 0.0011 0.0002 3.05458 0.004118395 0.68867 8.988 0.0011 0.0002 3.12526 0.004213678 0.69230 9.016 0.0011 0.0002 3.19668 0.004309948 0.69579 9.044 0.0011 0.0002 3.28559 0.004429812 0.70026 9.077 0.0011 0.0002 3.35906 0.004528843 0.70360 9.104 0.0011 0.0002 3.43345 0.004629121 0.70685 9.131 0.0011 0.0002 3.50832 0.004730040 0.71006 9.159 0.0011 0.0002 3.58321 0.004830993 0.71317 9.183 0.0011 0.0002 3.65953 0.004933874 0.71618 9.212 0.0011 0.0002 3.73629 0.005037339 0.71922 9.239 0.0011 0.0002 3.81321 0.005141032 0.72212 9.266 0.0011 0.0002 3.89142 0.005246457 0.72492 9.290 0.0011 0.0002 3.96956 0.005351773 0.72769 9.317 0.0011 0.0002 4.04863 0.005458358 0.73038 9.342 0.0011 0.0002 4.12841 0.005565897 0.73305 9.369 0.0011 0.0002 4.20823 0.005673494 0.73561 9.394 0.0011 0.0002 4.28848 0.005781658 0.73813 9.419 0.0011 0.0002 4.36910 0.005890321 0.74059 9.446 0.0011 0.0001 4.45074 0.006000369 0.74302 9.471 0.0011 0.0002 4.53323 0.006111549 0.74529 9.496 0.0012 0.0001 4.61564 0.006222637 0.74755 9.521 0.0012 0.0001 4.69841 0.006334192 0.74977 9.547 0.0012 0.0001 4.78212 0.006447032 0.75200 9.572 0.0012 0.0001 4.86707 0.006561523 0.75406 9.597 0.0012 0.0001 4.95192 0.006675892 0.75615 9.621 0.0012 0.0001 5.03646 0.006789834 0.75814 9.645 0.0012 0.0001 5.49902 0.007413145 0.77172 9.772 0.0012 0.0002 5.96259 0.008037847 0.78502 9.896 0.0012 0.0002 6.44969 0.008694188 0.79567 10.019 0.0012 0.0001 6.94257 0.009358324 0.80567 10.137 0.0012 0.0001 7.44392 0.010034034 0.81504 10.254 0.0013 0.0001 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Horvath-Kawazoe Cumulative Pore Volume Plot Slit Pore Geometry (Original H-K) 000-597 cook sample 6cs-3 Pore Width (Å) Pore Volume (cm³/g) 5.18014 1.98524e-005 5.04812 4.10762e-005 5.01423 6.23899e-005 5.05128 8.34549e-005 5.13462 0.000104074 5.24743 0.000123874 5.36843 0.000145308 5.48615 0.000166515 5.59707 0.00018734 5.70262 0.000207749 5.80237 0.000227677 5.90583 0.0002492 6.00244 0.00027006 6.09196 0.000290206 6.16136 0.000306077 6.22853 0.000321804 6.31102 0.000342092 6.37368 0.000357524 6.43392 0.000372799 6.49266 0.000387944 6.54986 0.000402934 6.60548 0.000417753 6.66046 0.000432442 6.71381 0.000446989 6.76648 0.000461382 6.83219 0.000480195 6.88253 0.00049424 6.94405 0.000512075 7.00296 0.000529585 7.06121 0.000546431 7.11575 0.000562604 7.16958 0.000578518 7.21961 0.000593427 7.26783 0.000607846 7.31421 0.000621515 7.3577 0.000634606 7.39929 0.000647064 7.44 0.000659083 7.47773 0.00067035 7.51454 0.000681146 7.55043 0.000691475 7.58432 0.000701293 7.61619 0.000710563 7.64603 0.000719295 7.67488 0.000727706 7.70274 0.000735624 7.7296 0.000743141 7.75544 0.000750285 7.77811 0.000756831 7.79975 0.000763086 7.82143 0.000768911 7.84207 0.000774428 7.86165 0.000779627 7.88019 0.000784598 7.91513 0.00079483 7.95128 0.000804939 7.98536 0.000814892 8.02064 0.000824718 8.05382 0.000834371 8.0871 0.000843873 8.1216 0.000853293 8.15508 0.000862563 8.18755 0.000871663 8.22123 0.000880626 8.25276 0.00088947 8.28551 0.000898159 8.31722 0.000906714 8.35811 0.000917748 8.39458 0.00092774 8.42888 0.000936651 8.45985 0.000944533 8.4909 0.000952305 8.52203 0.000959949 8.55325 0.00096743 8.58339 0.000974803 8.61361 0.00098205 8.64391 0.000989168 8.67312 0.000996135 8.70241 0.00100306 8.73176 0.00100982 8.76119 0.00101643 8.78951 0.00102298 8.81909 0.0010293 8.84755 0.00103547 8.87608 0.00104174 8.90468 0.00104777 8.93335 0.00105368 8.96088 0.00105955 8.98849 0.00106523 9.01615 0.00107085 9.04388 0.00107625 9.07651 0.00108316 9.10438 0.00108833 9.13109 0.00109335 9.15909 0.00109831 9.18349 0.00110314 9.2116 0.00110778 9.23855 0.00111248 9.26557 0.00111697 9.29018 0.00112131 9.3173 0.00112559 9.34202 0.00112974 9.36926 0.00113388 9.39408 0.00113785 9.41894 0.00114173 9.44635 0.00114554 9.47133 0.0011493 9.49635 0.00115282 9.52142 0.00115631 9.54655 0.00115975 9.57172 0.00116319 9.59694 0.00116637 9.62095 0.00116961 9.64501 0.00117268 9.77186 0.0011937 9.89613 0.00121426 10.019 0.00123074 10.1366 0.00124622 10.2538 0.0012607 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:00PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Horvath-Kawazoe Differential Pore Volume Plot Slit Pore Geometry (Original H-K) 000-597 cook sample 6cs-3 Pore Width (Å) dV/dw (cm³/g·Å) 5.18014 3.83241e-006 5.04812 -0.000160768 5.01423 -0.000628924 5.05128 0.000568562 5.13462 0.00024741 5.24743 0.00017552 5.36843 0.000177146 5.48615 0.000180151 5.59707 0.000187736 5.70262 0.000193371 5.80237 0.000199763 5.90583 0.000208046 6.00244 0.000215912 6.09196 0.000225036 6.16136 0.000228677 6.22853 0.000234143 6.31102 0.00024594 6.37368 0.000246317 6.43392 0.000253536 6.49266 0.00025785 6.54986 0.000262068 6.60548 0.000266435 6.66046 0.000267184 6.71381 0.000272657 6.76648 0.000273262 6.83219 0.000286328 6.88253 0.00027896 6.94405 0.000289906 7.00296 0.000297245 7.06121 0.000289219 7.11575 0.000296495 7.16958 0.000295658 7.21961 0.000298009 7.26783 0.000299033 7.31421 0.000294679 7.3577 0.000301039 7.39929 0.000299541 7.44 0.000295192 7.47773 0.000298659 7.51454 0.000293267 7.55043 0.000287822 7.58432 0.000289712 7.61619 0.000290854 7.64603 0.000292644 7.67488 0.000291516 7.70274 0.000284235 7.7296 0.000279885 7.75544 0.000276409 7.77811 0.000288731 7.79975 0.0002891 7.82143 0.000268674 7.84207 0.000267357 7.86165 0.000265404 7.88019 0.000268221 7.91513 0.000292812 7.95128 0.000279635 7.98536 0.000292103 8.02064 0.000278501 8.05382 0.000290905 8.0871 0.000285522 8.1216 0.000273065 8.15508 0.000276865 8.18755 0.000280278 8.22123 0.000266096 8.25276 0.000280498 8.28551 0.00026531 8.31722 0.000269776 8.35811 0.00026987 8.39458 0.000273954 8.42888 0.000259765 8.45985 0.000254564 8.4909 0.000250298 8.52203 0.000245531 8.55325 0.000239618 8.58339 0.000244608 8.61361 0.000239809 8.64391 0.000234933 8.67312 0.000238498 8.70241 0.000236507 8.73176 0.000230405 8.76119 0.000224608 8.78951 0.000231146 8.81909 0.000213813 8.84755 0.000216778 8.87608 0.000219633 8.90468 0.000210943 8.93335 0.000206098 8.96088 0.000213015 8.98849 0.000205934 9.01615 0.000202937 9.04388 0.000194902 9.07651 0.000211648 9.10438 0.000185588 9.13109 0.000187941 9.15909 0.000177361 9.18349 0.00019766 9.2116 0.000165246 9.23855 0.000174436 9.26557 0.00016616 9.29018 0.000176229 9.3173 0.000157906 9.34202 0.000167975 9.36926 0.000151854 9.39408 0.000159891 9.41894 0.000156216 9.44635 0.00013897 9.47133 0.000150484 9.49635 0.000140709 9.52142 0.000138951 9.54655 0.000136898 9.57172 0.000136715 9.59694 0.000126381 9.62095 0.000134718 9.64501 0.000127861 9.77186 0.000165666 9.89613 0.00016548 10.019 0.000134098 10.1366 0.000131639 10.2538 0.000123508 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:01PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Porosity Distribution by Original Density Functional Theory Model: N2 @ 77K on Carbon, Slit Pores Method: Non-negative Regularization; No Smoothing Standard Deviation of Fit: 0.02968, cm³/g STP Volume in Pores < 5.00 Å : 0.00005 cm³/g Total Volume in Pores <= 1366.77 Å : 0.00817 cm³/g Area in Pores > 1366.77 Å : 1.594 m²/g Total Area in Pores >= 5.00 Å : 3.193 m²/g Pore Size Table Cumulative Incremental Cumulative Pore Width Volume Volume Area Incremental (Å) (cm³/g) (cm³/g) (m²/g) Area (m²/g) ----- 5.00 0.00000 0.00000 0.000 0.000 5.36 0.00000 0.00000 0.000 0.000 5.90 0.00000 0.00000 0.000 0.000 6.43 0.00000 0.00000 0.000 0.000 6.79 0.00000 0.00000 0.000 0.000 7.33 0.00000 0.00000 0.000 0.000 8.04 0.00000 0.00000 0.000 0.000 8.58 0.00000 0.00000 0.000 0.000 9.29 0.00000 0.00000 0.000 0.000 10.01 0.00000 0.00000 0.000 0.000 10.90 0.00000 0.00000 0.000 0.000 11.79 0.00000 0.00000 0.000 0.000 12.69 0.00021 0.00021 0.332 0.332 13.58 0.00038 0.00017 0.576 0.243 14.83 0.00044 0.00007 0.665 0.090 15.91 0.00044 0.00000 0.665 0.000 17.16 0.00044 0.00000 0.665 0.000 18.59 0.00044 0.00000 0.665 0.000 20.02 0.00044 0.00000 0.665 0.000 21.62 0.00044 0.00000 0.665 0.000 23.41 0.00044 0.00000 0.665 0.000 25.20 0.00044 0.00000 0.665 0.000 27.34 0.00047 0.00003 0.685 0.020 29.49 0.00054 0.00007 0.735 0.050 31.81 0.00062 0.00008 0.784 0.048 34.31 0.00069 0.00007 0.825 0.041 36.99 0.00073 0.00004 0.846 0.022 40.03 0.00077 0.00004 0.868 0.022 43.25 0.00083 0.00005 0.893 0.025 46.64 0.00089 0.00007 0.921 0.029 50.40 0.00096 0.00007 0.949 0.028 54.33 0.00104 0.00007 0.977 0.028 58.80 0.00111 0.00007 1.001 0.024 63.44 0.00118 0.00007 1.023 0.022 68.45 0.00127 0.00009 1.048 0.025 73.99 0.00135 0.00008 1.071 0.023 79.88 0.00145 0.00010 1.095 0.024 86.32 0.00159 0.00014 1.127 0.032 93.11 0.00173 0.00015 1.159 0.032 100.61 0.00186 0.00013 1.184 0.025 108.66 0.00199 0.00013 1.208 0.023 117.23 0.00212 0.00013 1.230 0.022 126.53 0.00226 0.00014 1.253 0.023 136.71 0.00242 0.00016 1.276 0.023 147.61 0.00260 0.00017 1.300 0.024 159.41 0.00278 0.00018 1.322 0.023 172.10 0.00297 0.00019 1.345 0.022 185.86 0.00316 0.00019 1.365 0.020 200.69 0.00335 0.00020 1.384 0.020 216.60 0.00356 0.00020 1.403 0.019 233.93 0.00375 0.00020 1.420 0.017 252.52 0.00398 0.00022 1.438 0.018 272.71 0.00421 0.00024 1.455 0.017 294.51 0.00438 0.00017 1.467 0.011 317.92 0.00453 0.00015 1.476 0.009 343.30 0.00467 0.00015 1.484 0.008 370.64 0.00481 0.00013 1.491 0.007 400.31 0.00499 0.00018 1.501 0.009 432.30 0.00518 0.00019 1.509 0.009 466.79 0.00542 0.00024 1.520 0.010 503.96 0.00581 0.00039 1.535 0.015 544.17 0.00621 0.00040 1.550 0.015 587.60 0.00648 0.00027 1.559 0.009 634.42 0.00672 0.00024 1.567 0.008 684.99 0.00701 0.00029 1.575 0.008 739.68 0.00721 0.00020 1.580 0.005 798.65 0.00738 0.00017 1.585 0.004 862.45 0.00758 0.00020 1.589 0.005 931.26 0.00774 0.00016 1.593 0.003 1005.60 0.00784 0.00010 1.595 0.002 1085.66 0.00793 0.00009 1.596 0.002 1172.33 0.00803 0.00010 1.598 0.002 1265.80 0.00809 0.00006 1.599 0.001 1366.77 0.00812 0.00003 1.600 0.000 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:01PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Porosity Distribution by Original Density Functional Theory Model: N2 @ 77K on Carbon, Slit Pores Method: Non-negative Regularization; No Smoothing Standard Deviation of Fit: 0.02968, cm³/g STP Isotherm Table Fitted Experimental Quantity Absolute Quantity Adsorbed Residual Relative Adsorbed (cm³/g (cm³/g Relative Pressure (cm³/g STP) STP) STP) Residual ----- 0.000005075 0.0256 0.0385 -0.0130 -0.506694 0.000008995 0.0928 0.0434 0.0494 0.532701 0.000015520 0.1128 0.0512 0.0616 0.545807 0.000026102 0.1351 0.0643 0.0708 0.524079 0.000042841 0.1595 0.0862 0.0734 0.459798 0.000068697 0.1870 0.1234 0.0636 0.339915 0.000107744 0.2174 0.1849 0.0326 0.149759 0.000165451 0.2514 0.2684 -0.0170 -0.067622 0.000249000 0.2887 0.3507 -0.0619 -0.214517 0.000367617 0.3299 0.4175 -0.0876 -0.265558 0.000532902 0.3746 0.4703 -0.0957 -0.255340 0.000759152 0.4217 0.5128 -0.0912 -0.216235 0.001063641 0.4698 0.5482 -0.0784 -0.166866 0.001466847 0.5180 0.5784 -0.0604 -0.116692 0.001992604 0.5683 0.6048 -0.0366 -0.064332 0.002668156 0.6178 0.6287 -0.0109 -0.017653 0.003524104 0.6637 0.6508 0.0129 0.019417 0.004594232 0.7057 0.6728 0.0329 0.046670 0.005915212 0.7412 0.7215 0.0197 0.026542 0.007526182 0.7742 0.7499 0.0243 0.031405 0.009468212 0.8073 0.8114 -0.0041 -0.005118 0.011783670 0.8355 0.8333 0.0022 0.002631 0.014515520 0.8640 0.8532 0.0108 0.012520 0.017706521 0.8925 0.8894 0.0031 0.003478 0.021398440 0.9198 0.9083 0.0116 0.012561 0.025631230 0.9454 0.9271 0.0183 0.019348 0.030442240 0.9692 0.9465 0.0227 0.023446 0.035865448 0.9937 0.9669 0.0267 0.026920 0.041930798 1.0195 0.9889 0.0306 0.029986 0.048663601 1.0446 1.0130 0.0316 0.030210 0.056084011 1.0688 1.0398 0.0290 0.027139 0.064206667 1.0947 1.0697 0.0249 0.022762 0.073040441 1.1203 1.1028 0.0175 0.015636 0.082588248 1.1469 1.1385 0.0084 0.007326 0.092847057 1.1732 1.1753 -0.0021 -0.001756 0.103808001 1.1999 1.2117 -0.0118 -0.009871 0.115456402 1.2269 1.2466 -0.0197 -0.016060 0.127772301 1.2547 1.2793 -0.0246 -0.019621 0.140730694 1.2830 1.3099 -0.0269 -0.020972 0.154301897 1.3123 1.3385 -0.0263 -0.020026 0.168452203 1.3424 1.3656 -0.0232 -0.017246 0.183144197 1.3727 1.3914 -0.0187 -0.013621 0.198337302 1.4032 1.4163 -0.0131 -0.009302 0.213988706 1.4345 1.4406 -0.0061 -0.004279 0.230053306 1.4662 1.4735 -0.0073 -0.004982 0.246484801 1.5001 1.4974 0.0026 0.001759 0.263235897 1.5343 1.5216 0.0127 0.008275 0.280259013 1.5692 1.5709 -0.0017 -0.001084 0.297506303 1.6049 1.5962 0.0087 0.005412 0.314930797 1.6414 1.6491 -0.0077 -0.004689 0.332486212 1.6787 1.6764 0.0023 0.001390 0.350127310 1.7164 1.7050 0.0114 0.006640 0.367810607 1.7550 1.7598 -0.0047 -0.002699 0.385494202 1.7929 1.7908 0.0020 0.001140 0.403138310 1.8306 1.8229 0.0077 0.004203 0.420704991 1.8686 1.8695 -0.0009 -0.000485 0.438158900 1.9069 1.9016 0.0053 0.002781 0.455466807 1.9438 1.9490 -0.0052 -0.002667 0.472598106 1.9799 1.9794 0.0005 0.000236 0.489524394 2.0174 2.0089 0.0085 0.004226 0.506219923 2.0543 2.0572 -0.0029 -0.001403 0.522661209 2.0908 2.0848 0.0060 0.002869 0.538827300 2.1275 2.1373 -0.0098 -0.004601 0.554699600 2.1646 2.1637 0.0009 0.000431 0.570261598 2.2017 2.1900 0.0117 0.005328 0.585499227 2.2391 2.2438 -0.0047 -0.002110 0.600400090 2.2773 2.2703 0.0070 0.003084 0.614954293 2.3163 2.3272 -0.0109 -0.004725 0.629153311 2.3553 2.3548 0.0006 0.000239 0.642990828 2.3958 2.3832 0.0126 0.005264 0.656461716 2.4368 2.4413 -0.0045 -0.001850 0.669562697 2.4776 2.4714 0.0063 0.002523 0.682291925 2.5193 2.5315 -0.0122 -0.004850 0.694648683 2.5626 2.5624 0.0002 0.000090 0.706633508 2.6070 2.5934 0.0137 0.005240 0.718248010 2.6523 2.6599 -0.0076 -0.002867 0.729494929 2.6987 2.6897 0.0090 0.003323 0.740377605 2.7460 2.7554 -0.0094 -0.003439 0.750900388 2.7943 2.7837 0.0106 0.003801 0.761068285 2.8430 2.8538 -0.0109 -0.003817 0.770887017 2.8928 2.8809 0.0119 0.004113 0.780362606 2.9439 2.9702 -0.0262 -0.008902 0.789501607 2.9971 2.9968 0.0003 0.000103 0.798311174 3.0506 3.0236 0.0270 0.008847 0.806798697 3.1054 3.1191 -0.0137 -0.004405 0.814971626 3.1612 3.1467 0.0145 0.004580 0.822837889 3.2191 3.2340 -0.0149 -0.004619 0.830405474 3.2786 3.2630 0.0156 0.004751 0.837682605 3.3381 3.3532 -0.0151 -0.004525 0.844677329 3.3990 3.3833 0.0157 0.004627 0.851397991 3.4606 3.4764 -0.0158 -0.004571 0.857852995 3.5228 3.5064 0.0164 0.004647 0.864050388 3.5879 3.6066 -0.0187 -0.005213 0.869998574 3.6546 3.6353 0.0192 0.005256 0.875705481 3.7211 3.7418 -0.0207 -0.005562 0.881179392 3.7902 3.7691 0.0211 0.005577 0.886428118 3.8616 3.8841 -0.0225 -0.005816 0.891459525 3.9335 3.9107 0.0229 0.005810 0.896281302 4.0053 4.0294 -0.0241 -0.006026 0.900900900 4.0807 4.0562 0.0245 0.006002 0.905325770 4.1585 4.1835 -0.0250 -0.006022 0.909563184 4.2368 4.2114 0.0254 0.005986 0.913620114 4.3139 4.3381 -0.0242 -0.005608 0.917503417 4.3919 4.3674 0.0245 0.005573 0.921219707 4.4742 4.5012 -0.0270 -0.006025 0.924775481 4.5586 4.5313 0.0272 0.005970 0.928177178 4.6429 4.6694 -0.0266 -0.005721 0.931430817 4.7256 4.6989 0.0268 0.005669 0.934542298 4.8058 4.8337 -0.0279 -0.005807 0.937517405 4.8898 4.8617 0.0281 0.005748 0.940361619 4.9794 5.0120 -0.0325 -0.006533 0.943080306 5.0718 5.0391 0.0327 0.006451 0.945678592 5.1647 5.1969 -0.0322 -0.006226 0.948161721 5.2565 5.2241 0.0323 0.006148 0.950534225 5.3457 5.3456 0.0001 0.000018 0.952800930 5.4313 5.4564 -0.0251 -0.004613 0.954966187 5.5112 5.4860 0.0252 0.004569 0.957034409 5.5816 5.5992 -0.0176 -0.003151 0.959009588 5.6483 5.6306 0.0177 0.003132 0.960896015 5.7168 5.7382 -0.0214 -0.003744 0.962697208 5.7911 5.7696 0.0215 0.003713 0.964416981 5.8742 5.9060 -0.0318 -0.005416 0.966058910 5.9679 5.9360 0.0319 0.005348 0.967626274 6.0736 6.0735 0.0000 0.000008 0.969122529 6.1918 6.2426 -0.0508 -0.008207 0.970550597 6.3226 6.2717 0.0509 0.008053 0.971913695 6.4660 6.5278 -0.0618 -0.009556 0.973214507 6.6201 6.5582 0.0619 0.009349 0.974455774 6.7711 6.8266 -0.0555 -0.008191 0.975640416 6.9152 6.8597 0.0555 0.008032 0.976770699 7.0527 7.0527 0.0000 0.000003 0.977849126 7.1839 7.2294 -0.0455 -0.006332 0.978878021 7.3091 7.2635 0.0455 0.006232 0.979859591 7.4285 7.4691 -0.0407 -0.005474 0.980795979 7.5424 7.5017 0.0407 0.005397 0.981689274 7.6510 7.6510 0.0000 0.000001 0.982541502 7.7547 7.7878 -0.0331 -0.004263 0.983354270 7.8536 7.8205 0.0331 0.004214 0.984129488 7.9479 7.9750 -0.0271 -0.003413 0.984869003 8.0378 8.0107 0.0272 0.003378 0.985574186 8.1236 8.1453 -0.0216 -0.002664 0.986246824 8.2054 8.1838 0.0217 0.002640 0.986888289 8.2835 8.2835 0.0000 0.000000 0.987500012 8.3579 8.3749 -0.0170 -0.002036 0.988083303 8.4288 8.4118 0.0170 0.002021 0.988639593 8.4965 8.5105 -0.0139 -0.001641 0.989170074 8.5610 8.5471 0.0140 0.001630 0.989675879 8.6226 8.6226 0.0000 0.000000 0.990158200 8.6812 8.6812 0.0000 0.000000 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:01PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Cumulative Surface Area vs. Pore Width Cumulative Surface Area Pore Width (Angstroms) Cumulative Surface Area (m²/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 0.332258 13.5819 0.575734 14.8329 0.665497 15.9052 0.665497 17.1561 0.665497 18.5858 0.665497 20.0155 0.665497 21.6239 0.665497 23.411 0.665497 25.198 0.665497 27.3426 0.685365 29.4871 0.735288 31.8103 0.783785 34.3122 0.824785 36.9929 0.846496 40.0309 0.868246 43.2477 0.892882 46.6432 0.921474 50.3961 0.949384 54.3277 0.976903 58.7954 1.00095 63.4419 1.02318 68.4458 1.04806 73.9858 1.07098 79.8832 1.09509 86.3167 1.12717 93.1077 1.15918 100.613 1.1843 108.655 1.20777 117.233 1.23002 126.526 1.2529 136.713 1.27599 147.614 1.29968 159.409 1.32231 172.097 1.34479 185.858 1.36494 200.691 1.38447 216.596 1.40312 233.931 1.4199 252.517 1.43772 272.711 1.45513 294.513 1.46657 317.924 1.47578 343.301 1.48428 370.644 1.49148 400.309 1.50069 432.298 1.50937 466.789 1.5197 503.961 1.5351 544.171 1.54984 587.597 1.55902 634.419 1.56658 684.994 1.57503 739.679 1.58033 798.653 1.5847 862.452 1.58933 931.255 1.59278 1005.6 1.59483 1085.66 1.5964 1172.33 1.59814 1265.8 1.5991 1366.77 1.59954 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:01PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Incremental Surface Area vs. Pore Width Incremental Surface Area Pore Width (Angstroms) Incremental Surface Area (m²/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 0.332258 13.5819 0.243476 14.8329 0.0897627 15.9052 0 17.1561 0 18.5858 0 20.0155 0 21.6239 0 23.411 0 25.198 0 27.3426 0.0198682 29.4871 0.049923 31.8103 0.0484966 34.3122 0.0410001 36.9929 0.0217115 40.0309 0.0217492 43.2477 0.0246367 46.6432 0.0285917 50.3961 0.0279105 54.3277 0.0275185 58.7954 0.0240456 63.4419 0.0222357 68.4458 0.0248774 73.9858 0.022917 79.8832 0.0241158 86.3167 0.0320764 93.1077 0.0320047 100.613 0.025125 108.655 0.0234651 117.233 0.0222571 126.526 0.0228739 136.713 0.023096 147.614 0.0236838 159.409 0.0226383 172.097 0.0224789 185.858 0.0201439 200.691 0.0195298 216.596 0.0186514 233.931 0.0167836 252.517 0.0178154 272.711 0.0174101 294.513 0.0114372 317.924 0.00921867 343.301 0.00849622 370.644 0.0071985 400.309 0.00921243 432.298 0.00867878 466.789 0.0103351 503.961 0.0153984 544.171 0.0147401 587.597 0.00917258 634.419 0.00756362 684.994 0.00844904 739.679 0.00530317 798.653 0.00436352 862.452 0.00463526 931.255 0.00344979 1005.6 0.0020496 1085.66 0.00157438 1172.33 0.00173371 1265.8 0.000957287 1366.77 0.000447025 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:01PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Differential Surface Area vs. Pore Width Differential Surface Area Pore Width (Angstroms) Differential Surface Area (m²/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 10.8458 13.5819 7.18009 14.8329 2.61789 15.9052 0 17.1561 0 18.5858 0 20.0155 0 21.6239 0 23.411 0 25.198 0 27.3426 0.582091 29.4871 1.51906 31.8103 1.47367 34.3122 1.25095 36.9929 0.64862 40.0309 0.641144 43.2477 0.742154 46.6432 0.860759 50.3961 0.842798 54.3277 0.8221 58.7954 0.713997 63.4419 0.67378 68.4458 0.745144 73.9858 0.682982 79.8832 0.720447 86.3167 0.964267 93.1077 0.961661 100.613 0.749264 108.655 0.70683 117.233 0.673135 126.526 0.685284 136.713 0.68998 147.614 0.710122 159.409 0.679357 172.097 0.674348 185.858 0.60353 200.691 0.587633 216.596 0.56044 233.931 0.503713 252.517 0.534877 272.711 0.521144 294.513 0.343349 317.924 0.276961 343.301 0.255016 370.644 0.21578 400.309 0.275709 432.298 0.260135 466.789 0.310302 503.961 0.462318 544.171 0.442096 587.597 0.275283 634.419 0.227112 684.994 0.25347 739.679 0.159083 798.653 0.130856 862.452 0.138966 931.255 0.103458 1005.6 0.0615262 1085.66 0.0472597 1172.33 0.052008 1265.8 0.0287284 1366.77 0.0134118 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:01PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Cumulative Pore Volume vs. Pore Width Cumulative Pore Volume Pore Width (Angstroms) Cumulative Pore Volume (cm³/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 0.000210791 13.5819 0.000376135 14.8329 0.000442707 15.9052 0.000442707 17.1561 0.000442707 18.5858 0.000442707 20.0155 0.000442707 21.6239 0.000442707 23.411 0.000442707 25.198 0.000442707 27.3426 0.000469869 29.4871 0.000543473 31.8103 0.000620608 34.3122 0.000690948 36.9929 0.000731106 40.0309 0.000774638 43.2477 0.000827913 46.6432 0.000894593 50.3961 0.000964922 54.3277 0.00103967 58.7954 0.00111036 63.4419 0.0011809 68.4458 0.00126603 73.9858 0.00135081 79.8832 0.00144713 86.3167 0.00158557 93.1077 0.00173456 100.613 0.00186096 108.655 0.00198844 117.233 0.0021189 126.526 0.00226361 136.713 0.00242149 147.614 0.00259629 159.409 0.00277673 172.097 0.00297015 185.858 0.00315735 200.691 0.00335332 216.596 0.00355531 233.931 0.00375162 252.517 0.00397656 272.711 0.00421395 294.513 0.00438237 317.924 0.00452892 343.301 0.00467475 370.644 0.00480816 400.309 0.00499255 432.298 0.00518014 466.789 0.00542136 503.961 0.00580937 544.171 0.00621042 587.597 0.00647991 634.419 0.00671984 684.994 0.00700921 739.679 0.00720535 798.653 0.00737959 862.452 0.00757948 931.255 0.00774011 1005.6 0.00784316 1085.66 0.00792862 1172.33 0.00803025 1265.8 0.00809084 1366.77 0.00812138 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:01PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Incremental Pore Volume vs. Pore Width Incremental Pore Volume Pore Width (Angstroms) Incremental Pore Volume (cm³/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 0.000210791 13.5819 0.000165344 14.8329 6.6572e-005 15.9052 0 17.1561 0 18.5858 0 20.0155 0 21.6239 0 23.411 0 25.198 0 27.3426 2.71623e-005 29.4871 7.36041e-005 31.8103 7.71345e-005 34.3122 7.03402e-005 36.9929 4.01585e-005 40.0309 4.35321e-005 43.2477 5.32741e-005 46.6432 6.66804e-005 50.3961 7.03291e-005 54.3277 7.47508e-005 58.7954 7.06885e-005 63.4419 7.05338e-005 68.4458 8.51376e-005 73.9858 8.47768e-005 79.8832 9.63224e-005 86.3167 0.000138437 93.1077 0.000148994 100.613 0.000126396 108.655 0.000127481 117.233 0.000130464 126.526 0.000144708 136.713 0.000157876 147.614 0.000174803 159.409 0.000180437 172.097 0.000193428 185.858 0.000187195 200.691 0.000195972 216.596 0.000201991 233.931 0.00019631 252.517 0.000224934 272.711 0.000237396 294.513 0.00016842 317.924 0.000146542 343.301 0.000145838 370.644 0.000133404 400.309 0.000184391 432.298 0.000187591 466.789 0.000241216 503.961 0.00038801 544.171 0.000401056 587.597 0.000269489 634.419 0.000239925 684.994 0.000289377 739.679 0.000196132 798.653 0.000174247 862.452 0.000199885 931.255 0.000160632 1005.6 0.000103054 1085.66 8.54623e-005 1172.33 0.000101625 1265.8 6.05867e-005 1366.77 3.0549e-005 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:01PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Differential Pore Volume vs. Pore Width Differential Pore Volume Pore Width (Angstroms) Differential Pore Volume (cm³/g) 5.00387 0 5.36129 0 5.89742 0 6.43354 0 6.79096 0 7.32709 0 8.04193 0 8.57806 0 9.2929 0 10.0077 0 10.9013 0 11.7948 0 12.6884 0.00688076 13.5819 0.00487597 14.8329 0.00194154 15.9052 0 17.1561 0 18.5858 0 20.0155 0 21.6239 0 23.411 0 25.198 0 27.3426 0.000795792 29.4871 0.00223964 31.8103 0.0023439 34.3122 0.00214614 36.9929 0.00119972 40.0309 0.00128328 43.2477 0.00160482 46.6432 0.00200743 50.3961 0.00212369 54.3277 0.00223314 58.7954 0.00209899 63.4419 0.00213729 68.4458 0.0025501 73.9858 0.00252655 79.8832 0.00287758 86.3167 0.00416162 93.1077 0.0044769 100.613 0.00376931 108.655 0.00384004 117.233 0.0039457 126.526 0.00433532 136.713 0.00471645 147.614 0.0052412 159.409 0.00541478 172.097 0.00580267 185.858 0.00560854 200.691 0.00589663 216.596 0.00606945 233.931 0.0058917 252.517 0.00675327 272.711 0.00710608 294.513 0.00505604 317.924 0.00440263 343.301 0.00437737 370.644 0.00399888 400.309 0.00551845 432.298 0.0056228 466.789 0.00724228 503.961 0.0116495 544.171 0.0120288 587.597 0.00808778 634.419 0.0072042 684.994 0.00868126 739.679 0.00588353 798.653 0.00522543 862.452 0.00599258 931.255 0.00481729 1005.6 0.00309353 1085.66 0.0025654 1172.33 0.00304854 1265.8 0.00181822 1366.77 0.000916545 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:01PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Standard Deviation of Fit: 0.02968, cm³/g STP Goodness of Fit Input Data Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 4.90273e-006 0.0128345 3.01067e-006 0.0265556 2.64145e-006 0.0403348 3.0475e-006 0.0539532 4.15677e-006 0.0672834 6.21601e-006 0.0800843 9.34144e-006 0.0939413 1.35937e-005 0.107652 1.89817e-005 0.121115 2.56692e-005 0.134309 3.36969e-005 0.147192 4.41181e-005 0.161107 5.60239e-005 0.174593 6.93696e-005 0.187617 8.14081e-005 0.197877 9.46756e-005 0.208045 0.000113249 0.221161 0.000129123 0.231138 0.000146155 0.241013 0.000164359 0.250804 0.000183754 0.260495 0.000204548 0.270076 0.000226497 0.279572 0.00024963 0.288977 0.000274116 0.298282 0.000307637 0.310444 0.000335002 0.319524 0.000371234 0.331054 0.000409217 0.342374 0.000448445 0.353266 0.000488458 0.363721 0.000530314 0.37401 0.000571812 0.383648 0.000614215 0.39297 0.000656358 0.401807 0.00069866 0.41027 0.000741051 0.418325 0.000783677 0.426094 0.000825368 0.433379 0.00086738 0.440358 0.000908944 0.447036 0.000950026 0.453383 0.00099022 0.459376 0.0010293 0.465021 0.00106842 0.470459 0.00110637 0.475578 0.00114378 0.480438 0.0011804 0.485057 0.00121431 0.489288 0.00124766 0.493332 0.00127992 0.497098 0.00131125 0.500665 0.00134173 0.504026 0.00137167 0.507239 0.00142987 0.513854 0.00148924 0.52039 0.00154992 0.526825 0.00161148 0.533177 0.00167412 0.539417 0.00173845 0.545561 0.0018033 0.55165 0.0018693 0.557644 0.00193636 0.563526 0.00200495 0.569321 0.00207432 0.575039 0.00214468 0.580656 0.00221647 0.586187 0.00230935 0.59332 0.00239695 0.59978 0.0024791 0.605541 0.00255642 0.610637 0.00263472 0.615661 0.00271432 0.620603 0.0027948 0.625439 0.00287629 0.630206 0.00295881 0.634891 0.00304217 0.639493 0.00312647 0.643997 0.00321176 0.648474 0.00329794 0.652847 0.00338487 0.657121 0.00347275 0.661353 0.00356224 0.665441 0.00365319 0.66943 0.00374422 0.673481 0.00383697 0.677381 0.00392995 0.681201 0.00402393 0.684993 0.0041184 0.688668 0.00421368 0.692298 0.00430995 0.695792 0.00442981 0.700256 0.00452884 0.703599 0.00462912 0.706846 0.00473004 0.710056 0.00483099 0.713173 0.00493387 0.716177 0.00503734 0.719216 0.00514103 0.722118 0.00524646 0.724922 0.00535177 0.727691 0.00545836 0.730375 0.0055659 0.733049 0.00567349 0.735615 0.00578166 0.738126 0.00589032 0.740589 0.00600037 0.743019 0.00611155 0.745295 0.00622264 0.747547 0.00633419 0.749771 0.00644703 0.751995 0.00656152 0.754056 0.00667589 0.756148 0.00678983 0.758136 0.00741314 0.771722 0.00803785 0.785017 0.00869419 0.795671 0.00935832 0.805674 0.010034 0.815038 0.0302722 0.968469 0.0495382 1.04746 0.0696998 1.1109 0.0899651 1.16608 0.110441 1.21539 0.130479 1.26066 0.150574 1.30424 0.171178 1.34814 0.190653 1.38784 0.210767 1.42808 0.231572 1.46924 0.251656 1.51075 0.271042 1.55028 0.291238 1.59187 0.311267 1.63368 0.332289 1.67828 0.351269 1.71887 0.372248 1.76462 0.391448 1.8056 0.412538 1.85064 0.431565 1.89276 0.452945 1.93847 0.47279 1.98032 0.49291 2.02493 0.512889 2.06905 0.533405 2.11503 0.553174 2.16104 0.57299 2.20832 0.593125 2.25841 0.613266 2.31174 0.633172 2.36679 0.653431 2.42753 0.673583 2.4904 0.693317 2.55787 0.713682 2.63423 0.733686 2.71656 0.75371 2.80747 0.773974 2.909 0.794024 3.02424 0.814072 3.15487 0.834056 3.30807 0.85423 3.48729 0.874047 3.70139 0.894174 3.97332 0.914214 4.3253 0.934099 4.79426 0.953755 5.46727 0.972771 6.56621 0.990498 8.7226 Model Fit Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 5.07465e-006 0.0385216 8.99464e-006 0.0433516 1.552e-005 0.0512302 2.61021e-005 0.0642761 4.28409e-005 0.0861841 6.86973e-005 0.123443 0.000107744 0.184862 0.000165451 0.268367 0.000249 0.350668 0.000367617 0.417544 0.000532902 0.470282 0.000759152 0.512837 0.00106364 0.548197 0.00146685 0.578392 0.0019926 0.604849 0.00266816 0.628664 0.0035241 0.650844 0.00459423 0.672787 0.00591521 0.721479 0.00752618 0.749862 0.00946821 0.81143 0.0117837 0.833332 0.0145155 0.853202 0.0177065 0.889355 0.0213984 0.908287 0.0256312 0.927148 0.0304422 0.946519 0.0358654 0.966926 0.0419308 0.988904 0.0486636 1.01301 0.056084 1.03982 0.0642067 1.06974 0.0730404 1.10283 0.0825882 1.13846 0.0928471 1.17529 0.103808 1.21173 0.115456 1.24659 0.127772 1.27932 0.140731 1.3099 0.154302 1.33854 0.168452 1.36559 0.183144 1.3914 0.198337 1.4163 0.213989 1.44062 0.230053 1.47349 0.246485 1.49744 0.263236 1.52165 0.280259 1.57091 0.297506 1.59619 0.314931 1.64912 0.332486 1.67637 0.350127 1.70502 0.367811 1.75978 0.385494 1.79085 0.403138 1.82287 0.420705 1.86953 0.438159 1.90164 0.455467 1.94899 0.472598 1.97943 0.489524 2.0089 0.50622 2.0572 0.522661 2.0848 0.538827 2.13725 0.5547 2.1637 0.570262 2.19001 0.585499 2.24381 0.6004 2.27031 0.614954 2.32724 0.629153 2.35477 0.642991 2.38318 0.656462 2.44132 0.669563 2.47136 0.682292 2.53148 0.694649 2.56241 0.706634 2.59337 0.718248 2.65991 0.729495 2.68971 0.740378 2.75542 0.7509 2.78365 0.761068 2.85382 0.770887 2.8809 0.780363 2.97016 0.789502 2.99676 0.798311 3.02362 0.806799 3.11905 0.814972 3.14669 0.822838 3.23401 0.830405 3.26302 0.837683 3.35322 0.844677 3.38331 0.851398 3.47644 0.857853 3.50639 0.86405 3.60665 0.869999 3.63534 0.875705 3.74177 0.881179 3.7691 0.886428 3.88407 0.89146 3.91065 0.896281 4.02942 0.900901 4.05619 0.905326 4.18354 0.909563 4.21139 0.91362 4.33809 0.917503 4.36744 0.92122 4.5012 0.924775 4.53134 0.928177 4.66943 0.931431 4.69886 0.934542 4.83372 0.937517 4.86174 0.940362 5.01196 0.94308 5.03907 0.945679 5.19686 0.948162 5.22414 0.950534 5.34557 0.952801 5.45638 0.954966 5.48604 0.957034 5.59916 0.95901 5.6306 0.960896 5.73821 0.962697 5.76964 0.964417 5.90601 0.966059 5.93602 0.967626 6.07353 0.969123 6.24259 0.970551 6.27172 0.971914 6.52776 0.973215 6.55823 0.974456 6.82658 0.97564 6.85968 0.976771 7.0527 0.977849 7.22939 0.978878 7.26352 0.97986 7.46913 0.980796 7.50167 0.981689 7.65103 0.982542 7.78777 0.983354 7.82049 0.984129 7.97501 0.984869 8.01068 0.985574 8.14526 0.986247 8.18378 0.986888 8.28347 0.9875 8.37491 0.988083 8.41181 0.98864 8.51046 0.98917 8.54709 0.989676 8.62257 0.990158 8.68124 ASAP 2020 V3.05 H Unit 1 Serial #: 1413 Page 1 Sample: 000-597 cook sample 6cs-3 Operator: Submitter: File: C:\...\DOCUME~1\000-597.SMP Started: 8/22/2017 12:01:56PM Analysis Adsorptive: N2 Completed: 8/23/2017 10:37:52AM Analysis Bath Temp.: -196.004 °C Report Time: 9/1/2017 4:40:01PM Thermal Correction: No Sample Mass: 1.1235 g Warm Free Space: 16.4561 cm³ Measured Cold Free Space: 48.5698 cm³ Equilibration Interval: 30 s Low Pressure Dose: 0.010 cm³/g STP Automatic Degas: No Comments: Ann Cook sample rerun for isotherm Standard Deviation of Fit: 0.02968, cm³/g STP Goodness of Fit Input Data Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 4.90273e-006 0.0128345 3.01067e-006 0.0265556 2.64145e-006 0.0403348 3.0475e-006 0.0539532 4.15677e-006 0.0672834 6.21601e-006 0.0800843 9.34144e-006 0.0939413 1.35937e-005 0.107652 1.89817e-005 0.121115 2.56692e-005 0.134309 3.36969e-005 0.147192 4.41181e-005 0.161107 5.60239e-005 0.174593 6.93696e-005 0.187617 8.14081e-005 0.197877 9.46756e-005 0.208045 0.000113249 0.221161 0.000129123 0.231138 0.000146155 0.241013 0.000164359 0.250804 0.000183754 0.260495 0.000204548 0.270076 0.000226497 0.279572 0.00024963 0.288977 0.000274116 0.298282 0.000307637 0.310444 0.000335002 0.319524 0.000371234 0.331054 0.000409217 0.342374 0.000448445 0.353266 0.000488458 0.363721 0.000530314 0.37401 0.000571812 0.383648 0.000614215 0.39297 0.000656358 0.401807 0.00069866 0.41027 0.000741051 0.418325 0.000783677 0.426094 0.000825368 0.433379 0.00086738 0.440358 0.000908944 0.447036 0.000950026 0.453383 0.00099022 0.459376 0.0010293 0.465021 0.00106842 0.470459 0.00110637 0.475578 0.00114378 0.480438 0.0011804 0.485057 0.00121431 0.489288 0.00124766 0.493332 0.00127992 0.497098 0.00131125 0.500665 0.00134173 0.504026 0.00137167 0.507239 0.00142987 0.513854 0.00148924 0.52039 0.00154992 0.526825 0.00161148 0.533177 0.00167412 0.539417 0.00173845 0.545561 0.0018033 0.55165 0.0018693 0.557644 0.00193636 0.563526 0.00200495 0.569321 0.00207432 0.575039 0.00214468 0.580656 0.00221647 0.586187 0.00230935 0.59332 0.00239695 0.59978 0.0024791 0.605541 0.00255642 0.610637 0.00263472 0.615661 0.00271432 0.620603 0.0027948 0.625439 0.00287629 0.630206 0.00295881 0.634891 0.00304217 0.639493 0.00312647 0.643997 0.00321176 0.648474 0.00329794 0.652847 0.00338487 0.657121 0.00347275 0.661353 0.00356224 0.665441 0.00365319 0.66943 0.00374422 0.673481 0.00383697 0.677381 0.00392995 0.681201 0.00402393 0.684993 0.0041184 0.688668 0.00421368 0.692298 0.00430995 0.695792 0.00442981 0.700256 0.00452884 0.703599 0.00462912 0.706846 0.00473004 0.710056 0.00483099 0.713173 0.00493387 0.716177 0.00503734 0.719216 0.00514103 0.722118 0.00524646 0.724922 0.00535177 0.727691 0.00545836 0.730375 0.0055659 0.733049 0.00567349 0.735615 0.00578166 0.738126 0.00589032 0.740589 0.00600037 0.743019 0.00611155 0.745295 0.00622264 0.747547 0.00633419 0.749771 0.00644703 0.751995 0.00656152 0.754056 0.00667589 0.756148 0.00678983 0.758136 0.00741314 0.771722 0.00803785 0.785017 0.00869419 0.795671 0.00935832 0.805674 0.010034 0.815038 0.0302722 0.968469 0.0495382 1.04746 0.0696998 1.1109 0.0899651 1.16608 0.110441 1.21539 0.130479 1.26066 0.150574 1.30424 0.171178 1.34814 0.190653 1.38784 0.210767 1.42808 0.231572 1.46924 0.251656 1.51075 0.271042 1.55028 0.291238 1.59187 0.311267 1.63368 0.332289 1.67828 0.351269 1.71887 0.372248 1.76462 0.391448 1.8056 0.412538 1.85064 0.431565 1.89276 0.452945 1.93847 0.47279 1.98032 0.49291 2.02493 0.512889 2.06905 0.533405 2.11503 0.553174 2.16104 0.57299 2.20832 0.593125 2.25841 0.613266 2.31174 0.633172 2.36679 0.653431 2.42753 0.673583 2.4904 0.693317 2.55787 0.713682 2.63423 0.733686 2.71656 0.75371 2.80747 0.773974 2.909 0.794024 3.02424 0.814072 3.15487 0.834056 3.30807 0.85423 3.48729 0.874047 3.70139 0.894174 3.97332 0.914214 4.3253 0.934099 4.79426 0.953755 5.46727 0.972771 6.56621 0.990498 8.7226 Model Fit Relative Pressure (P/Po) Quantity Adsorbed (cm³/g STP) 5.07465e-006 0.0385216 8.99464e-006 0.0433516 1.552e-005 0.0512302 2.61021e-005 0.0642761 4.28409e-005 0.0861841 6.86973e-005 0.123443 0.000107744 0.184862 0.000165451 0.268367 0.000249 0.350668 0.000367617 0.417544 0.000532902 0.470282 0.000759152 0.512837 0.00106364 0.548197 0.00146685 0.578392 0.0019926 0.604849 0.00266816 0.628664 0.0035241 0.650844 0.00459423 0.672787 0.00591521 0.721479 0.00752618 0.749862 0.00946821 0.81143 0.0117837 0.833332 0.0145155 0.853202 0.0177065 0.889355 0.0213984 0.908287 0.0256312 0.927148 0.0304422 0.946519 0.0358654 0.966926 0.0419308 0.988904 0.0486636 1.01301 0.056084 1.03982 0.0642067 1.06974 0.0730404 1.10283 0.0825882 1.13846 0.0928471 1.17529 0.103808 1.21173 0.115456 1.24659 0.127772 1.27932 0.140731 1.3099 0.154302 1.33854 0.168452 1.36559 0.183144 1.3914 0.198337 1.4163 0.213989 1.44062 0.230053 1.47349 0.246485 1.49744 0.263236 1.52165 0.280259 1.57091 0.297506 1.59619 0.314931 1.64912 0.332486 1.67637 0.350127 1.70502 0.367811 1.75978 0.385494 1.79085 0.403138 1.82287 0.420705 1.86953 0.438159 1.90164 0.455467 1.94899 0.472598 1.97943 0.489524 2.0089 0.50622 2.0572 0.522661 2.0848 0.538827 2.13725 0.5547 2.1637 0.570262 2.19001 0.585499 2.24381 0.6004 2.27031 0.614954 2.32724 0.629153 2.35477 0.642991 2.38318 0.656462 2.44132 0.669563 2.47136 0.682292 2.53148 0.694649 2.56241 0.706634 2.59337 0.718248 2.65991 0.729495 2.68971 0.740378 2.75542 0.7509 2.78365 0.761068 2.85382 0.770887 2.8809 0.780363 2.97016 0.789502 2.99676 0.798311 3.02362 0.806799 3.11905 0.814972 3.14669 0.822838 3.23401 0.830405 3.26302 0.837683 3.35322 0.844677 3.38331 0.851398 3.47644 0.857853 3.50639 0.86405 3.60665 0.869999 3.63534 0.875705 3.74177 0.881179 3.7691 0.886428 3.88407 0.89146 3.91065 0.896281 4.02942 0.900901 4.05619 0.905326 4.18354 0.909563 4.21139 0.91362 4.33809 0.917503 4.36744 0.92122 4.5012 0.924775 4.53134 0.928177 4.66943 0.931431 4.69886 0.934542 4.83372 0.937517 4.86174 0.940362 5.01196 0.94308 5.03907 0.945679 5.19686 0.948162 5.22414 0.950534 5.34557 0.952801 5.45638 0.954966 5.48604 0.957034 5.59916 0.95901 5.6306 0.960896 5.73821 0.962697 5.76964 0.964417 5.90601 0.966059 5.93602 0.967626 6.07353 0.969123 6.24259 0.970551 6.27172 0.971914 6.52776 0.973215 6.55823 0.974456 6.82658 0.97564 6.85968 0.976771 7.0527 0.977849 7.22939 0.978878 7.26352 0.97986 7.46913 0.980796 7.50167 0.981689 7.65103 0.982542 7.78777 0.983354 7.82049 0.984129 7.97501 0.984869 8.01068 0.985574 8.14526 0.986247 8.18378 0.986888 8.28347 0.9875 8.37491 0.988083 8.41181 0.98864 8.51046 0.98917 8.54709 0.989676 8.62257 0.990158 8.68124